• Title/Summary/Keyword: 노화시험

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Study on the Degradaion Behavior of Acrylonitrile Rubber(NBR) O-ring by Intermittent CSR and Time-Temperature Superposition Principle (간헐 압축응력완화 시험법과 시간-온도 중첩 이론을 이용한 NBR 오링의 노화 거동 분석 연구)

  • Lee, Jin Hyok;Bae, Jong Woo;Choi, Myung Chan;Yun, Yu Mi;Kim, Wonho;Park, Sung Han;Jo, Nam-Ju
    • Journal of the Korean Society of Propulsion Engineers
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    • v.23 no.1
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    • pp.46-51
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    • 2019
  • Intermittent CSR testing was used to investigate the degradation of a NBR O-ring, and also the prediction of its life-time. An intermittent CSR jig was designed taking into consideration the O-ring's environment under use. Degradation of O-rings by thermal aging was observed between $40^{\circ}C$ and $120^{\circ}C$. O-rings showed non-linear degradation behavior under $80^{\circ}C$. At 20% of failure condition, predicted life-times were 32.5 years by Arrhenius plot and 22.6 years by WLF plot.

A Study on Discoloration of Traditional Paintings by an Inorganic Pigment (무기 안료에 의한 전통회화의 변색 연구)

  • Kim, Dong Won;Kwak, Sam Tak;Seo, Yong Soo;Kim, Il Kyu;Moon, Myung Jun
    • Applied Chemistry for Engineering
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    • v.23 no.6
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    • pp.567-571
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    • 2012
  • The discoloration of traditional paintings could be induced by various chemical reactions of inorganic pigments due to temperature, humidity, light and air pollution. In this study, we made artificial samples including azurite and malachite as inorganic pigments using the traditional method on hanji called 'Korean paper'and investigated the artificial aging process occurred by the interaction between pigments and environmental factors. It was found that the azurite was influenced by the humidity of weathering tests and the salt fog of salt spray tests according to XRD and TGA results. However, it was shown that the malachite was chemically changed by the ultraviolet radiation of weathering tests and UV radiation tests according to color difference and TGA results.

Evaluation of Dynamic Modulus based on Aged Asphalt Binder (아스팔트 바인더의 노화특성을 고려한 동탄성계수 평가)

  • Lee, Kwan-Ho;Cho, Kyung-Rae;Lee, Byung-Sik;Song, Yong-Seon
    • Journal of the Korean Society of Hazard Mitigation
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    • v.8 no.3
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    • pp.51-58
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    • 2008
  • Development of a new design guide which is based on empirical-mechanistic concept for pavement design is in action. It is called AASHTO 2002 Design Guide in USA and the KPRP(Korean Pavement Research Project) in Korea. The material characteristic of hot mix asphalt is a key role in the design guide. Therefore it is urgent to get a proper materials database, especially the dynamic modulus of hot mix asphalt. In this research, dynamic modulus test, which is based on aged asphalt binder, has been carried out and proposed the predicted equation of dynamic modulus. Nine different hot mix asphalt with three different asphalt binder have been used for the dynamic modulus test. Short-term aging, which is covers the time for the production of asphalt plant, transportation, lay-down, and compaction, can be simulated at $135^{\circ}C$ with 2 hour curing. Long-term aging has been carried out for a performance period of asphalt pavement. The dynamic modulus of asphalt pavement increases with aging time. As the nominal aggregate size increases, the change of dynamic modulus is not big.

A Study on the Life Time Prediction and Acid-Heat aging Property of NBR Rubber for Fuel Cell Gasket (연료전지 카스켓용 NBR 고무의 산-열 노화 특성과 수명예측에 관한 연구)

  • Kim, Mi-Suk;Kim, Jin-Hak;Kim, Seok-Jin;Kim, Jin-Kuk
    • Elastomers and Composites
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    • v.42 no.1
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    • pp.20-31
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    • 2007
  • Material characteristics and lifetime evaluation are very important in design procedure to assure the safety and reliability of the rubber components. In this paper, the NBR compound was prepared by sulfur-cure system, and was used in predicting the lifetime of rubber gasket made by the compound. The accelerated material aging was investigated at different temperatures at 120, 140 and $160^{\circ}C$ and aging time from 3 hours to 600 hours at 5, 6, 7 vol %. of $H_2SO_4$ concentrations The rubber strips were placed in acid solution using pyrex g1ass tube. Both ends of pyrex g1ass tube were sealed to avoid evaporation of solution during heating at given time. The material test and accelerated acid-heat aging test were carried out to predict the useful life of NBR rubber gasket for a fuel cell stack. In order to investigate the effects of acid-heat aging on the properties of the NBR, tensile strength, elongation at break, hardness and crosslink-density were measured. The tensile strength decreases as the $H_2SO_4$ concentrations and temperature increase. Results were evaluated using Arrhenius equation.

Relationship between Leaf Senescence and Photosynthate Translocation during Grain filling in Barley (대맥의 등숙기간중 엽신의 노화와 동화산물의 전류와의 관계)

  • 남윤일;구본철;연규복;맹돈재
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.36 no.1
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    • pp.34-40
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    • 1991
  • The study aimed to investigate the relationship between the rates of leaf senescence and photosynthate translocation at post-anthesis. Seven barley varieties were observed at Suweon in 1988-89. The varieties differed significantly in the number of leaves survived and the rate of photosynthate transolcation with the progress of grain filling. The rate of grain filling was higher in the fast leaf sene-scencing varieties than the slow senescencing ones. There was a close coincidence between the rates of grain filling and $\^$14/c translocation into grains. Photosynthesis was higher in the fast leaf senescencing varieties at early stage of grain filling, but the reverse phenomenon was observed at the late stage of grain filling. The grain yield of fast senescencing varieties was higher than that of slow ones.

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Evaluation of the Aging Effects on the Performance of the Pyrotechnic Igniter (파이로 테크닉 점화기의 노화 성능 평가)

  • 장승교;류병태
    • Journal of the Korean Society of Propulsion Engineers
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    • v.1 no.2
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    • pp.91-102
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    • 1997
  • In order to evaluate the effects of aging on the ignition performance, pyrotechnic igniters were separated from twelve-year-old, fifteen-year-old, and sixteen-year-old live rocket motors. The characteristic values of the ignition material were measured, and the firing tests of the igniters were performed. The moisture content, the outer dimension, the crush strength, the thermal decomposition characteristics, and the heat of formation the B/$KNO_3$ ignition pellet were measured. The crush strength was increased and the heat of formation was reduced as aged, but no change was detected for other characteristic values. The burning test results of the igniter pellet in the closed bomb and the inert motor showed that the burning rate of the ignition pellet was increased by 10%, and the integration of pressure $P_t$ of the p-t curve was reduced by 15% for aged samples. It was inferred that the burning rate was increased as the crack was appeared in the pellet and $P_t$ could be proportionally decreased with the heat of explosion.

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Study of Aging and Performance About Separation Devices Has Been Stored (장기 보관된 분리장치의 성능 및 노화에 관한 연구)

  • Kim, Dong-seong;Jin, Hong-Sik
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.49 no.7
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    • pp.565-572
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    • 2021
  • In this study, a study on the performance and aging of explosive bolts stored for a long time among pyrotechnic mechanical devices(PMD) used as separation devices in the defense field is conducted. For this, explosive bolts that had been installed in the weapon system for about 10 years are secured. Performance and life extension test procedures are established based on the AIAA Standard and MIL-STD. Before performance evaluation, non-functional tests are performed to check whether external changes or failures occurred. Next, circuit inspection and X-ray tests are conducted to check the failure in internal circuits and structures. After that, performance test is carried out to confirm the operation of the samples that passed the non-functional test. Through this test, separation of bolt and separation time are measured, and some samples are tested after a high temperature storage test to confirm the remaining life and the possibility of extension. Finally, the remaining life and reliability are predicted based on the results of the test and the Arrhenius model to identify remaining shelf life and reliability depend on time.

Procedure and Method of Equipment Qualification for Solenoid-Operated Valves Used in Nuclear Power Plants (원전용 솔레노이드 밸브의 기기검증 절차 및 방법)

  • Lim, Byung-Ju;Park, Chang-Dae;Chung, Kyung-Yul
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.35 no.6
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    • pp.683-691
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    • 2011
  • In order to develop technology for an equipment qualification (EQ) test, which is an important process in localizing solenoid-operated valves used in nuclear power plants, we analyzed related regulations, test procedures, conditions, equipment, and acceptance criteria. EQ regulations for the solenoid-operated valve are classified as law, guide, and standard, and are subdivided according to test specimens and contents. The EQ test is composed of functional, normal-, and accident- condition tests. The solenoid-operated valve is aged under normal and accident conditions, which are predicted in the design conditions of a nuclear power plant, and the performance of the valve is measured by a functional test. The test method and procedure analyzed in this paper might be very useful for manufacturers as well as EQ testers.

Influence of Filler and Cure Systems on Whitening of EPDM Composites by Formation of Metal Salt (충전 시스템과 가교 시스템이 금속염 형성에 의한 EPDM 복합체의 백화에 미치는 영향)

  • Chung, Hye-Seung;Choi, Sung-Seen
    • Elastomers and Composites
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    • v.47 no.3
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    • pp.210-215
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    • 2012
  • Whitening phenomena of the EPDM composites with different inorganic filler compositions which were aged at $90^{\circ}C$ for 7 days in air and tap water atmospheres, respectively, were investigated. The aged samples in tap water containing stearic acid exhibited severe whitening phenomena, while all the samples aged in air did not show any whitening. Depending on the filler compositions, there was no big difference in the whitening phenomena. The whitening materials were analyzed using gas chromatography/mass spectrometry (GC/MS), image analysis, energy-dispersive X-ray spectroscopy (EDX), and attenuated total reflectance-Fourier transform infrared spectroscopy (ATR-FTIR). The whitening materials were identified to be salts of stearic acid. The salts of stearic acid were formed by reaction of metal cation in tap water and stearic acid in the sample.

Retrogradation Characteristics of Jeolpyon Prepared by Different Moisture Addition (수분 첨가량에 따른 절편의 노화도에 관한 연구)

  • 윤숙자
    • Korean journal of food and cookery science
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    • v.16 no.5
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    • pp.402-409
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    • 2000
  • Jeolpyon was prepared by different moisture addition and then retrogradation characteristics and quality evaluation were investigated during storage periods. In Hunter's color value, lightness of Jeolpyon was decreased, whereas yellowness was increased during storage. In texture profile analysis, hardness, gumminess and chewiness of Jeolpyon were increased during storage and texture parameters were decrease by increasing moisture level. Jeolpyon prepared with 35% moisture addition was slowly retrograded in avrami equation. In the results of sensory evaluation, the parameters were significantly different during storage. The results showed that Jeolpyon prepared with 35% moisture addition had good sensory quality and slow rate of retrogradation.

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