• Journal of the Korean Vacuum Society
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• v.9 no.3
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• pp.279-284
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• 2000

In order to analysis the degradation process of epoxy/glass fiber for outdoor condition, FRP laminate was exposed to high temperature and water. Then the degradation process was evaluated by comparing contact angle, surface potential decay, and surface resistivity. For the change of wettability, the contact angle of thermal-treated specimen with the high temperature of $200^{\circ}C$ increased. But that of water-treated specimen decreased. The characteristic of surface potential decay shows the tendency of the remarkable decrease on water-treated specimens, but increase on thermal-treated specimen compared with untreated one. Also, for the surface resistivity, it shows the same trend compared with the change of contact angle.

• Journal of Conservation Science
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• v.32 no.3
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• pp.321-331
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• 2016

Textiles damage caused by acetaldehyde($CH_3CHO$) is not clear as compared to other materials. Total 20 specimens were prepared using 4 different materials (silk, cotton, ramie, hemp) after dyed with 4 colors (undyed, red, yellow, blue, black). The specimens were exposed to $CH_3CHO$ gas in the test chamber. First, textile specimens' damage by differert concentration of acetaldehyde(0.1, 0.5, 1, 10, 100, 500, 1000 ppm) was tested. Second, accelerared damage to the textile specimens were tested according to the temperature and humidity conditions at the damage levels. Third, damage of deliberately degraded textile specimens were examined at the damage levels. After the exposure, optical, chemical, and physical evaluation was carried out. As a result, at 1000 ppm/day, the color difference of cotton_yellow has increased. At the condition of $25^{\circ}C-80%$, $30^{\circ}C-50%$, $30^{\circ}C-80%$, the color difference of yellow specimens has increased and grey scale rating has decreased. At $30^{\circ}C-80%$, acetate of cotton_undyed increased and the pH of silk_undyed decreased. In the case of deliberately degraded textile specimens, actetate concentration of black specimens increased. In conclusion, damage to the traditional fabric by acetaldehyde is not impact. However, it is expected that yellow specimens will be bleach and black specimens' actetate concentration will be increase.

• Journal of the Korean Electrochemical Society
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• v.23 no.3
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• pp.57-65
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• 2020

It is crucial to investigate the thermal degradation of lithium-ion batteries (LIBs) to understand the possible malfunction at high temperature. Herein, we investigated the effects of surface film formation on the thermal degradation of lithium cobalt oxide (LiCoO₂, LCO) cathode that is one of representative cathode materials. Cycling test at 60℃ exhibited poorer cycleability compared with the cycling at 25℃. Cathodes after the initial 5 cycles at 60℃ (60-LCO) exhibited higher impedance compared to the cathode after initial 5 cycles at 25℃ (25-LCO), resulting in the lower rate capability upon subsequent cycling at 25℃, although the capacity values were similar at the lowest C-rate of 0.1C. In order to understand degradation of the LCO cathode at the high temperature, we analyzed the cathodes surface using X-ray photoelectron spectroscopy (XPS). Among various peaks, intensity of lithium hydroxide (LiOH) increased substantially after the operation at 60℃, and the C-C signal that represents the conductive agent was distinctly lower on 60-LCO compared to 25-LCO. These results pointed to an excessive formation of cathode-electrolyte interphase including LiOH at 60℃, leading to the increase in the resistance and the resultant degradation in the electrochemical performances.

• Journal of the Korean Society of Food Science and Nutrition
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• v.38 no.1
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• pp.98-104
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• 2009

The objective of this study was to characterize quality changes of PET-packaged green tea beverage during 4-week storage at $60^{\circ}C$. Changes in oxygen transmission of the PET bottle package and cap removal torque were also examined. MXD6 blend PET bottle showed stability in the gas barrier. Its cap removal torque was kept stable during the 4 weeks. pH, color value, contents of vitamin C and catechin showed significant changes during the storage while caffeine and amino acid did not change significantly. Four alcohol flavor components (hexanol, linalool, menthol, and ${\alpha}$-terpineol) increased rapidly during the first three weeks while d-limonene did not show significant change. Sensory test showed decrease in astringent flavor lowering the product flavor and acceptability.

• Composites Research
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• v.35 no.6
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• pp.425-430
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• 2022

In this study, the mechanical properties of the pressure vessel composite exposed to the thermal environment were evaluated to establish the standard for high temperature static pressure test of the pressure vessel for hydrogen bus. As the tensile strength of the composite material approaches the glass transition temperature of the epoxy resin, the strength decreases due to the deterioration of the epoxy resin. In addition, it was confirmed that the tensile strength increased again due to the post-curing of the epoxy resin during long-term exposure. Therefore, the accelerated stress rupture test conditions of the pressure vessel for the hydrogen bus should be set based on the epoxy resin properties of the carbon fiber composite material.

• Korean Chemical Engineering Research
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• v.61 no.3
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• pp.356-361
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• 2023

In order to improve the durability of the proton exchange membrane fuel cell (PEMFC), it is important to accurately evaluate the durability of the polymer membrane in a short time. The test conditions for chemically accelerated durability evaluation of membranes are high voltage, high temperature, low humidity, and high gas pressure. It can be said that the protocol is developed by changing these conditions. However, the relative influence of each test condition on the degradation of the membrane has not been studied. In chemical accelerated degradation experiment of the membrane, the influence of 4 factors (conditions) was examined through the factor experiment method. The degree of degradation of the membrane after accelerated degradation was determined by measuring the hydrogen permeability and effluent fluoride ion concentration, and it was possible to determine the degradation order of the polymer membrane under 8 conditions by the difference in fluoride ion concentration. It was shown that the influence of the membrane degradation factor was in the order of voltage > temperature > oxygen pressure > humidity. It was confirmed that the degradation of the electrode catalyst had an effect on the chemical degradation of the membrane.

• JOURNAL OF ELECTRICAL WORLD
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• s.257
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• pp.78-82
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• 1998

CD(Computer Disc) 의 약 7배의 용량을 가진 디스크와 그 관련기기가 시판되기 시작했다. DVD(Digital Versatile Disc), DVD-ROM이라는 이 기기는 디스크위에 집광되는 광스포트의 크기를 작게 하여 기록밀도를 높이기 위해, 대물렌즈의 NA,를 0.6으로 크게 하였고(CD에서는 NA가 0.45)광원이 되는 레이저의 파장도 650mm대로 단파장화(CD에서는 780nm)하였다. 이의 실현을 본격화하기 위해서는 DVD에 대응할 수 있는 대용량의 기록미디어와 장치가 필요하다. 이미 CD-R을 비롯한 몇 가지의 추기형, 서환형의 DVD-RAM 등이, 재생전용 DVD가 시판되기 이전부터 제안되어 규격화되었으며 미쓰비시전기에서도 그것에 조준을 맞추어 광원이 되는 고출력 반도체레이저의 개발과 제품화를 추진하여 온 것이다. 여기서는 다음에 제시하는 DVD-RAM용 반도체레이저에 대한 요구성능과 이를 실현하기 위한 방법 및 결과에 대하여 기술한다. $\cdot$파장 650nm대에서 30~50mW의 높은 광출력을 얻을 수 있는 활성층의 재료와 구조의 개발 $\cdot$60$^{\circ}C$의 고온에서도 동작전류 증가가 적은 활성층구조의 최적화 $\cdot$고온, 고출력의 장시간 동작에서도 발광부 단면의 열화를 방지 할 수 있는 단면 강화기술의 개발 동사는 이들 기?과 과제에 대하여 검토를 거듭한 결과 DVD-RAM광원에 적합한 고출력 반도체레이저(MLIxx6시리즈)의 제품화를 실현할 수 있었다.

• Journal of the Korea Institute of Military Science and Technology
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• v.4 no.1
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• pp.255-263
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• 2001

The main purpose of this paper is to investigate strength characteristics of Aluminum 2024-T3 in high temperature environment. Tensile test of Aluminum 2024-T3 has been carried out in high temperature environment. The stress-strain relations are investigated with temperature and Young's modulus, yield strength and ultimate strength are deduced from the test results. The modulus and strength of the test are compared with those of MIL HANDBOOK and tips on structural design in high temperature environment are suggested.

• Transactions of the Korean Society of Automotive Engineers
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• v.8 no.6
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• pp.279-286
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• 2000

The stud bolts tend to degrade faster by high temperature(over 45$0^{\circ}C$). Therefore, replacement cycle inspection of stud bolts were carried out various method such as ultrasonic test(UT), magnetic test(MT), wobble test, visual test and hardness test. Especially, wobble test method has been applied to determine replacement evaluation criteria of stud bolt after long time operation. We applied three different methods on the three site and the obtained data are compared with the results from the evaluation methods. From the results, the replacement criteria for stud bolts under high temperature in power plants are proposed.

• The tire
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• s.65
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• pp.3-9
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• 1976

가유 고무에 대변형의 반복왜를 외부자극으로서 부여하면 초기에는 대폭의 응력의 변화현상이 보여져 서서히 일정응력치에 접근하여 파단에 이른다. 이 응력의 변화현상과 피로수명(파단하기까지의 회수)이 여하한 기계적 화학적 인자의 영향을 받는가를 천연고무의 순고무 가유물로 검토했다. 그 결과 실온으로 고무에 반복신장피로를 부여하면 가교구조, 망목밀도 및 신장률이 응력변화의 대소, 피로수명의 증감에 영향을 주었다. 고온으로 고무에 반복신장피로를 주면 열산화에 의하여 어느 온도로부터 현저한 응력연화(화학응력연화) 현상이 보였다. 연이나 고무에 열화방지제를 첨가하면 고온에 있어서의 산화반응이 억제되기 때문에 무첨가의 경우와 달라서 파단이나 현저한 응력연화가 일어나지 않았다. 피로수명(F)와 파괴신장(εb),반복신장률(ε)사이에 F=A(εb-ε)n 의 관계가 성립함이 인정되었다. An은 고유의 파라메에터어이며 천연고무의 순고무가유물로서 n은 4.0~4.5의 거의 일정치를 표시했다.