• Tribology and Lubricants
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• v.14 no.3
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• pp.17-23
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• 1998

Friction materials with three different formulations containing different solid lubricants were investigated to study the role of lubricants on the friction performance. The three friction materials contained graphite 10 vol.%, graphite 7 vol.%+$MoS_2$ 3 vol.%, and graphite 7 vol.%+$Sb_2S_3$ 3 vol.%, respectively, with the same amount of other ingredients. Results of this work showed that each formulation with different lubricants had unique advantages and disadvantages. The friction materials containing graphite 7 vol.%+$MoS_2$ 3 vol.% and graphite 7 vol.%+$Sb_2S_3$ 3 vol.% showed better resistance to fading and improved friction stability compared to the friction materials containing graphite only as a lubricant. However, the friction materials with two lubricants (graphite+$MoS_2$ or $Sb_2S_3$) showed disadvantages on DTV generation and rotor wear.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2009.05a
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• pp.205-207
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• 2009

아크이온플래이팅 기술과 스퍼터링 기술이 결합된 하이브리드 코팅 시스템을 이용하여 STS 304와 Si 기판에 4성분계 Cr-Al-Mo-N 코팅을 증착하였다. $N_2$/Ar 혼합가스 분위기하에 아크 타겟은 Cr을 사용하였고 스퍼터링 타겟은 Al과 Mo를 사용하였으며 합성된 Cr-Al-Mo-N 코팅은 주로 치환고용된 (Cr, Al, Mo)N으로 구성되었다. 최고 경도값은 Mo 함량이 24.2 at.%일 때 35 GPa을 나타냈으며 마찰계수는 Mo의 함량이 0에서 33.2 at.%로 증가함에 따라 0.9에서 0.48로 감소하였다. 이는 $MoO_3$가 코팅면과 스틸볼 계면에서 고체 윤활제로 작용한 것으로 사료된다. 그러나 Cr-Al-Mo-N 코팅은 MoN의 낮은 내산화온도로 인하여 Cr-Al-N에 비하여 더 낮은 온도에서 산화되었다.

• Journal of the KSME
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• v.19 no.3
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• pp.164-168
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• 1979

이상에서 논술한 바와 같이 금속절삭에 있어서는 절삭공구는 열의 와중의 격열한 상태하에서 작동이 이루어져야 하기 때문에 절삭유제를 분사함으로써 냉각작용으로 경도저하를 방지하고, 균체작용을 시킴으로써 열의 발생을 적게 하며 동력 소비를 감소함과 동시에 절삭면의 정밀도를 향상시킨다. 또한 절삭유제에 극압첨가제를 첨가함으로써 고체윤활을 생성케하여 용찰을 방지 하는 효과를 얻고 있다. 이 외에도 절살유제는 칩의 세척작용, 공작물과 기계의 방작용등의 효 과를 얻고 있다. 요는 절삭가공에서 절삭유제의 사용은 절삭공구의 수명을 연장하고 생산능률을 올리는 효과를 기대하는 것이라고 요약할 수 있다. 여기서 부차적으로 고려해야할 것은 절삭유 제의 토방법도 중요하다. 동일한 조건하에서는 토방법에 따라 효과가 다르다. 가장 효과적인 토 법은 공구의 앞여유면쪽으로 분사하는 것이 가장 좋으며, 칩 위에 분사하는 것이 가장 비효과 적이다. 이와 같은 절삭유제 작용과 효능을 알고 실제가공에 있어서 다소라도 도움이 되었으면 다행으로 생각하는 마음 간절하면서 끝맺는 바이다.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2014.11a
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• pp.200-201
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• 2014

다이아몬드 마이크로 블레이드의 절삭 효율을 향상시키고 절삭 과정에서의 블레이드 측면 경질 박막이 절삭 성능에 미치는 영향을 연구하기 위해 Cu/Sn 금속 결합재에 $MoS_2$와 $WS_2$ 고체 윤활제를 각각 동일 분율 첨가한 후 PAPVD법으로 DLC 박막을 블레이드의 측면에 증착하였다. 실착 절삭 시험을 위해 마이크로 블레이드 시편을 제조하여 충분한 드레싱 과정 후 절삭 시험을 행하였으며 절삭 중 순간 소모 전력과 블레이드의 마모량을 비교 평가하였다. DLC 코팅은 절삭 중 측면에 안정적으로 존재하며 측면 지립의 돌출을 억제하고 마찰을 감소시켜 절삭 효율이 향상되었으며 결과적으로 수명이 증가하였다.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2015.05a
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• pp.145-146
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• 2015

초미세 가공 및 치수안정성 향상을 위한 다이아몬드 마이크로 블레이드의 DLC 코팅이 연삭 과정에서 결합구조가 안정적으로 유지되는지 알아보기 위해 Cu/Sn 금속 결합재에 $MoS_2$ 고체 윤활제를 첨가한 후 PAPVD법으로 DLC 박막을 블레이드의 측면에 증착하였다. 실착 절삭 시험을 위해 마이크로 블레이드 시편을 제조하여 충분한 드레싱 과정 후 절삭 시험을 행하였으며 라만 분광법을 통해 절삭 전후 DLC 코팅에 존재하는 $sp^2$, $sp^3$ 결합의 분율을 조사하고 그 결과를 토대로 DLC 코팅의 특성의 변화를 분석하였다. DLC 코팅에 존재하는 D밴드와 G밴드의 비인 ID/IG는 절삭 후 증가하는 경향을 보였으며 결과적으로 절삭 과정 중 흑연화가 진행되었음을 확인하였다.

• Tribology and Lubricants
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• v.16 no.3
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• pp.173-181
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• 2000

Friction, wear and corrosion characteristics of various MoS$_2$ bonded film lubricants were investigated to apply them to automotive wheel joints. MoS$_2$ bonded film lubricants were formulated by combinations of several additives and binders, and they were coated onto the pre-treated surfaces of specimens. Friction and wear characteristics were evaluated with Falex pin & vee-block test and LFW-1 block-on-ring test. For the corrosion resistant characteristics of the films, salt solution spray corrosion tests were performed. Results showed that MoS$_2$ bonded films containing both inorganic and organic corrosion-resistant additives yielded a synergy effect on anti-corrosion resistance. Also, binders having the better water-proof and thermal stability showed the lower friction and higher corrosion resistance.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.37 no.11
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• pp.1349-1354
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• 2013

Sealing structure to prevent flowing hot gas into the driving device, located between the driving shaft and the liner of On-Off valve for controlling the hot gas flow path was studied. Wear occurs due to the constant movement of the driving shaft controlled by actuator on graphite as the sealing material. In this paper, the dynamic wear behavior in high temperature of graphite(HK-6) to be used as sealing material was evaluated. Reciprocating wear test was carried out for the graphite(HK-6) to the relative motion between shaft materials(W-25Re). The results of friction coefficient and specific wear rate according to contact load, sliding speed at room temperature and $485^{\circ}C$ considering the actual operating environment were evaluated. Through the SEM analysis of the worn surface, third body as lubricant films were observed and lubricant effect of third body was considered.

• Tribology and Lubricants
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• v.19 no.4
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• pp.203-210
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• 2003

In order to enhance the thermal stability of binder materials of bonded type solid lubricants, several metal-alkoxide based sol-gel materials such as methyltrimethoxysilane(MTMOS), titaniumisopropoxide (Ti(Opr$\^$i/)$_4$), zirconiumisopropoxide (Zr(Opr$\^$i/)$_4$) and aluminumbutoxide (Al(Obu$\^$t/)$_4$) were modified chemically by both epoxy and acrylic silane compounds. Friction and wear characteristics of the bonded solid lubricants, whose binders were of several hybrid ceramic materials, were tested with a reciprocating tribo-tester. Wear life was evaluated with respect to the heat-curing temperature, friction temperature, type of supplement lubricants, and ratio of binder materials. Test results showed that the Si-Zr hybrid ceramic materials modified by epoxy-silane compounds had a higher wear life compared to others. Sb$_2$O$_3$ was the most effective supplement lubricants in the high temperature, and BUS analyses revealed that it was caused mainly by a strong anti-oxidation effect to MoS$_2$ particles. The higher heat-curing temperature resulted in the higher wear life, and the higher friction temperature resulted in the lower wear life.

• Transactions of Materials Processing
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• v.15 no.6 s.87
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• pp.453-458
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• 2006

While the die casting has been mainly used to manufacture the magnesium alloy parts, the press forming is considered as an alternative to the die casting for saving the manufacturing cost and improving the structural strength of the magnesium alloy parts. Because the magnesium alloy has low formability at room temperature, forming at elevated temperatures is a necessary condition to obtain the required material flow for press forming. However, the elevated temperature forming does not always guarantee the sufficient formability under the dry friction condition because the surface damage such as scratch or wear may accelerate the material failure. In the present study, the solid-type lubricants such as PTFE, graphite and $MoS_2$ were tested for the square cup warm deep drawing using the magnesium alloy AZ31 sheet. The formability improvement by using the lubricant was examined by comparing the maximum deep drawing depth using the PTFE against no lubricant. The formability difference for the different lubricant was also examined based on the maximum deep drawing depth.

• Tribology and Lubricants
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• v.13 no.1
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• pp.34-41
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• 1997

Frictional behavior of three automotive friction materials (brake pads) containing different amounts of antimony trisulfide ($Sb_2S_3$) and zirconium silicate ($ZRSiO_4$) were investigated using a front brake system. The friction materials were tested on a brake dynamometer (dyno) with gray cast iron rotors. The dynamometer(dyno) test simulated the dragging of a ehicle maintaining 70 km/h and vehicle stops from 100 km/h using 20 different combinations of initial brake temperature (IBT) and input pressure (IP). The results showed a strong influence of the relative amount of $Sb_2S_3$ and $ZrSiO_4$ in friction materials on friction characteristics. Friction stability was improved with the higher concentration of $Sb_2S_3$ in the friction material. Torque variation during drag cycle was increased with an increase of the $ZrSiO_4$ concentration in the friction material. Average friction coefficient and the wear rate of the friction material increased by using more aggressive friction materials containing more $ZrSiO_4$ and less $Sb_2S_3$. Generation of the disk thickness variation (DTV) increased when friction materials with higher concentration of $ZrSiO_4$ were used Careful examination of DTV change showed that aggressiveness of the friction material played an important role in determining torque variation.