• Title/Summary/Keyword: 글로브박스

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Modification of Hydrogen Determinator for Total Hydrogen Analysis in Irradiated Zircaloy Cladding Tube (수소분석기 개조 및 조사후 지르칼로이 피복관의 총수소분석)

  • Park, Soon-Dal;Choi, Kwang-Soon;Kim, Jong-Goo;Joe, Kih-Soo;Kim, Won-Ho
    • Analytical Science and Technology
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    • v.12 no.6
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    • pp.490-497
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    • 1999
  • A hydrogen determinator was modified and installed in the glove box to analyse total hydrogen content in irradiated zircaloy tube. The analysis method of hydrogen is Inert Gas Fusion(IGF)-Thermal Conductivity Detection(TCD). The hydrogen recoveries of no tin method using Ti and Zr matrix standards, respectively, were available within $3{\mu}g$ of hydrogen. Also the smaller size of sample showed the better hydrogen recovery. It was found that the hydrogen standard of Ti matrix is avaliable to hydrogen analysis in zircaloy sample. The mean radioactivity of irradiated zircaloy sample was 10 mR/hr and hydrogen concentration was 130 ppm.

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Development of Rattle and Squeak Detection Methodology Considering Characteristics of Road Vibration Input (차량 부품의 노면 가진 특성을 고려한 래틀과 스퀵 현상 검출 방법의 개발)

  • Lyu, Su Jung;Jun, In Ki;Choi, Jae Min;Lee, Won Ku;Woo, Jae Chul
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.37 no.5
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    • pp.679-683
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    • 2013
  • BSR noise emerges in a vehicle as a result of road vibrations, engine vibrations, and speaker vibrations. BSR noise occurs with an irregular impact or stick slip friction phenomenon as the influence of the resonance mode when the vibration input load is transferred along poor joint and contacting pairs of the system. A sub-structure method of finite element analysis is required to detect impacts and slip in the full vehicle model. This study presents a method for sub-structure modeling and a rattle and squeak detection methodology that considers the characteristics of road vibration inputs.

Dynamic Property Identification of Structural Systems with Hinge Joint Using Equivalent Stiffness (등가강성모델을 활용한 힌지체결부 동특성 동정)

  • Won, Junho;Lim, Che Kyu;Lee, Doo-Ho;Choi, Joo-Ho
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.36 no.12
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    • pp.1635-1642
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    • 2012
  • The identification of the dynamic properties of structural joints is important for predicting the dynamic behavior of assembled systems. However, the identification of the properties using analytical or experimental approaches is extremely difficult or even impossible. Several studies have proposed hybrid or synthesis methods that simultaneously used analytical and experimental approaches to identify the dynamic properties of a joint. However, among the many types of joints, only the bolt joint was treated as a practical example in these studies. In this study, for a simple assembly system comprising two plates and one hinge joint, a simple methodology involving the use of the static-based subpart analysis method to identify the dynamic properties is proposed. Finally, the proposed method is applied to a glove box in a passenger vehicle that includes hinge joints.

Characteristic Feature of Inductively Coupled Plasma Atomic Emission Spectrometer/Shielding System and Evaluation of Its Applicability to Analysis of Radioactive Materials (유도 결합 플라스마 원자방출분광기/차폐 시스템의 특성 및 방사성 물질 분석에 대한 적용성 평가)

  • Lee, Chang Heon;Suh, Moo Yul;Choi, Kae Chun;Park, Yang Soon;Jee, Kwang Yong;Kim, Won Ho
    • Analytical Science and Technology
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    • v.13 no.4
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    • pp.474-483
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    • 2000
  • An inductively coupled plasma atomic emission spectrometer/shielding system was specially designed and built for the analysis of radioactive materials. Both of an inductively coupled plasma source and a sample transfer system to be contacted with radioactive materials was installed in a stainless steel glove box. In terms of analytical capability and radiation safety, characteristic feature of the system was investigated. Its applicability to the determination of fission products and corrosion products in the radioactive materials such as spent fuel dissolver solution and the primary coolant of nuclear power reactors was evaluated. In the concentration range $0.01-0.1mgL^{-1}$, the relative standard deviation was found to be less than 5%.

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A Study on the Separation of Long-lived Radionuclides and Rare Earth Elements by a Reductive Extraction Process (환원추출에 의한 장수명핵종과 희토류 원소의 분리 연구)

  • 권상운;안병길;김응호;유재형
    • Proceedings of the Korean Radioactive Waste Society Conference
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    • 2003.11a
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    • pp.421-425
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    • 2003
  • The reductive extraction process is an important step to refine the TRU product from the electrorefining process for the preparation of transmutation reactor fuel. In this study, it was studied on the reductive extraction between the eutectic salt and Bi metal phases. The solutes were zirconium and the rare earth elements, where zirconium was used as a surrogate for the transuranic(TRU) elements. All the experiments were performed in a glove box filled with a argon gas. Li-Bi alloy was used as a reducing agent to reduce the high chemical activity of Li. The reductive extraction characteristics were examined using ICP, XRD and EPMA analysis. The reduction reaction was equilibrated within 3 hours after the Li addition. Three eutectic salt systems were compared and Zr was successfully separated from the rare earth elements in all the three salt systems.

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Determination of La in $U_3Si/Al$ Spent Nuclear Fuel by Ion Chromatography-Inductively Coupled Plasma-Mass Spectrometry (Ion Chromatography-Inductively Coupled Plasma-Mass Spectrometry에 의한 $U_3Si/Al$ 사용후핵연료 중 La의 분리 및 정량)

  • Han, Sun Ho;Choi, Kwang Soon;Kim, Jung Suk;Jeon, Young Shin;Park, Yang Soon;Jee, Kwang Yong;Kim, Won Ho
    • Analytical Science and Technology
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    • v.13 no.5
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    • pp.601-607
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    • 2000
  • Lanthanum has been used as one of the burnup monitor in spent nuclear fuel. $U_3Si/Al$ spent nuclear fuel contains small amount of La in high concentration of U and Al. Therefore, chemical separation of La is required to remove matrix elements. At first, ion chromatography (IC) and inductively coupled plasma systems were installed in radiation shielded glove box to handle the radioactive samples. Retention behavior of uranium, aluminum, lanthanum and some interesting fission products (Sr, Zr, Y, Mo, Ru, Pd, Rh, Cs, Ba, Ce, Pr, Nd, Sm, Eu and Cd) was investigated using the CG10 column and ${\alpha}$-HiBA eluent. As all elements were eluted earlier than lanthanum in 0.2 M ${\alpha}$-HiBA eluent, a portion of U and Al was directly passed to waste using a three way valve between the column and the nebulizer. Thus it was possible to determine the lanthanum in a high concentration of U and Al matrix. Retention time of La was about 12 minutes in this separation condition. Optimum range for the determination of La in $U_3Si/Al$ spent nuclear fuel was $1-10{\mu}g/L$ (ppb) with this system and detection limit was $0.25{\mu}g/L$ in case of $200{\mu}L$ of sample volume.

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Changes of the Oxidation/Reduction Potential of Groundwater by the Biogeochemical Activity of Indigenous Bacteria (토착미생물의 생지화학적 활동에 의한 지하수의 산화/환원전위 변화 특성)

  • Lee, Seung Yeop;Roh, Yul;Jeong, Jong Tae
    • Economic and Environmental Geology
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    • v.47 no.1
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    • pp.61-69
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    • 2014
  • As we are trying to in-situ treat (purify or immobilize) heavy metals or radionuclides in groundwater, one of the geochemical factors to be necessarily considered is the value of oxidation/reduction potential (ORP) of the groundwater. A biogeochemical impact on the characteristic ORP change of groundwater taken from the KAERI underground was observed as a function of time by adding electron-donor (lactate), electron-acceptor (sulfate), and indigenous bacteria in a laboratory condition. There was a slight increase of Eh (slow oxidation) of the pure groundwater with time under a $N_2$-filled glove-box. However, most of groundwaters that contained lactate, sulfate or bacteria showed Eh decrease (reduction) characteristics. In particular, when 'Baculatum', a local indigenous sulfate-reducing bacterium, was injected into the KAERI groundwater, it turned to become a highly-reduced one having a decreased Eh to around -500 mV. Although the sulfate-reducing bacterium thus has much greater ability to reduce groundwater than other metal-reducing bacteria, it surely necessitated some dissolved ferrous-sulfate and finally generated sulfide minerals (e.g., mackinawite), which made a prediction for subsequent reactions difficult. As a result, the ORP of groundwater was largely affected even by a slight injection of nutrient without bacteria, indicating that oxidation state, solubility and sorption characteristics of dissolved contaminants, which are affected by the ORP, could be changed and controlled through in-situ biostimulation method.

An Efficient Integration of 3D User Interface Device with Tiled Display System in PC Cluster Environment (3차원 사용자 인터페이스 장비와 PC 클러스터 환경 타일 가시화 시스템의 효율적인 연동)

  • Oh, Min-Hwan;Kim, Kwang-Sik;Choi, Yun-Hyuk;Yang, Jin-Oh;Cho, Jin-Yeon
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.36 no.2
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    • pp.185-194
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    • 2008
  • In this paper, an efficient technique is proposed to integrate the 3D user interface with the tiled display system in PC cluster environment. In the developed 3D user interface software, various menus are provided to increase the user friendliness of the interface, including the several model-control-commands. To eliminate the noise produced from the 3D user interface devices, the box filtering algorithm is employed. Further, a communication splitting algorithm, which is a kind of asynchronous communication method, is proposed to reduce the motion delay between the 3D interface and the tiled display system, and its efficiency is validated through the benchmarking tests.