• Title/Summary/Keyword: 반복측정 안정성

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Development of characteristics evaluating system for low vacuum gauges (저진공게이지 종합특성 평가장치 개발)

  • 홍승수;정광화;신용현;임인태;박근섭;정원호
    • Journal of the Korean Vacuum Society
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    • v.11 no.4
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    • pp.189-193
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    • 2002
  • We have developed a characteristics evaluating system for low vacuum gauges with a project of basis of vacuum technology construction. By using this system, we also performed a characteristics evaluation as to the accuracy, linearity, repeatability, gas sensitivity, and long-term stability of thermal conductivity gauges.

Estimation of conbined uncertainty for dioxin reference materials from the fly ash (소각재에 함유된 다이옥신의 확장불확도 평가)

  • Kim, Woo-Il;Shin, Sun-Kyoung;Lee, Su-Young;Kim, Dong-Hoon;Kang, Hak-Gu;Han, Jin-Suk
    • Analytical Science and Technology
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    • v.23 no.4
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    • pp.363-370
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    • 2010
  • This study was performed to validate reference materials (RMs) for proficiency testing (PT) in waste inter-laboratories. Dioxin RMs were prepared from fly ash in industrial incinerators. The relative standard deviations (RSDs) of analytical results were 2.6~15.7% for the dioxin RMs in 10 replicates (between and withinbottles). Data were collected and statistical analysis was performed by the One-way ANOVA test. The combined uncertainties of target isomers in dioxin analysis were 0.114~7.091.

Experimental studies on surface resistance method of levee based on bio-polymer (바이오폴리머 기반 제방 표면 강화 공법에 대한 실험적 연구)

  • Ko, Dongwoo;Kang, Joongu
    • Proceedings of the Korea Water Resources Association Conference
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    • 2019.05a
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    • pp.50-50
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    • 2019
  • 최근 국지성 호우 및 하천 제방의 노후화로 인한 제방 붕괴 피해가 빈번히 발생하면서 제방의 안정성 및 표면 보강을 위한 다양한 연구가 시도되고 있다. 본 연구에서는 제방 붕괴에 따른 피해 최소화 및 대책을 수립하기 위한 방법으로 시멘트와 같은 지구온난화를 야기시키는 물질이 아닌 친환경 신소재 바이오폴리머를 흙과 혼합한 재료를 활용하여 제방의 내구성을 강화하기 위한 연구가 수행되고 있다. 이에 안동하천실증연구센터에서는 현장토를 사용하여 높이 1 m, 폭 3 m, 사면경사 1 : 2, 총 길이 5 m 의 중규모 제방모형을 제작하였으며, 공동연구기관인 카이스트에서 개발된 바이오폴리머와 흙을 적정 비율로 혼합한 바이오-소일을 제방 전면에 일정 두께로 피복하여 월류 발생에 따른 제방 안정성 평가 실험을 수행하였다. 1차 실험은 흙 제방 조건이며, 2 3차 실험은 제방 표면에 5 cm 두께로 신소재가 피복된 조건으로 안정된 결과 도출을 위해 반복 실험을 수행하였다. 제방 천단면 및 사면에서의 유속분포를 측정하기 위해 드론 및 비디오카메라를 활용한 LSPIV 기법을 적용하여 실험조건에 따른 표면유속과 월류 흐름이 제방 붕괴에 미치는 영향에 대해 비교분석하였다. 또한 그래픽 소프트웨어를 이용한 픽셀기반 영상분석 기법을 적용하여 시간에 따른 제방사면의 붕괴면적을 산정하여 신소재 피복에 따른 붕괴 지연효과 분석을 통한 신소재 활용 제방의 현장 적용가능성 및 안정성을 평가하였다. 본 연구결과, 흙 제방의 경우 월류 흐름 발생 직후 침식현상이 전개되어 유속분포가 집중되고 있었으며, 이후 발생하는 강한 수직흐름으로 인해 입자추적을 통한 분석이 더 이상 불가능하였다. 신소재 제방의 경우 월류 흐름 발생 직후 침식은 발생하지 않았으며 일정시간동안 유속분포가 유지되었다. 지속적인 월류 흐름으로 인해 제방 끝단에서 침식이 발생하였으며 이때 최대 유속은 3.3 m/s 로 나타났다. 또한 픽셀기반 분석을 통해 30초 단위로 표면손실률을 산정한 결과, 신소재 활용 제방(2, 3차)의 경우 같은 실험조건에도 불구하고 최종 붕괴시간은 약 3배의 차이를 보였으며, 양생 과정에서의 크랙 발생을 최소화한다면 월류 발생 시 상당한 붕괴지연효과가 있는 것으로 판단된다.

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Measurement uncertainty for QC/QA applied to the chemical analysis (화학 분석 결과의 QA/QC를 위한 측정 불확도)

  • Woo, Jin-Chun;Oh, Sang-Hyub;Kim, Byoung-Moon;Bae, Hyun-Kil;Kim, Kwang-Sub;Kim, Young-Doo
    • Analytical Science and Technology
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    • v.18 no.6
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    • pp.475-482
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    • 2005
  • The expression of uncertainty applied to the chemical analysis is highly recommended with increasing demands upon the systematic quality assurance and control(QA/QC) with ISO 17025. For the quantification of quality source, 7 major common sources of uncertainty, normally contributing to the quality of the chemical analysis, were selected from QA/QC literatures of chemical analysis. They were classified into repeatability, drift, uncertainty in standards, linearity of calibration, homogeneity, stability of sample, and matrix effect. And, the quantification of the sources by means of measurement uncertainty was proposed as a prerequisite steps for QA/QC. Examples applied to the quantification procedures of modelling, combination and expression of standard uncertainty for the 7 major common sources were presented as a reference guide for QA/QC in chemical analysis.

Reliability study on rolling deformation of ITO thin film on flexible substrate (유연 기판상 ITO 박막의 롤링변형에 따른 신뢰성 연구)

  • Seol, Jae-Geun;Lee, Dong-Jun;Kim, Tae-Wook;Kim, Byoung-Joon
    • Journal of the Microelectronics and Packaging Society
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    • v.25 no.1
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    • pp.29-33
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    • 2018
  • Flexible electronics must be stable under various deformations such as bending, folding, and rolling. The reliability of ITO (Indium Tin Oxide) film used widely as a transparent electrode for flexible electronics has been studied using rolling fatigue test and bending test. During repeated rolling deformations, the electrical resistance was in-situ measured with different number of rotation. During rolling fatigue test, the electrical resistance of ITO film was significantly increased with increasing the number of rotation. As the stress state of ITO film is different according to the relative position of ITO and substrate, the rolling fatigue test was investigated under both outer and inner bending conditions. Inner rolling fatigue test showed superior electrical stability because the crack nucleation and propagation were retarded under compressive stress state.

Development of Nanoenzymes for the Production of Glucose from Seaweed and Various Polysaccharide (해조류 및 다당류로부터 포도당 생산을 위한 나노효소 개발 및 특성)

  • Jin, Lie-Hua;Lee, Jung-Heon
    • KSBB Journal
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    • v.25 no.5
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    • pp.453-458
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    • 2010
  • The magnetically separable polyaniline nanofiber enzymes were developed for the recycle of enzyme and enhanced enzyme stability. The stability of enzyme was maintained over 90% for 8 days under room temperature and vigorous shaking conditions (200 rpm). The residual activity of immobilized enzyme was over 60% after 8 days incubation at $55^{\circ}C$. Glucose was produced from various polysaccharides, agarose, curdlan, cellulose, and sea weed, using magnetically separable immobilized enzyme. Glucose production rate with curdlan was 1.2 g/(l h) and showed high decomposition rate due to high mass transfer. After 10 times recycle, the residual activity of immobilized enzyme was over 75%. 1 g/L of glucose was produced with 5 mg of immobilized enzymes.

Effects of self stretching exercise and movement with mobilization in lunge position on the muscle activity and balance in chronic stroke patients (런지자세에서의 자가 신장운동과 능동운동을 동반한 가동술이 만성 뇌졸중 환자의 근활성도 및 균형에 미치는 영향)

  • Jeong, Yong-Sik
    • Journal of Digital Convergence
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    • v.11 no.10
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    • pp.549-556
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    • 2013
  • In this study, we investigated the effects of stretching and movement with mobilization in lunge position on the muscle activity of the lower limb and limited of stability in chronic stroke patients with hemiplegia. Sixteen subjects were randomly selected and classified into the experimental and control groups. The experimental group performed self stretching exercises in the lunge position, and in the control group performed movement with mobilization in the lunge position. The interventions were conducted for 20 min, 5 times a week for 8 weeks. Statistical analyses were performed using repeated ANOVA. The analysis results showed no statistically significant between-group differences with respect to the muscle activity(%MVIC;maximum voluntary isometric contraction) of lower limb and limited of stability(LOS)(p>.05). However, statistically significant within-group differences were observed in the maximum voluntary isometric contraction and limited of stability for both the groups (p<.05). Therefore, self stretching in the lunge position is considered to have positive influences on the muscle strength and balance in stroke patients with hemiplegia.

Evaluation of Traffic Vibration Effect for Utilization of Abandoned Mine Openings (휴·폐광산 채굴 공동 활용을 위한 교통 진동 영향 평가)

  • Hyeon-Woo Lee;Seung-Joong Lee;Sung-Oong Choi
    • Tunnel and Underground Space
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    • v.33 no.2
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    • pp.95-107
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    • 2023
  • In this study, the effect of repeated traffic vibration on the long-term stability of mine openings is analyzed for re-utilization of abandoned mine galleries. The research mine in this study is an underground limestone mine which is developed by room-and-pillar mining method, and a dynamic numerical analysis is performed assuming that the research mine will be utilized as a logistics warehouse. The actual traffic vibration generated by the mining vehicles is measured directly, and its waveform is used as input data for dynamic numerical analysis, As a results of dynamic numerical analysis, after 20,000 repetitions of traffic vibration, the mine openings is analyzed to be stable, but an increase in the maximum principal stress and an additional area of plastic zone are observed in the analysis section. As shown in the changes of displacement, volumetric strain, and maximum principal stress which are measured at the mine opening walls. It is confirmed that if the repeated traffic vibration is continuously applied, the instability of the mine openings can be increased. Authors expect that the results of this study can be used as a reference for basic study on utilization of abandoned mine.

Comparison of Oxidative Stability for the Thermally-oxidized Vegetable Oils using a DPPH Method (DPPH법에 의한 식용유지의 열산화 안정성 비교)

  • Lee, Jae-Min;Chang, Pahn-Shick;Lee, Jae-Hwan
    • Korean Journal of Food Science and Technology
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    • v.39 no.2
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    • pp.133-137
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    • 2007
  • The 2,2-diphenyl picrylhydrazyl (DPPH) method, which can be used to predict the oxidative stability of edible oils, was previously reported by our research group. Not only free radical scavenging antioxidants but also radicals from oxidized oils are capable of reacting with DPPH radicals, thereby reducing the absorbance of DPPH. In this study, the optimum sample size of edible oils for the DPPH method was determined, and the oxidation of the edible oils was monitored via DPPH, coupled with other conventional methods. The optimum sample size was determined as 1.5 g using soybean oil. Soybean, corn, virgin olive, and refined olive oils were thermally oxidized for 3 hr at $180^{\circ}C$ and analyzed via DPPH, conjugated dienoic acid (CDA) value, and p-anisidine value (p-AV) protocols. Soybean and corn oils were found to be more sensitive to thermal oxidation than virgin and refined olive oils, on the basis of the CDA value and p-AV measurements. The DPPH method can indicate the inherent radical scavenging activity of unoxidized samples, the time required for the depletion of antioxidants, and the rate of degradation of the antioxidants. The soybean and corn oils evidenced higher levels of free radical scavenging compounds, required more time for the consumption of inherent antioxidants, and also manifested steeper antioxidant degradation rates than olive oils, based on the results of DPPH analysis. The DPPH method, accompanied by other conventional methods, may prove useful in predicting the degree of oxidation of vegetable oils.

A Effect of the Shoulder Stabilizer Muscle Activity During a Push-up-Plus on a Different Condition Surface (다른 지면 조건에서의 푸시업 플러스 운동이 어깨 안정근의 근 활성도에 미치는 영향)

  • Kim, Jin-Seop;Lee, Dong-Yeop
    • Journal of Digital Convergence
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    • v.10 no.1
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    • pp.399-405
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    • 2012
  • The purpose of this study was to compare the shoulder stabilizer muscle activity during a push up plus on a different conditioning surface. Eighteen healthy volunteers were tested. Surface EMG was recorded from the upper trapezius(UT), pectoralis major(PM), and serratus anterior(SA) using surface differential conditions. Measurements were performed for 7 days. The mean root mean square (RMS) of EMG activity was calculated. A one-way repeated measures analysis of variance was performed to compare RMS normalized values. The UT and PM did not show significant differences of electric activation amplitude in relation to different surface conditions(p>.05). However, the SA showed greater mean electric activation amplitude values on the push up plus exercise on a upper and lower unstable surface(p<.05). These results suggest that to improve SA EMG activity is more useful when performed on a upper and lower unstable surface conditions than on a stable surface conditions.