• Transactions of the Korean Society of Mechanical Engineers
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• v.4 no.3
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• pp.105-112
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• 1980

정현적 응력을 받고 있는 정탄성 결합부의 에너지 손실을 여러 가지 인자를 고려하여 구하였다. 탄성접착결합부의 해를 구하고 탄성해의 전단계수를 복소전단계수로 대치하여 점탄성 접착결 합부의 전단변형분포를 구하였다. 주어진 접착제의 최대강쇠현상은 접착제의 강성과 피접착물의 비를 증가 시킴으로서 얻을 수 있다. 구조적 결합부에서 파괴가 일어나지 않도록 피접착부와의 강성비를 결정함에 있어 주의를 요한다.

• Restorative Dentistry and Endodontics
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• v.34 no.5
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• pp.450-459
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• 2009

The aim of this study was to measure the initial dynamic modulus changes of light cured composites using a custom made rheometer. The custom made rheometer consisted of 3 parts: (1) a measurement unit of parallel plates made of glass rods, (2) an oscillating shear strain generator with a DC motor and a crank mechanism, (3) a stress measurement device using an electromagnetic torque sensor. This instrument could measure a maximum torque of 2Ncm, and the switch of the light-curing unit was synchronized with the rheometer. Six commercial composite resins [Z-100 (Z1), Z-250 (Z2), Z-350 (Z3), DenFil (DF), Tetric Ceram (TC), and Clearfil AP-X (CF)] were investigated. A dynamic oscillating shear test was undertaken with the rheometer. A certain volume ($14.2\;mm^3$) of composite was loaded between the parallel plates, which were made of glass rods (3 mm in diameter). An oscillating shear strain with a frequency of 6 Hz and amplitude of 0.00579 rad was applied to the specimen and the resultant stress was measured. Data acquisition started simultaneously with light curing, and the changes in visco-elasticity of composites were recorded for 10 seconds. The measurements were repeated 5 times for each composite at $25{\pm}0.5^{\circ}C$. Complex shear modulus G*, storage shear modulus G', loss shear modulus G" were calculated from the measured strain-stress curves. Time to reach the complex modulus G* of 10 MPa was determined. The G* and time to reach the G* of 10 MPa of composites were analyzed with One-way ANOVA and Tukey's test ($\alpha$ = 0.05). The results were as follows. 1. The custom made rheometer in this study reliably measured the initial visco-elastic modulus changes of composites during 10 seconds of light curing. 2. In all composites, the development of complex shear modulus G* had a latent period for $1{\sim}2$ seconds immediately after the start of light curing, and then increased rapidly during 10 seconds. 3. In all composites, the storage shear modulus G" increased steeper than the loss shear modulus G" during 10 seconds of light curing. 4. The complex shear modulus of Z1 was the highest, followed by CF, Z2, Z3, TC and DF the lowest. 5. Z1 was the fastest and DF was the slowest in the time to reach the complex shear modulus of 10 MPa.

• Transactions of the Korean Society for Noise and Vibration Engineering
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• v.21 no.1
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• pp.9-17
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• 2011

In this paper, the general equation of motion of damped sandwich beam with multi-viscoelastic material layer was derived based on the equation presented by Mead and Markus. The viscoelastic layer, which has characteristics of complex shear modulus, was assumed to be dominantly under shear deformation. The equation of motion of n-layered damped sandwich beam in bending could be represented by (n+3)th order ordinary differential equation. Finite element model for the n-layered damped sandwich beam was formulated and programmed using higher order shape functions. Several numerical examples were implemented to show the effects of damped material.

• The Korean Journal of Rheology
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• v.7 no.2
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• pp.120-127
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• 1995

중량비가 측쇄의 함량이 각각 4.37%(시료I)와 8.97%(시료II)인 두종류의 사과 펙틴을 이용하여 측쇄가 펙틴용액의 점탄성에 미치는 역할에 대하여 연구하였다. 시료II가 시료 I보 다 동일한 농도에서 더높은 전단속도에서는 오히려 시료 I의 전단점도가 시료 II보다 높은 값을 보였다. 시료I과 시료 II의 η0는 농도에 대하여 각각 η0 C4.23의 관계를보여 시료II가 더높은 농도의존성을 보였다. 한편 용액의 탄성특성을 나타내는 저장탄성계수(G＇)와 zero-shear recoverable compliance(Jeo)의 경우에는 시료II가 시료I보다 높은 값을 보였는데 이는 측쇄가 탄성과 밀접한 관계가 있다는 것을 의미한다. 펙틴용액의 전단점도와 복소점도 를 비교했을 때 거의 비슷한 값을 보였으나 예외적으로 고측쇄의 시료 II의 경우 고농도에 서 서로 상이한 값을 보였다. 본연구의 결과는 진한 용액하에서 측쇄가 분자간의 상호엉킴 에 상당한 기여를 하고 있음을 나타내었다.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2006.05a
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• pp.411-414
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• 2006

In this paper, the forced vibration of damped composite beam with arbitrary section was analyzed. The damping material was assumed to have either complex shear modulus or complex Young???smodulus. Damped composite beam could be modeled using beam elements with less D.O.F. rather than solid elements. Finite element method for these methods was formulated and programmed using complex values. The results of frequency responses revealed good agreement with those of NASTRAN in several beam structures.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2005.05a
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• pp.978-981
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• 2005

The vibration analysis of damped sandwich beam is conducted using finite element method. The equation of motion presented by Mead and Markus is used to formulate FEM. Also as the thickness of the core in the damped sandwich beam goes to zero, conventional beam theory based on the transformed-section method and the equation of Mead and Markus are compared. According to the change of thickness and loss factor of the core, the forced frequency response of beam is calculated and discussed. And then using the half-power band width method, the damping ratio of each mode is calculated and discussed about each case.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.33 no.5
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• pp.489-495
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• 2009

A novel technique to measuret of viscoelastic properties of polymers is proposed to investigate complex Poisson's ratio as a function of frequency. The forced vibration responses for the samples under the normal and the shear deformation are to be measured with varying load masses. The measured data were used to obtain the viscoelastic properties of the material based on an accurate 2D numerical deformation model of the sample. The 2D model enabled us to exclude data correction by the empirical form factor used in 1D model. Comprehensive measurements of viscoelastic properties of two slightly varied silicone RTV rubber ($Silastic^{(R)}$ S2) compositions were performed. Standard composition (90% PDMS polymer + 10% catalyst) and modified composition (92.5% polymer + 7.5% catalyst) were tested in temperature range from $30^{\circ}C$ to $70^{\circ}C$. Shear modulus, modulus of elasticity, loss factor, and both the real and the imaginary parts of the Poisson's ratio were determined for frequencies from 50 to 400Hz in the linear deformation regime (at relative deformations $10^{-4}{\sim}10^{-3}$).

• Korean Journal of Materials Research
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• v.2 no.3
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• pp.220-227
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• 1992

Electrorheological(ER) fluid's storage shear modulus(G') and loss factor(${\eta}$) have been directly measured using small amplitude forced oscillating rheometer as a function of oscillating frequency, strain amplitude and applied electric field. Two types of experiment were performed , (a) frequency sweep and (b) amplitude sweep. Two kinds of sample were employed for this experiment ; cornstarch particles in corn oil and zeolite particles in silicone oil. The storage shear modulus was a strong function of driving frequency. Generally, the modulus increased with driving frequency. On the other hand, the loss factor was not well behaved as storage modulus, but as the driving frequency increases the loss factor slightly decreases was the trend of the material's characteristics. Also the modulus was a strong function of strain amplitude. Generally, modulus decreased with increasing strain, but loss factor increases slightly with increasing strain amplitude. For G', cornstarch in corn oil ER fluid has higher values than zeolite based fluid as we increased applied electric field. On the other hand, zeolite based fluid has higher values for ${\eta}$. There is a reasonable agreement between theoretical calculation and experiment.

• Restorative Dentistry and Endodontics
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• v.36 no.5
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• pp.377-384
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• 2011

Objectives: The purpose of this study was to observe the change in the viscoelastic properties of thermoplasticized injectable root canal filling materials as a function of temperature and to compare the handling characteristics of these materials. Materials and Methods: Three commercial gutta perchas and Resilon (Pentron Clinical Technologies) in a pellet form were heated in the Obtura-II system (Obtura Spartan) at $140^{\circ}C$ and $200^{\circ}C$, and the extrusion temperature of the thermoplasticized materials was measured. The viscoelastic properties of the materials as a function of temperature were evaluated using a rheometer. The elastic modulus G', viscous modulus G", loss tangent tan${\delta}$, and complex viscosity ${\eta}^*$ were determined. The phase transition temperature was determined by both the rheometer and a differential scanning calorimeter (DSC). The consistency of the materials was compared under compacting pressure at $60^{\circ}C$ and $40^{\circ}C$ by a squeeze test. Results: The three gutta perchas had dissimilar profiles in viscoelastic properties with varying temperature. The phase transition of softened materials into solidification occurred at $40^{\circ}C$ to $50^{\circ}C$, and the onset temperatures obtained by a rheometer and a DSC were similar to each other. The onset temperature of phase transition and the consistency upon compaction pressure were different among the materials (p < 0.05). Resilon had a rheologically similar pattern to the gutta perchas, and was featured between high and low-flow gutta perchas. Conclusions: The rheological characteristics of the thermoplasticized root canal filling materials changed under a cooling process. The dissimilar viscoelastic properties among the materials require different handling characteristics during an injecting and compacting procedure.

• International Journal of Highway Engineering
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• v.1 no.2
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• pp.121-133
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• 1999

This study was based on the evaluation of 9 asphalts that were produced in five major Korean refineries. The study was concentrated to identify the problems of the current asphalt specification (KS M 2201) and to determine the ranges of visco-elastic asphalt behavior. As a conventional asphalt property. asphalt penetration, ring and ball(R&B) softening point, asphalt viscosity, and flash point of asphalt were measured. Also Dynamic Shear Rheometer (DSR) were used to evaluate visco-elastic properties of asphalts in the $-20^{\circ}C$ through $30^{\circ}C$ temperature range. These properties before and after the short-term (RTFO) and long-term (PAV) aging were compared and analyzed to achieve the research objectives. The conclusion from this study can be summarized by the followings. The low temperature rheological behavior of all the straight asphalt from five major Korean refineries is similar regardless of asphalt grade. In the mean while, the rheological behavior at high and intermediate temperature of Korean straight asphalt varies depending on asphalt grade.