• Title/Summary/Keyword: 금속화

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The Micro Coil Production through Research on the Additive Conditions of Electrochemical Metal 3D Printer (전기화학적 금속 3D 프린터의 적층 조건 연구를 통한 마이크로 코일 제작)

  • Kim, Young-Kuk;Kang, Donghwa;Kim, Sung-Bin;Yoo, Bongyoung
    • Journal of the Korean institute of surface engineering
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    • v.53 no.4
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    • pp.138-143
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    • 2020
  • In this study, we produced a coil of micro-pattern that can be used for electromagnetic wave absorber, heating material, wireless charging, sensor, antenna, etc. by using electrochemical additive manufacturing method. Currently, it contains research contents for manufacturing a micro pattern coil having practicality through control of process control variables such as applied voltage, distance between electrode, and nozzle injection. Circulation of the electrolyte through the nozzle injection control can significantly contribute to improving the surface characteristics of the coil because of minimizing voltage fluctuations that may occur during the additive manufacturing process. In addition, by applying the pulse method in the application of voltage, the lamination characteristics of the plated body were improved, which showed that the formation of a fine line width plays an important role in the production of a micro pattern coil. By applying the pulse signal to the voltage application, the additive manufacturing characteristics of the produced product were improved, and it was shown that the formation of a fine line width plays an important role in the production of a micro pattern coil.

Study on Evaluation of Carbon Fiber Reinforced Composite Groove Using Inverse Ballistics Technology (역탄도 기법을 이용한 탄소섬유/열경화성수지 복합재 그루브의 파단 특성 연구)

  • 최재호;박인서;송흥섭;박관진
    • Composites Research
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    • v.17 no.2
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    • pp.15-20
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    • 2004
  • It is a primary object of the present study to test and evaluate the shear load carrying capability of a carbon fiber reinforced thermoses composite structure with buttress grooves for military applications. The buttress form of groove is an effective structure in any applications where high shear loads are transferred in one direction between structural components. Inverse ballistics methodology was introduced to investigate the high strain rate properties of composite groove specimens. In comparison with the conventional methods, inverse ballistics technique is a proper one under dynamic environment.

A Study on the Reason of the Changes of MILC Poly-Si TFT's Characteristics by Electrical Stress (전기적 스트레스에 의한 MILC poly-Si TFT 특성변화 원인에 관한 연구)

  • Kim, Gi-Bum;Kim, Tae-Kyung;Lee, Byung-Il;Joo, Seung-Ki
    • Journal of the Institute of Electronics Engineers of Korea SD
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    • v.37 no.12
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    • pp.29-34
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    • 2000
  • The effects of electrical stress on MILC(Metal Induced Lateral Crystallization) poly-Si TFT were studied. After the electrical stress was applied on the TFT’s which were fabricated by MILC process, off-state(VG<0V) current was reduced by $10^2{\sim}10^4$ times. However, when the device on which electrical stress was applied was annealed in furnace, the off-state current increased as annealing temperature increased. From the dependence of off-state current on the post-annealing temperature, activation energy of the trap states in MILC poly-Si thin films was calculated to be 0.34eV.

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Synthesis and Characterization of Square Planar Mixed-Ligand Complexes (Ⅰ) : Synthesis and Spectroscopic Property of M(S-S)(N-N) Type Complexes with Ni (Ⅱ), Pd (Ⅱ), and Pt (Ⅱ) (평면사각형 혼합 리간드 착물의 합성과 그 특성 (제 1 보) : Ni (Ⅱ), Pd (Ⅱ) 및 Pt (Ⅱ) 의 M(S-S)(N-N) 형 착물의 합성과 분광학적 성질)

  • O, Sang O;Jeong, Deok Yeong
    • Journal of the Korean Chemical Society
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    • v.34 no.6
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    • pp.593-599
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    • 1990
  • A series of new, square planar, and mixed-ligand complexes of Ni(Ⅱ), Pd(Ⅱ), and Pt(Ⅱ) have been prepared. From the observation of electronic spectrum for the variation of the ligand substituents, the very intense absorption band in the visible range is by the electronic transition of dithiolene to diimine ligand, HOMO to LUMO. In the various solvent systems the IT band shows the similar behavior to IT transition of mixed-valence dinuclear complexes followed with Hush theory, happens rto dominently by the inner sphere charge transfer transition. The negative solvatochromism represents that the excited-state electric dipole is reduced or reversed by the electronic transition.

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A Study on the Synthesis, Electronic Structure, and Electrochemical Behavior of Rare Earth Metal(III) Complexes (II) (희토류금속(III) 착물들의 합성과 전자적 구조와 전기화학적 거동에 관한 연구 (II))

  • Chil Nam Choe;Se Bong Kim;Nyon Yong Park
    • Journal of the Korean Chemical Society
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    • v.37 no.10
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    • pp.895-902
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    • 1993
  • The chemical behavior of trivalent lanthanide ($Pr^{3+}\;and\;Dy^{3+}$) and organo ligands (phen' and terpy') complexes was investigated by the use of UV/vis-spectrophotometric, magnetization and electrochemical method. The magnitude of crystal field splitting energy, the pairing energy and spin state was obtained from the spectra of complexes. These complexes were founded to be diamagnetics, delocalization and low spin complexes. The electrochemical behavior of complexes was observed by the use of cyclic voltammetry in aprotic media. These reduction peaks were irreversible two step reduction processes by electron transfer.

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Amorphous-to-crystalline phase-change properties of $(Ag_{5.5}In_{6.5}Sb_{59}Te_{29})_{1-x}(Ag)_x$ (x = 0, 0.1, 0.2) thin films ($(Ag_{5.5}In_{6.5}Sb_{59}Te_{29})_{1-x}(Ag)_x$ (x = 0, 0.1, 0.2) 박막의 비정질-결정질 상변화 특성)

  • Seo, Jae-Hee;Kim, Sung-Won;Lee, Hyun-Yong
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.06a
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    • pp.229-230
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    • 2008
  • 본 논문에서는 비정질-결정질간 가역적 상변화 기록 매질로 이용되고 있는 $(Ag_{5.5}In_{6.5}Sb_{59}Te_{29})$ 합금 박막의 Ag 조성 증가에 따른 원자구조와 상변화 특성간의 상관관계를 연구하였다. 실험에 사용된 AgInSbTe 조성은 5N의 금속 파우더를 용융-냉각법으로 벌크를 제작하였고 열증착 방법으로 Si (100) 및 유리(corning glass, 7059) 기판위에 200 nm 두께로 박막을 증착하였다. 비정질 박막의 결정화속도를 평가하기 위해서 658 nm의 LD가 장착된 나노-펄스 스캐너를 이용하여 power; 1~17mW, pulse duration; 10~460 ns의 범위에서 각 조성의 상변화에 따른 반사도 차이를 측정, 비교 분석하였다. 또한 각각의 박막을 $100^{\circ}C$ 에서 $300^{\circ}C$까지 $50^{\circ}C$ 간격으로 $N_2$ 분위기에서 1시간동안 열처리 한 후 XRD와 UV-Vis-NIR spectrophotometer를 사용하여 각 상의 구조분석 및 광학적 특성을 분석하였으며, 4-point probe로 면저항을 측정하였다.

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Preparation of Alum and Poly Aluminum Chloride Using Waste Aluminum Dross (알루미늄 폐드로스를 재활용(再活用)한 Alum과 Poly Aluminum Chloride 제조(製造) 연구(硏究))

  • Park, Hyung-Kyu;Lee, Hoo-In;Choi, Young-Yoon
    • Resources Recycling
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    • v.16 no.5
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    • pp.3-7
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    • 2007
  • Waste aluminum dross was processed to prepare alum with sulfuric acid, and poly aluminum chloride(PAC) with hydrochloric acid. Metallic aluminum remained in the waste dross was dissolved into the sulfuric acid solution, and the solution could be used as alum for water treatment chemicals after adjusting the required alumina concentration and pH of the solution. Also, it was dissolved into the hydrochloric acid solution and processed to make PAC solution. Compared with the conventional method for preparation of alum and PAC using aluminum hydroxide, material cost could be saved in this method. Also, there is an additional merit in view of recycling of the waste aluminum dross by reducing the amount of waste disposed to landfill.

A Simplified Procedure for the Large-Scale Purification of Urokinase from Human Urine (인뇨로부터 유로키나제 대량정제공정의 단순화)

  • 정광회;선우명
    • KSBB Journal
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    • v.5 no.2
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    • pp.183-189
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    • 1990
  • An efficient method has been developed for the purification of urokinase from 1, 000 liter batches of human urine. The procedure involved precipitation of urokinase with 2mM zinc chloride, resuspension of the precipitate with 0.1M EDTA/0.5M Glycine solution, and CM-Toyopearl and benzamidine-Sepharose column chromatography. The purified urokinase was fully active and possessed a specific activity of 1.07$\times$105IU/mg. The recoveries ranged from 42 to 65% in several preparations(mean value was 51%). And the urokinase purified by this process consisted of about 13% of single chain urokinase (pro-urokinase) as evaluated by SDS-polyacrylamide gel electrophoresis in reducing condition and by S-2444 amldolytic activity under plasmin treatment.

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리사이클공장의 초기가동과 시스템 구축 - 리사이클률 향상과 코스트 저감 -

  • KOREA ELECTRIC ASSOCIATION KOREA ELECTRIC ASSOCIATION
    • JOURNAL OF ELECTRICAL WORLD
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    • s.301
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    • pp.68-73
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    • 2002
  • 미쓰비시(삼릉)전기는 1999년 5월치바현 이치가와시 동빈에$''$특정가정용기기재상품화법(통칭 : 가전리사이클법)$''$에 대응하기 위하여 일본국내 최초의 전기제품 리사이클 플랜트를 가동시켰다. 이 플랜트에서는 종합전기메이커로서의 특징을 살려 연소를 수반하지 않는 철저한 머티어리얼 리사이클, 물을 쓰지 않는 완전건식에 의한 소재(素材)의 분리$\cdot$분별(分別)을 실현하였다. 최대의 특징은 수(手)작업에 의한 부분분해와 기계분해(파쇄에 의한 소재분리)를, 리사이클률, 경제성, 환경부하성의 3가지 관점에서 조화를 시키고 있는 점이다. 본고에서는 리사이클 플랜트의 개요를 소개하고 리사이클률 향상과 리사이클 처리비용 저감을 위해 대처해 온 다음의 3개 항목에 대하여 기술한다. (1) 플라스틱찌꺼기(殘材) 리사이클설비의 개발 주파쇄분리(主破碎分離) 프로세스에서 배출되는 금속과 염화비닐을 포함한 플라스틱찌꺼기를 처리하여, 플라스틱을 고로환원재(高爐還元材)로서 유효 활용할 수 있도록 하였다. (2)효율적인 물류(物流)레이아웃 및 수해체방식(手解體方式)의 설계 공장내의 폐제품(廢製品)$\cdot$분별물(分別物)에 대한 보관장소, 반송수단$\cdot$경로를 최적 설계하여 처리비용을 요하는 수해체 작업을 효율적으로 할 수 있도록 업무흐름을 설계하였다. (3)리사이클공장 관리시스템의 구축 공장관리의 효율화와 배출자(排出者)에 대한 리사이클정보가 분명하게 나타날 수 있게 하기 위하여 리사이클공장관리시스템을 개발하여 도입하였다.

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Deformation Behavior of a $Zr_{55}Al_{10}Ni_5Cu_{30}$ Bulk Metallic Glass at High Temperatures (고온에서 $Zr_{55}Al_{10}Ni_5Cu_{30}$ 벌크 유리금속의 변형거동)

  • Jeong, Young-Jin;Kim, Ki-Hyun;Oh, Sang-Yeob;Shin, Hyung-Seop
    • Proceedings of the KSME Conference
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    • 2004.04a
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    • pp.342-347
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    • 2004
  • The deformation behavior of a $Zr_{55}Al_{10}Ni_5Cu_{30}$ bulk metallic glass under tensile loading at different range of strain rates and temperatures between 680 K and 740 K were investigated. The variation in the deformation behavior of $Zr_{55}Al_{10}Ni_5Cu_{30}$ bulk metallic glass which resulted from the crystallization induced during testing was reported. The$Zr_{55}Al_{10}Ni_5Cu_{30}$ bulk metallic glass has showed either homogeneous or inhomogeneous deformation depending on test condition. It exhibited a maximum elongation of about 560 % at the condition of $407^{\circ}C{\times}\;10^{-4}/s$. The flow behavior exhibited three different types and the flow stress became lower at higher temperatures and lower strain rates. The increase of the time elapsed during heating resulted in the partial crystallization of bulk metallic glass phase and eventually strain hardening and brittle fracture.

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