• Title/Summary/Keyword: 고온충격

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Estimation of Fracture Toughness Degradation of High Temperature Materials by Nonlinear Acoustic Effects (비선형 음향효과에 의한 고온 재료의 파괴인성 열화도 평가)

  • Jeong, Hyun-Jo;Nahm, Seung-Hoon;Jhang, Kyung-Young;Nam, Young-Hyun
    • Journal of the Korean Society for Nondestructive Testing
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    • v.20 no.5
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    • pp.424-430
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    • 2000
  • In order to develop an ultrasonic evaluation method for properties degradation of high temperature materials, a number of Cr-Mo-V steel samples were heat-treated and their damage mechanism was examined. Ultrasonic parameters such as velocity, attenuation, and more recently developed nonlinear acoustic parameter were measured. The nonlinear acoustic parameter was found to be most sensitive to material degradation mainly attributed to the precipitation of impurities in grain boundaries. When compared to the electrical resistivity results, the nonlinear parameters showed similar behavior. There existed a relatively good correlation between the nonlinear parameter and the fracture appearance transition temperature (FATT) obtained by Charpy V-notch impact test. Based on the relationship between the FATT and the fracture toughness ($K_{IC}$), correlation between the nonlinear parameter and $K_{IC}$ was established.

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Synthesis and thermotolerance of heat shock proteins in campylobacter jejuni (Campylobacter jejuni에서 고온충격 단백질의 합성과 내열성)

  • 김치경;김현옥;이길재
    • Korean Journal of Microbiology
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    • v.29 no.1
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    • pp.49-55
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    • 1991
  • The heat shock responses of Campylobacter jejuni were studied by examination of their survival rates and synthesis of heat shocd proteins. When C. jejuni cells were treated at the sublethal temperatures of 48.deg.C for 30 minutes, most of the cells maintained their viabilities and synthesized the heat shock proteins of 90, 73, and 66 kD in molecular weight. By the method of two-dimensional electrophoresis, the heat shock proteins of C. jejuni were identified to be Hsp90, Hsp73, and Hsp66. During the heat shock at 48.deg.C, the heat shock proteins were induced from about 5 minutes after the heat shock treatment. Their synthesis was continued upto 30 minutes, but remarkably retarded after 50 minutes. When C. jejune cells were heat shocked at 51.deg.C for 30 minutes, the survival rates of the cells were decreased by about $10^{3}$ fold and synthesis of heat shock proteins and normal proteins was also generally retarded. The cells exposed to 55.deg.C for 30 minutes died off by more than $10^{5}$ cells and the new protein synthesis was not observed. But when C. jejuni cells were heat-shocked at the sublethal temperature of 48.deg.C for 15 to 20 minutes and then were exposed at the lethal temperature of 55.deg.C for 30 minutes, their viabilities were higher than those exposed at 55.deg.C for 30 minutes without pre-heat shock at 48.deg.C. Therefore, the heat shock proteins synthesized at the sublethal temperature of 48.deg.C in C. jejuni were thought to be responsible for thermotolerance. However, when C. jejuni cells heat-shocked at various ranges of sublethal and lethal temperatures were placed back to the optimum temperature of 42.deg.C, the multiplication patterns of the cells pretreated at different temperatures were not much different each other.

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Study on Anti-oxidization Coating for Staged Combustion Cycle Rocket Engine (다단연소 사이클 엔진 적용을 위한 내산화 코팅에 관한 연구)

  • Kim, Young-June;Byon, Eung-Sun;Rhee, Byong-ho;Han, Yeoung-Min;Noh, Yong-Oh;Bae, Byung-Hyun;Hyun, Seong-Yoon;Cho, Hwang-Rae;Bang, Jeong-Suk
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2017.05a
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    • pp.864-870
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    • 2017
  • The propellants are burned in the pre-burner of the staged combustion cycle engine, and the resulting hot gas drives the turbine, and the turbine operates the turbo pump. The burned gas passing through the turbo pump is supplied to the combustor at high temperature and high pressure, where the gas is supplied in an excess of fuel or an excess of oxidant depending on the amount of fuel or oxidant. When the cycle works at oxidizer-rich staged combustion, its metal pipe can ignite or explode by the impact of even small particles. In this study, we develop the powder combinations for anti-oxidation coating through the analysis of other coating materials and establish the coating process.

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A Study on Anti-oxidization Coating for Staged Combustion Cycle Rocket Engines (다단연소 사이클 엔진 적용을 위한 내산화 코팅에 관한 연구)

  • Kim, Young-June;Rhee, Byong-ho;Noh, Yong-Oh;Bae, Byung-Hyun;Hyun, Seong-Yoon;Cho, Hwang-Rae;Bang, Jeong-Suk;Byon, Eung-Sun;Han, Yeoung-Min
    • Journal of the Korean Society of Propulsion Engineers
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    • v.22 no.5
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    • pp.125-131
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    • 2018
  • Some propellants in a liquid rocket engine are burned in the pre-burner of a staged combustion cycle engine, resulting hot gas drives the turbine. The burned gas passing through the turbine is supplied to the combustor at high temperature and pressure. The form of the gas can be fuel rich or oxidizer rich dependent upon the mixture ratio or the engine scheme. When the cycle works at oxidizer-rich condition, the metal pipes composing the engine can be ignited or even exploded by an impact of very a small particle. In this study, we developed the powder combination and processes for an anti-oxidation coating through the analysis of various coating materials.

Ag Sintering Die Attach Technology for Wide-bandgap Power Semiconductor Packaging (Wide-bandgap 전력반도체 패키징을 위한 Ag 소결 다이접합 기술)

  • Min-Su Kim;Dongjin Kim
    • Journal of the Microelectronics and Packaging Society
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    • v.30 no.1
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    • pp.1-16
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    • 2023
  • Recently, the shift to next-generation wide-bandgap (WBG) power semiconductor for electric vehicle is accelerated due to the need to improve power conversion efficiency and to overcome the limitation of conventional Si power semiconductor. With the adoption of WBG semiconductor, it is also required that the packaging materials for power modules have high temperature durability. As an alternative to conventional high-temperature Pb-based solder, Ag sintering die attach, which is one of the power module packaging process, is receiving attention. In this study, we will introduce the recent research trends on the Ag sintering die attach process. The effects of sintering parameters on the bonding properties and methodology on the exact physical properties of Ag sintered layer by the realization 3D image are discussed. In addition, trends in thermal shock and power cycle reliability test results for power module are discussed.

Differential Susceptibility to High Temperature and Variation of Seasonal Occurrence between Spodoptera exigua and Plutella xylostella (파밤나방과 배추좀나방의 고온 감수성 차이와 연중 발생 변이)

  • Kim, Minhyun;Lee, Seunghee;Kim, Yonggyun
    • Korean journal of applied entomology
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    • v.55 no.1
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    • pp.17-26
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    • 2016
  • Climate change has been regarded as one of main factors to change Korean insect pest fauna. Especially, a global warming model predicts to expand habitat for insect pests originated from tropical or subtropical regions. Two insect pests, the beet armyworm (Spodoptera exigua) and the diamondback moth (Plutella xylostella), are known to overwinter in some greenhouse conditions without diapause induction in Korea. There was a clear difference between these two insects in seasonal occurrence. P. xylostella occurred only at early spring and fall seasons, but did not occur during summer. In contrast, S. exigua maintained their occurrence from late spring to fall seasons. This study set up a hypothesis that the difference in the seasonal occurrence may be resulted from variation in susceptibility to high temperature. To test the hypothesis, heat tolerance was compared between these two insects. Exposure to $42^{\circ}C$ for 40 min killed 100% individuals of P. xylostella larvae. However, most larvae of S. exigua survived in response to $42^{\circ}C$ even for 80 min. Heat tolerance varied among developmental stages in both insects. Highest tolerant stages were $4^{th}$ instar larvae and adults for P. xylostella, but $1^{st}$ instar larvae for S. exigua. Pre-exposure to $37^{\circ}C$ for 30 min significantly increased heat tolerance in both insects. Induction of heat tolerance accompanied with significant increase of glycerol contents in the hemolymph in both insects and up-regulation of three heat shock protein expressions in S. exigua. These results suggest that the differential susceptibility to high temperature explains the disappearance of P. xylostella during summer, at which S. exigua maintains its occurrence.

Improving Charge Injection Characteristics and Electrical Performances of Polymer Field-Effect Transistors by Selective Surface Energy Control of Electrode-Contacted Substrate (에폭시 개질 한 다관능 아크릴레이트를 포함하는 충격 저항성이 향상된 불포화폴리에스터 SMC (Sheet Molding Compound) 소재제조 및 그의 물성연구)

  • Jang, Jeong Beom;Kim, Taehee;Kim, Hye Jin;Lee, Wonjoo;Seo, Bongkuk;Kim, Yongsung;Kim, Changyoon;Lim, Choong-Sun
    • Journal of Adhesion and Interface
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    • v.21 no.3
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    • pp.101-106
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    • 2020
  • In this study, epoxy-modified acrylate was synthesized. The synthesized acrylate was added to the composition for sheet molding compound (SMC) in the range of 5 phr to 15 phr. The prepared SMC prepreg was molded at high temperature and pressure to produce a glass fiber reinforced composite. Physical properties such as tensile and impact strength of the composite were measured, respectively. Experimental data show that the composite with 5 phr of synthesized acrylate has 20% improved tensile strength and 12% improved impact strength than that of the reference sample.

Characterization of Biomass-Based Foam Structures for Home-Meal-Replacement Containers (가정간편식 용기용 바이오매스 기반 발포구조체의 특성에 관한 연구)

  • Kim, Inae;Kim, Sumin;Kambiz, Sadeghi;Han, Jeonggu;Hwang, Kiseop;Kwon, Hyukjoon;Kim, Yongsu;Yoo, Seung Ran;Seo, Jongchul
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.26 no.2
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    • pp.77-83
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    • 2020
  • A series of foamed plastic sheets containing biomass (as HMR container) were developed via different foaming process temperatures, and their density, porosity, WVTR, and pore morphology were evaluated. Thermal stability of samples during re-heating the food in oven, change in morphology, density, porosity, and WVTR were investigated using a simulated thermal shock process according to MIL-STD-883E assay. As such, the pore size of samples was generally increased with increasing temperature of the foaming process. It can be explained that as foaming temperature increased, the viscosity of molten resins and the repulsive force against pore expansion decreased. In addition, an increase in the thermal shock cycle reduced the pore size and WVTR, while density increased because high temperature treatment that softened the sheet matrix was followed by a low temperature incubation, which contracted the matrix, thereby changing the physical and morphological properties of samples. However, an insignificant change in density was observed and WVTR tended to be decreased, indicating that as-prepared foamed plastic sheets could be used as a high thermal stable container for HMR application. Therefore, it found that the properties of newly developed HMR containers containing biomass were dependent on the foaming process temperature. Moreover, to better understanding of these newly developed containers, further investigations dealing with foaming process temperature based on various food items and cooking conditions are needed.

방향성 다공질금속의 제조 및 기계적성질

  • Hyeon, Seung-Gyun;Nakajima, Hideo
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.11a
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    • pp.19.2-19.2
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    • 2009
  • 금속을 용해 응고시킬 때 생성되는 소위, 주조 결함이나 소결금속 내의 기공은 재료의 성능이나강도를 현저하게 낮추는 결함으로서 예전부터 기피되어 왔다. 또한, 재료공정에있어서도 여하의 기공이나 기포가 없는 치밀한 고강도 및 고기능성 재료를 개발하는 것에 최대한의 주의와 관심을 기울여 왔다. 그렇지만, 우리가 자연계의 천연물이나 인공물을 둘러보면 그 대부분이다공질임을 쉽게 눈치챌 수 있다. 예를 들어 목재, 지엽등의 생물을 시작해서 콘크리트 등의 인공물, 우리 체내의 뼈도 전형적인 다공질구조로 구성되어 있다. 이러한 구조로부터 재료의 재질제어 이외에 구조제어라는 새로운 어프로치를 고려할 수 있고, 최근 들어, 금속재료에 있어서도 이러한 다공질구조에 관한 연구가활성화되어 충격흡수재, 생체재료, 베어링재료 등의 다양한응용이 전개되고 있다. 특히, 원주상의 방향성 기공을 갖는 로터스금속은 기존의 복잡한구조의 다공질금속보다 뛰어난 기계적 성질을 갖는다. 이러한 다공질금속은 일방향응고할 때 생성하는 과포화가스원자를 석출시켜 기공을 일방향으로 성장시킨다. 즉, 융점에서의 고상과 액상의 가스 용해도 차를 이용하는 것으로서 응고시에 고용할 수 없는 가스원자가 기공을 형성한다. 이와같이 제조한 방향성 다공질금속은 BT (인플란트, 생체적합성, 저탄성, 경량), ST (초음속기엔진부품, 경량), IT (고성능수냉모듈), ET(고온촉매, 필터)의 분야로의 응용이 기대된다. 본 강연에서는 방향성 다공질금속의 제조법, 특성 및 응용을 포함하여그 동안의 연구성과 및 앞으로의 과제 등을 소개하고자 한다.

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Effects of high temperatures and hygrothermals on the collapse characteristics of CFRP thin-walled laminates (고온 .senter dot. 고습환경이 CFRP 적층 원통부재의 압궤특성에 미치는 영향)

  • 곽훈이;김정호;양인영
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1995.10a
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    • pp.650-654
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    • 1995
  • In this study, in order to measure energy-absorbing charactistics in collapse test of CFRP thin-walled laminates and interpretate the cause of decreasing age when collapse test is carried out under the environments of high temperatures and hygrothermals, the moisture absorbing behavior according to the variety of orientation angel is observed and collapse characteristics is compared with the influence of high temperatures and hygrothermals. Especially, we supposed to clearly understand reationship between collapse characteristics in proportion to the variety of orientation angel and moisture absorbing. The value of the maximum loading, mean loading,rate of energy absorption energy per unit volume and mass in CFRP thin-walled laminates on the high temperatures and hygrothermals is measured lower than under no moisture absorbing. The maximum collapse loading in dynamic impact test is taken measurement lower than in static collapse test regarding compared with collapse characteristics conformity with the variety of the CFRP circular laminates in high temperatures and hygrothermals. But the absorbed energy per unit mass and volume is almost same and the biggest amount of energy is shown in the CFRP circular laminates with orientation angel of 15 .deg.. Therefore, in the case of use to CFRP circular laminates with axisymmetric mode, CFRP thin-walled structal members with orientation angel of 10 .deg. , 15 . deg. are generally useful.

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