• Journal of the Korean Crystal Growth and Crystal Technology
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• v.16 no.3
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• pp.101-105
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• 2006

We fabricated the nano $TiN_x$ by making of reaction between titanium powder and $Si_3N_4$ during planetary milling. The $TiN_x$ powder was sintered by spark plasma sintering machine after mixing with 50 wt% of titanium powder, and the sintered body was heat-treated at $850^{\circ}C$ in order to investigate its hardness property at the elevated temperature. We analyzed crystal structure by XRD. We observed the peaks of $TiN_{0.26}$ and TiN after 10 hours milling, and we observed TiN peak mainly after 20 hours milling. The reacted particle size distribution was investigated by FE-SEM. Increase of milling time, the size of reacted particles was decreased and the $10{\sim}20nm$ size of $TiN_x$ on the surface of titanium and $TiN_x$ was observed after 20 hours milling. The micro-Vickers hardness of mixed sintered body was about $1050kgf/mm^2$.

• Journal of the Korean Institute of Gas
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• v.24 no.5
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• pp.39-46
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• 2020

This paper is considered about centerline segregation of API 5L steel used in pipeline. Mn/S, Nb and C were known as segregated elements in the centerline of pipe thickness. The Mn usually was accompanied by S consisting of long viscous shape. Microstructure of the centerline was composed of MnS and Nb/Ti indusions including oxide. The segregation effect in centerline region was analyzed by OM, SEM/EDS and micro Vickers hardness. The Mn, Nb and C are retarded elements in transformation from austenite to ferrite or martensite. These elements could derive a bainitic microstructure as a kind of martensite, which is different from difference and element segregation between in matrix and centerline derived from steel melting and heat treatment.

• Journal of the Korean Society for Railway
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• v.13 no.4
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• pp.447-454
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• 2010

The defects of rail head induced by fatigue and deterioration are mainly classified by two types ; one occurred on the surface of rail head the another occurred on the inner rail head. This study performed the surface irregularity measurement of rail head according to the passing tonnage in the urban railway. Also, we carried out microscopic structure test, chemical component test and micro-hardness test for the specimen which is the used rail on metro line by accumulated passing tonnage. As a result of this study, for new rail, it should be performed initial grinding in order to remove 0.3mm of de-carbonized layer. The preventive-cyclic grinding for preventing RCF defects is proposed two options : grinding by the whole line and grinding by specified sections.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.34 no.4
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• pp.475-480
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• 2010

The thermal barrier coating of a gas turbine blade was degraded by isothermal heating in a furnace and by varying the exposure time and temperature. Then, a micro-Vickers hardness test was conducted on the cross section of the bond coat and Ni-based superalloy substrate. Further, the thickness of TGO(Thermally Grown Oxide) was measured by using an image analyzer, and the changes in the microstructure and element contents in the coating were analyzed by using an optical microscope and by performing SEM-EDX analysis. No significant change was observed in the Vickers hardness of the bond coat when the coated specimen was degraded at a high temperature; delamination was observed between the top coat and the bond coat when the coating was degraded for 50 h at a temperature $1,151^{\circ}C$.

• Journal of Advanced Marine Engineering and Technology
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• v.24 no.5
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• pp.58-68
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• 2000

When SS400 steel was welded with low hydrogen type and ilmennite type welding, the effect of post-weld heat treatment(PWHT) was investigated with parameters such as micro vickers hardness, corrosion potential, polarization behaviors, galvanic current, Al anode generating current and Al anode weight loss etc. Hardness of each parts(HAZ, BM, WM) by PWHT in case of low hydrogen type and ilmennite type welding was lower than that of each parts by As-welded However hardness of WM area in case of low hydrogen type and ilmennite type welding was the highest among those three parts regardless of PWHT, Whereas in case of ilmennite type welding, WM area was the highest potential among these three parts on galvanic potential series with As-welded while BM area was the highest potential among these three parts by PWHT on the contrary. And in case of low hydrogen type welding, galvanic corrosion and micro cell corrosion of welding parts was decreased with PWHT. However, It was increased with PWHT in case of ilmennite type welding. Moreover Al anode generating current and anode weight loss in case of low hydrogen type was decreased by PWHT compared to As-wedled but, which was increased than that of As-welded in case of ilmennite type welding. Therefore, it is suggested that Corrosion resistance property in case of low hydrogen type welding is increased by PWHT. However its property was devreased with PWHT in case of ilmennite type welding.

• Journal of the Korean Society for Nondestructive Testing
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• v.18 no.5
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• pp.381-388
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• 1998

The ultrasonic method, which is well known as non-destructive test method, is widely used to evaluate the material damage caused by degradation practically. However, this method is just used for measuring the crack size and the thickness loss of tube. The purpose of this study is to investigate the applicability of the ultrasonic technique for the evaluation of carburized material and to suggest the correlations between the ultrasonic characteristics and carburized degradation. The miniaturized specimens($40{\times}20{\times}6.3mm$) are adopted from the HK-40 (25Cr-20Ni-0.4C) centrifugal cast tube after carburization treatment. Carburization was carried at $1200^{\circ}C$ by the pack method. The results of ultrasonic test present that the longitudinal wave velocity increased with the increase of carburized depth. The correlation between the longitudinal wave velocity and carburization was changed with the density and Young's modulus. Therefore, the average velocity in the materials carburized for 336 hours and the unused one were 5,840 m/s and 5,755 m/s at 5 MHz, respectively. With the obtained results from this study, it can be recognized that the technique using the ultrasonic velocity property is very useful method to evaluate the degree of carburized material non-destructively.

• Journal of Korea Foundry Society
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• v.41 no.2
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• pp.127-131
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• 2021

Based on its good compatibility with high-temperature environments, the Ti-48Al-2Cr-2Nb alloy is used for high-temperature materials of industrial equipment. In this study, a Ti-48Al-2Cr-2Nb alloy turbocharger turbine wheel was fabricated by a vacuum centrifugal casting method. The conditions that prevent misrun defects of the turbocharger turbine wheel blade from centrifugal casting using alumina molds were investigated. The microstructure of the alloy prepared by vacuum centrifugal casting was studied by means of optical microscopy (OM), with a micro-Vickers hardness analyzer (HV), by X-ray diffraction (XRD) and by SEM-EDS. The HV and SEM-EDS examinations of the as-cast Ti-48Al-2Cr-2Nb alloy showed that the thickness of the oxide layer (α-case) was typically less than 50 ㎛. At a high preheating temperature of 1,100℃, a moderate RPM of 260, and with an alumina mold with a large gate size, there were almost no misrun defects. Therefore, it was confirmed that a Ti-48Al-2Cr-2Nb alloy turbocharger turbine wheel with fewer misrun defects could be achieved through a high preheating temperature, a moderate RPM, a large gate size and an alumina mold to suppress the formation of alpha-case components.

• Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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• 2002.05a
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• pp.23-28
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• 2002

This paper describes the machining characteristics of the $MoSi_2$ based composites by electric discharge drilling with various tubular electrodes, besides, Hardness characteristics and microstructures of $Nb/MoSi_2$ laminate composites were evaluated from the variation of fabricating conditions such as preparation temperature, applied pressure and pressure holding time. $MoSi_2$ -based composites has been developed in new materials for jet engine of supersonic-speed airplanes and gas turbine for high- temperature generator. Achieving this objective may require new hard materials with high strength and high temperature-resistance. However, With the exception of grinding, traditional machining methods are not applicable to these new materials. Electric discharge machining (EDM) is a thermal process that utilizes a spark discharge to melt a conductive material, the tool electrode being almost non-unloaded, because there is no direct contact between the tool electrode and the workpiece. By combining a nonconducting ceramics with more conducting ceramic it was possible to raise the electrical conductivity. From experimental results, it was found that the lamination from Nb sheet and $MoSi_2$ powder was an excellent strategy to improve hardness characteristics of monolithic $MoSi_2$. However, interfacial reaction products like (Nb, Mo)$SiO_2$ and $Nb_2Si_3$ formed at the interface of $Nb/MoSi_2$ and increased with fabricating temperature. $MoSi_2$ composites which a hole drilling was not possible by the conventional machining process, enhanced the capacity of ED-drilling by adding $NbSi_2$ relative to that of SiC or $ZrO_2$ reinforcements.