• Title/Summary/Keyword: 광 산란법

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Evaluation of Molecular Structural Changes in Starch Depending on Amylose Content Using Dynamic Light Scattering (동적광산란법을 이용한 아밀로즈 함량에 따른 전분 분자 구조 변화 분석)

  • Moon, Ju-Hyeon;Ma, Jin-Gyeong;Kim, Jong-Yea
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.46 no.5
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    • pp.653-658
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    • 2017
  • To evaluate the effects of amylose content and dissolution media on the molecular structure of maize starch, changes in the hydrodynamic diameter of starch molecules were assessed via dynamic light scattering depending on amylose content and dissolution media. As the amylose content of starch increased, the hydrodynamic diameter of starch molecules proportionally decreased from 204 to 92 nm. To alter ionic strength, hydrogen bonding, or polarity of dissolution media, various contents of NaCl (1, 2, or 3 M), urea (1, 2, or 3 M), or 1-butanol (0.1, 0.5, or 1.0%) were added to media, respectively, resulting in increased hydrodynamic diameter of starch. However, the degree of expansion was dependent on amylose content and the concentration and/or type of additive. The hydrodynamic diameter of starch molecules exhibited significant correlation with amylose content obtained by size exclusion chromatography, regardless of dissolution conditions.

연소현상의 가시화

  • 정석호
    • 한국가시화정보학회:학술대회논문집
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    • 2005.04a
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    • pp.61-83
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    • 2005
  • 연소현상의 가시화를 위한 몇 가지 레이저 진단기법의 응용 예를 소개한다. 이에는 유동 가시화를 위한 반응성 Mie 산란, 주화학종의 계측을 위한 Rayleigh 및 Raman 산란, 미소화학종 계측을 위한 레이저유도 형광법, 온도계측을 위한coherent anti-Stokes Raman 산란법 및 매연계측을 위한 광 소멸/산란법 등이 포함된다. 이러한 기법들이 확산화염, 층류 및 난류 부상 화염, 비예혼합 와도 내의 화염전파, 매연생성 등의 연구에 적용되어 물리적 메커니즘을 이해하는데 유용하게 적용된 사례를 보고한다.

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Measurments of 2-D Image Soot Distribution in Late Combustion Stage Using Elastic Scattering, Laser-Induced Incandescence and Flame Luminosity (레이저 탄성산란법, 여기적열법, 자발광을 이용한 가시화 디젤엔진의 후기연소의 2차원 soot 분포 측정)

  • Noh, S.M.;Won, Y.H.;Park, J.G.;Choi, I.Y.;Chun, K.M.
    • Proceedings of the KSME Conference
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    • 2000.11b
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    • pp.162-167
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    • 2000
  • Soot formation and oxidation is closely related to the combustion phenomena inside a diesel engine. Laser-based diagnostics provide a means for improving our understanding of diesel combustion, because they have highly temporal and spatial ability. To understand the soot behavior we did preliminary study by taking flame luminosity photographs and 2-D imaging soot distribution using Laser Elastic Scattering(LIS) and Laser-Induced Incandescence(LII). From the data we found that soot concentration was high in the bowl and disappeared from the central region in the late combustion stage.

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Measurments of 2-D Image Soot Distribution for Different Piston-Shapes of a DI Diesel Engine Using Elastic Scattering, Laser-Induced Incandescence and Flame Luminosity (레이저 탄성산란법, 여기적열법, 자발광을 이용한 직분식 디젤엔진의 피스톤 형상에 따른 2차원 soot 분포 측정)

  • Noh, S.M.;Won, Y.H.;Park, J.G.;Choi, I.Y.;Chun, K.M.
    • 한국연소학회:학술대회논문집
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    • 2000.12a
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    • pp.183-193
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    • 2000
  • Soot formation and oxidation is closely related to the combustion phenomena inside a diesel engine. Laser-based diagnostics provide a means for improving our understanding of diesel combustion, because they have highly temporal and spatial ability. To understand the soot behavior we did preliminary study by taking flame luminosity photographs and 2-D images of soot distribution using Laser Elastic Scattering(LIS) and Laser-Induced Incandescence(LII). From the data we found that soot concentration was high in the bowl and disappeared from the central region in the late combustion stage and that soot exists in the flame using luminosity, LIS and LII.

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Study on Stability of Ceramides in Liquid Crystalline Emulsions at High Temperature (세라마이드의 액정에멀젼 내 고온 제형 안정성 연구)

  • Hong, Sung Yun;Chang, Yujin;Lee, Jun Bae;Park, Chun Ho;Park, Myung Sam
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.45 no.1
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    • pp.1-7
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    • 2019
  • We introduce to prepare liquid crystalline emulsion composed of cetearyl alcohol, cetyl palmitate, sorbitan palmitate, sorbitan olivate, ceramide and so on which can enforce interface between oil-based particle and water phase. In terms of structural analysis, the stability of the liquid crystalline emulsion including ceramide, which is immisible ingredient, at high temperature was proved by polarized microscope, cryo-SEM, small-angle x-ray scattering, in addition to viscometer and static light scattering by physical analysis.

Soot Measurement in an Optically Accessible Diesel Engine Using Laser Sheet (2nd reprot: The Measurement for diameter and number density of Soot) (레이저시트광을 이용한 가시화 디젤엔진에서의 Soot 계측(제2보 : Soot 입경분포 및 수밀도 계측))

  • 이명준;박태기;하종률;정성식
    • Transactions of the Korean Society of Automotive Engineers
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    • v.8 no.3
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    • pp.37-45
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    • 2000
  • The technique of laser sheet beam has been applied to optically accessible diesel engine for the quantitative measurement of soot. The results provide the information for us for reduction of soot in diesel engine. We used both LIS nad LII techniques simultaneously in this study. LIS and LII images show the quantitative distribution of the soot concentration in an optically accessible diesel engine. In this study, several results were obtained by the simultaneous measurement of LIS and LII technique. The diameter and number density of soot in combustion chamber of the test engine were obtained from ATDC 20$^{\circ}$ to 110$^{\circ}$ . The increase rate of soot diameter was about 40$^{\circ}$ between ATDC 20$^{\circ}$and 110$^{\circ}$. And the number density of soot decreased significantly between ATDC 20$^{\circ}$and 40$^{\circ}$.

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Pre-Charged Particle Deposition in an Impactor subjected to an Electric Field (전기장이 형성된 관성 충돌기에서 대전 입자의 거동과 부착 특성에 대한 연구)

  • Park, Hyung-Ho;Kim, Sang-Soo
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.23 no.3
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    • pp.299-310
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    • 1999
  • Effect of electrostatic and inertial forces on the pre-charged particle deposition was theoretically and experimentally studied by introducing the inertia impactor subjected to an electric field. To derive the analytic solution, we assumed that a flow was an ideal stagnation flow, a particle had saturation charges, and the electric field within the test section was uniform. On the other hand, $Al_2O_3$ particle groups were used as the test particles, which mean sizes were $1{\mu}m$, $3{\mu}m$, and $5{\mu}m$. To measure the deposition efficiency, the light scattering method was used. The results showed that the deposition efficiency was minimized at a certain nozzle velocity as increasing the nozzle velocity, only if the electric force was applied. As the electric field strength increased, $Stk_{50}{^{1/2}}$ was decreased, and its decreasing rate was reduced with increasing the flow velocity. Moreover the existence of electric field was against the cut-off performance of the inertia impactor.

The Measurement of the Temperature Variation in a Constant Volume Combustion Chamber by the Laser Rayleigh Scattering (레이저 레일레이 산란법에 의한 定積燃燒室內의 溫度變動에 대한 計測)

  • ;;苦井和憲;志水昭史
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.15 no.1
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    • pp.328-340
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    • 1991
  • The combustion process in the combustion chamber has been investigated by taking pressure, temperature, chemical equilibrium and the shape of flame. To predict temperature of a flame in a combustion chamber is one of very important problems in the field of combustion and the temperature is a important factor of ignition and counteraction to inflammation. In this paper, the flame temperature was determined by the method of the Rayleigh scattering of Ar-Ion Laser (514.5nm). The Rayleigh scattering has been got considerably attention because of its strong cattering intensity. As a result, it is shown that I can measure the shape of flame by schlieren photography and that I can get the flame temperature variation in constant volume combustion chamber by Laser Rayleigh Scattering.

Soot Measurement in an Optically Accessible Diesel Engine Using Laser Sheet 1st report : The Development of Optically Accessible Diesel Engine and Photography of 2D Soot Images Using Laser Sheet (레이저시트광을 이용한 가시화 디젤엔진에서의 Soot 계측 제1보 : 가시화 디젤엔진의 제작 및 레이저를 이용한 Soot의 2D 화상촬영)

  • 이명준;박태기;하종률;정성식
    • Transactions of the Korean Society of Automotive Engineers
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    • v.8 no.2
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    • pp.64-71
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    • 2000
  • In order to clarify the characteristics of soot formation and oxidation in-cylinder of a diesel engine, it is necessary to diagnose accurately for combustion of in-cylinder. The past techniques for soot measurement have limitations in providing the characteristics of soot in a diesel engine, whereas, laser-based 2D imaging diagnostics have the potential to provide better temporally and spatially resolved measurements of the soot distribution. We rebuilt an optically accessible diesel engine which is similar to the conditions of a conventional engine and tried to measure soot distribution in a cylinder of the diesel engine using laser induced scattering(LIS) and laser induced incandescence(LII). Some results were acquired in this study. LIS and LII signal that show soot distribution of a in-cylinder were taken by ICCD properly. The signal of LIS was intenser than that of LII. Although they have some differences of signal intensity in early combusion period, both of signals show that they are generally similar in late combustion period, after ATDC 50 degree.

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Preparation and Gas Permeation Properties of Silica Membranes on Porous Stainless Steel-Tube Supports (다공성 금속 지지체에 제조된 실리카 분리막의 기체 투과 특성)

  • Lee, Hye Ryeon;Seo, Bongkuk
    • Membrane Journal
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    • v.24 no.3
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    • pp.177-184
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    • 2014
  • Silica membranes with high permeability were prepared using colloidal and polymeric silica sols on a porous stainless steel-tube support by a DRFF and SRFF method. Silica sols were derived with tetraethylorthosilicate (TEOS) by sol-gel method and analyzed with DLS, FE-SEM, and $N_2$ adsorption. The coating of the intermediate layer with colloidal silica sol on the stainless steel-tube support led to a denser surface morphology of the membrane along with a considerable reduction in the number of surface defect. As the polymeric silica sol enclosed the colloidal silica sol with spherical particles during the SRFF method, the separation-layer-coated silica membrane showed a denser surface than the intermediate layer. Moreover, the silica membranes showed high hydrogen gas permeability of $(6.63-9.21){\times}10^{-5}mol{\cdot}m^{-2}{\cdot}s^{-1}{\cdot}Pa^{-1}$ with low $H_2/N_2$ perm-selectivity (2.9-3.1) at room temperatures.