• Title/Summary/Keyword: 굴곡시험

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Fabrication and Characteristics of CFRC(Carbon Firber Reinforced Carbon Composites) Fabricated with Carbon Fiber and Coal Tar Pitch Matrix (석탄계 핏치를 결합재로한 탄소/탄소 복합재의 제조 및 특징)

  • Ju, Hyeok-Jong;Choe, Don-Muk;O, In-Seok
    • Korean Journal of Materials Research
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    • v.4 no.2
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    • pp.194-205
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    • 1994
  • In this research, we attempt to fabricate an excellent CFRC(Carbon Fiber Reinforced Carbon), which has good thermal and mechanical properties, with 8H/satin woven fabric prepreg, high modulus and high strength type continuous carbon fiber and raw coal tar pitch(RCTP) matrix or THF soluble fraction(THFSP) matrix which has good graphitizability. Green bodies were fabricated with hot press molding technique and CFRC samples were made after carbonization, impregnation, recarbonization and graphitization steps. For the purpose of characterization of the physical properties, SEM, polarized light microscope, TGA were observed, and tested flexural strength, modulus and ILSS. After heat treating the THFSP matrix up to $2300^{\circ}C$, the value of $C_0$/2 was 3.380$\AA$, which is analogous to the structure of natural graphite and the value of 2$\theta$ is $26.276^{\circ}$ approached to the Bragg's angle of natural graphite. As a result of TGA to test the high temperature air oxidation, the THFSP matrix, graphitized up to $2300^{\circ}C$, exhibited the best air oxidation resistance. And mechanical properties were increased up to 65~70% as fiber volume fraction increased. Because of the good orientation graphitizability, the fracture surface of THFSP matrix CFRC is very good.

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Influence of water absorption on flexural strength and elastic modulus in several resinous teeth splinting materials (수분 흡수가 여러 레진계 치아고정 재료의 굴곡강도와 탄성계수에 미치는 영향)

  • Park, Bae-Young;Kim, Soo-Yeon;Kim, Jin-Woo;Park, Se-Hee;Cho, Kyung-Mo
    • Journal of Dental Rehabilitation and Applied Science
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    • v.34 no.2
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    • pp.72-79
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    • 2018
  • Purpose: The purpose of this study was to compare flexural strength and elastic modulus of several splinting materials dependent on water absorption. Materials and Methods: Three different materials; LightFix, G-FIX, G-aenial Universal Flo; were used in this study. Thirty rectangular bar specimens ($25{\times}2{\times}2mm$) of each materials were prepared. Fifteen specimens of each materials were stored in 100% relative humidity atmosphere, $37^{\circ}C$ for 24 hours. The other specimens were stored in distilled water, $37^{\circ}C$ for 30 days. Flexural strength and elastic modulus were calculated using Universal testing machine. One-way ANOVA and Scheffe's post hoc test at 95% level of significance were used on all test results. Results: In LightFix, flexural strength and elastic modulus were significantly decreased after aging. In G-FIX, there was no significant change in flexural strength and elastic modulus after aging. In G-aenial Universal Flo, flexural strength was significantly decreased, but elastic modulus did not change significantly. Statistical analysis reveals that flexural strength and elastic modulus increased in the order of LightFix, G-FIX, G-aenial Flo in both 24 hours and 30 days. Conclusion: It could be deduced from this study that flexural strength and elastic modulus of some resins could be changed when it aged in oral environment. Thus this should be considered when choosing a resin to perform a resin-bonded splint.

Effects of the color components of light-cured composite resin before and after polymerization on degree of conversion and flexural strength (광중합형 복합레진의 중합 전, 후의 색 성분이 중합률과 굴곡강도에 미치는 영향)

  • Yoo, Ji-A;Cho, Byeong-Hoon
    • Restorative Dentistry and Endodontics
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    • v.36 no.4
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    • pp.324-335
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    • 2011
  • Objectives: This study investigated the effects of the color components of light-cured composite resin before and after polymerization on degree of conversion (DC) and biaxial flexural strength (FS). Materials and Methods: Four enamel shades (A1, A2, A3, A4) and two dentin shades (A2O, A3O) of Premisa (Kerr Co.) and Denfil (Vericom Co.) were evaluated on their CIE $L^*,\;a^*,\;b^*$ color components using the spectrophotometer before curing, after curing and at 7 day. The DC of same specimens were measured with Near-infrared spectrometer (Nexus, Thermo Nicolet Co.) at 2 hr after cure and at 7 day. Finally, the FS was obtained after all the other measurements were completed at 7 day. The correlations between each color component and DC and FS were evaluated. Results: The light-curing of composite resin resulted in color changes of Premisa in red-blue direction and Denfil in green-blue direction. The DC and FS were affected by product, time and shade (3-way ANOVA, p < 0.05) and product and shade (2-way ANOVA, p < 0.05), respectively. Premisa only showed a significant correlation between the DC and CIE $a^*$ component - before and after polymerization (Pearson product moment correlation, p < 0.05). The FS of Premisa showed significant negative correlations with CIE $a^*$ and CIE $b^*$ components. Conclusions: The DC and FS of the light-curing composite resin were affected by the color components of the material before and after polymerization.

The effects of the number of times dipped in coloring liquid and final sintering temperature on flexural strength of zirconia ceramics: Zirconia ceramics having improved transparency (착색액 침지 횟수와 최종 소결 온도가 지르코니아 세라믹의 굴곡강도에 미치는 영향)

  • Kong, Moon-Chun;Kim, Kap-Jin;Kown, Tae-Yub;Hong, Min-Ho
    • Korean Journal of Dental Materials
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    • v.44 no.2
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    • pp.171-178
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    • 2017
  • The purpose of this study is to investigate the effect of number of times dipped in coloring liquid and sintering temperature on the flexural strength of zirconia ceramic. In this study, using a zirconia block having improved transparency, specimens with size of $25mm{\times}2mm{\times}1.5mm$ were fabricated. The zirconia ceramic specimens were divided into three groups according to the number of times dipped in coloring liquid by 0, 2 and 4 times, and dyed in the coloring liquid to give color to each specimen. Then, after sintering them at the final temperature of $1,450^{\circ}C$ and $1,600^{\circ}C$, flexural strength was measured using a universal testing machine (total 6 group, n=10 for each group). Also, a scanning electron microscopy (SEM) was performed to observe its microstructure, and the data obtained through the experiment were analyzed with two-way ANOVA. The results of the flexural strength analysis show that the highest value was measured $762.3{\pm}42.3MPa$ in EKL2 group, while the lowest value was $516.4{\pm}77.1MPa$ in EKH4 group. According to the results of the two-way ANOVAs, flexural strength was not related with interaction between sintering temperature and number of times dipped in coloring liquid ($R^2=0.737$). However, there were statistically significant differences in flexural strength depending on sintering temperature (P<0.001). The flexural strength of zirconia ceramics having improved transparency was dependent on sintering temperature. The number of times dipped in the coloring liquid did not affect flexural strength of the zirconia ceramic having improved transparency.

A Study on Logicality for the Periodic Replacements of Continuous Welded Rail based on Accumulated Passing Tonnage (누적통과톤수에 의한 레일교체기준의 타당성 분석)

  • Sung, Deok-Yong;Kong, Sun-Yong;Kim, Park-Jin;Shin, Hyo-Jung;Park, Yong-Gul
    • Proceedings of the KSR Conference
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    • 2007.11a
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    • pp.1058-1070
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    • 2007
  • Internal and external railway management corporations are using the periodic replacement criteria of rail by accumulated passing tonnage and wear to maintain rails for servicing. However, internal the periodic replacement criteria of continuous welded rail(CWR) by accumulated passing tonnage is the one(50kg/m-5 million gross tonnage, 60kg/m-6 million gross tonnage) presented in Japan before. It was estimated with the fatigue life about 50kg N rail joints applied diesel train load but it wasn't applied to current conditions of track; elimination of rail joint, using the concrete slab track and operation of light train load and effect of welding, manufacturing technique, grinding of rail. Therefore, in this study, it was investigated the types of damage and cause in welded rails and examined standards and information resources. Also, this study presents preliminary data to revise the periodic replacement criteria of CWR by current accumulated passing tonnage in bending test of laid welded rail and a survey of track maintenance history of Seoul metro.

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Design of Insulation and Bending Test for a 154 kV Class HTS Cable (154 kV급 HTS 케이블의 절연설계 및 굴곡시험)

  • Choi, Jin-Wook;Choi, Jae-Hyeong;Lim, Eung-Choon;Kim, Hae-Jong;Cho, Jeon-Wook;Kim, Sang-Hyun
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.21 no.11
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    • pp.1024-1028
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    • 2008
  • It is important that study on cryogenic electrical insulation design to develop the cold dielectric(CD) type HTS cable because the cable is operated under the high voltage environment in cryogenic temperature. This paper proposes two types of insulation design to carry out the maximum insulation design for 154 kV-class HT cable. The proposed insulation design method takes into consideration AC and lightning impulse withstand voltage so as to prevent AC breakdown for power frequency operating voltage during operating the cable and breakdown for lightning impulse voltage. The final insulation thickness is determined by selecting high value out of two insulation thickness calculated through the two insulation design methods. And we researched electrical insulation characteristics of HTS cable according to bending ratio and the number of bending.

An Experimental Study on Load Bearing Capacity of Lattice Girder as a Steel Support in Tunnelling (터널 지보재로서 격자지보의 하중지지력에 관한 실험적 연구)

  • 유충식;배규진
    • Geotechnical Engineering
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    • v.13 no.4
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    • pp.163-176
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    • 1997
  • It has long been recognized that the H-beam steel rib has many shortcomings when used as a steel support in tunneling. One of the major shortcomings is the shotcrete shadow created behind H-beam flange which eventually reduces the load bearing capacity of shotcrete shell. In many European countries, plate girder as the H-beam steel rib has been replaced by lattice girder which has many advantages over the H-beam steel rib. Successful application of the lattice girder as a steel support requires a thorough investigation on the load bearing capacity of the lattice girder. Therefore, laboratory bending and compression tests were conducted on lattice girders with the aim of investigating the load bearing capacity of the lattice girders. The results of tests show that the load bearing capacity of laIn twice girders is higher than that of H-beams, which indicates that the lattice girder can be effectively used as a support in tunneling.

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Effects of Wood Flour Size on the Physical Properties of Polypropylene/Wood Flour Composites (목분의 크기가 폴리프로필렌/목분 복합재료의 물성에 미치는 영향)

  • Seo, Yong Won;Kim, Dae Su
    • Polymer(Korea)
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    • v.38 no.3
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    • pp.327-332
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    • 2014
  • Polymer/wood flour composites are recently attracting a lot of interest because they are economic and ecofriendly. In this study, the effects of wood flour size on the thermal and mechanical properties of a polypropylene/wood flour composite were investigated. Mechanical properties of the composite samples prepared by melt-mixing and compression molding were tested by UTM and an izod impact tester, and thermal properties of them were measured by TGA, DMA, DSC and TMA. The best coupling agent was selected by testing three kinds of maleic anhydride modified polypropylene coupling agents, and under the same condition, the effects of wood flour size on the physical properties of the composite were investigated. According to the test results for four different wood flour sizes of 600, 250, 180 and $150{\mu}m$, flexural strength, flexural modulus, crystallinity and water-resistivity of the composite increased with decreasing wood flour size.

The Influence of Mechanical Properties with the Number of Recycling of Fiber-reinforced Thermoplastic Composites Damaged by Impact (충격에 의해 손상된 섬유강화 열가소성 수지 복합재료의 재활용 횟수에 따른 물성의 변화)

  • Bae, Kwak Jin;Lee, Joon Seok
    • Composites Research
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    • v.35 no.2
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    • pp.75-79
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    • 2022
  • In this study, the effect of mechanical and chemical properties of glass fiber reinforced thermoplastic (GFRTPs) according to the number of recycling was confirmed. The composite materials were manufactured through a hot press compression molding process using an E-glass chopped strand mat and a polypropylene film. Four specimens were named according to the number of recycled test repeat: First manufacture, 1st Recycle, 2nd Recycle, and 3rd Recycle. To investigate the mechanical properties of the prepared specimen, tensile test, flexural test, drop-weight impact test, differential scanning calorimetry (DSC), and field emission electron gun-scanning electron microscope (FE-SEM) was performed. As a result, as the number of recycling steps repeat, the degree of crystallization, tensile strength, elastic modulus, and flexural strength were increased, but the impact properties were greatly reduced.

A Study on the mechanical properties of electroless NiP film as a function of nickel salt (니켈염 종류에 따른 무전해 니켈 도금피막의 기계적 특성 연구)

  • ;Lee, Hong-Gi;Lee, Min-Hyeong;Lee, Ho-Nyeon;Heo, Jin-Yeong
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2011.05a
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    • pp.151-152
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    • 2011
  • 본 연구에서는 황산니켈, 아세트산니켈, 썰파민산니켈 등 니켈 염 종류에 따른 무전해 니켈 도금피막의 기계적 특성을 평가하고자 하였다. 동일한 두께로 도금피막을 형성하여 내절성 시험결과 황산니켈을 사용한 무전해 니켈 도금피막의 경우 97회, 아세트산니켈을 사용한 경우 259회, 썰파민산 니켈을 사용한 경우 467회의 굴곡 시험 후 도금 피막이 파괴되어 썰파민산니켈이 니켈염으로 사용될 경우 가장 우수한 피막을 나타내었다. 도금피막의 연신울 측정결과 니켈염으로 황산니켈을 사용할 경우 0.28%의 연신율을 나타내었고 아세트산니켈을 사용할 경우 0.32%의 연신율을 나타내었고 썰파민산니켈을 니켈염으로 사용한 결과 0.69%의 높은 연신율을 나타내었으며 개발한 도금액을 PCB 도금을 위한 Cu Pattern에 도금한 경우 Cu line에 선택적으로 도금이 가능하였다.

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