• Title/Summary/Keyword: 고온균열시험

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고온의 염기성 수용액에서 Ni기 합금의 응력부식파괴

  • 김홍표;황성식;국일현;김정수
    • Proceedings of the Korean Nuclear Society Conference
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    • 1998.05b
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    • pp.84-89
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    • 1998
  • Alloy 600 및 alloy 690과 Ni-8Cr-lOFe 합금 등의 응력부식(stress corrosion cracking, SCC) 거동을 고온의 염기성 분위기에서 C-ring 시편을 사용하여 연구하였다. Alloy 600과 alloy 690을 여러 조건에서 열처리하여 etching한 후 탄화물의 분포와 입계 주변의 Cr고갈 정도 등의 미세조직을 광학현미경과 주사 전자현미경(SEM)으로 관찰하였다. 이들 재료에 대한 SCC 시험을 315$^{\circ}C$의 40% NaOH 수용액에서 일정한 부하전위(부식전위 + 200㎷)를 가하면서 수행하였으며, 동일 조건에서의 분극거동도 측정하였다. Alloy 600 MA(mill anneal) 및 TT(thermal treatment)의 SCC 저항성은 alloy 690 TT와 Ni-8Cr-10Fe SA(solution anneal)보다 낮았다. Alloy 600 TT 재료는 alloy 600 MA 및 SA 재료에 비해 SCC 저항성이 더 컸다. 고용 탄소농도는 alloy 600의 SCC 저항성에 큰 영향을 주지 못했다. 대부분의 Alloy 600은 균열전파 입계균열을 보였으나, 일부에서는 입계 및 입내 혼합양상(mixed mode cracking)을 보였다. 염기성 분위기에서 Ni기 합금의 SCC 거동을 미세조직, 분극거동의 관점에서 고찰하였다.

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Performance of Hybrid Fiber Reinforced Concrete at Elevated High Temperature (고온에서 하이브리드 섬유보강 콘크리트의 성능)

  • Won, Jong-Pil;Park, Kyung-Hoon;Park, Chan-Gi
    • Journal of the Korea Concrete Institute
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    • v.20 no.3
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    • pp.325-333
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    • 2008
  • This study evaluated the mechanical performance, shrinkage crack and fire resistance of hybrid fiber (blended steel and polypropylene fiber with different diameter and length) reinforced concrete at elevated temperature. The compressive, splitting tensile, flexural, plastic shrinkage test were conducted to the evaluate the mechanical properties and the resistance of shrinkage crack. Also, the surface investigation, reduction rate of mass and residual compressive test were performed to evaluate the physical and mechanical properties after 400$^{\circ}C$, 600$^{\circ}C$, 800$^{\circ}C$ and 1,200$^{\circ}C$ exposure. Test results showed that the hybrid fiber reinforced concrete improved the mechanical performance, shrinkage crack and fire resistance. The reduction of performance with a temperature change were high at the temperature of $600\sim800^{\circ}C$.

A study on the Creep Behavieo of Rene 80 Superalloy (Rene 80초내열 합금의 크리프 거동에 관한 연구)

  • Han, Seong-Ho;Lee, Gi-Ryong;Jo, Chang-Yong;Kim, In-Bae;Kim, Hak-Min
    • Korean Journal of Materials Research
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    • v.3 no.6
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    • pp.575-584
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    • 1993
  • The effects of atmosphere on the creep rupture properties of Ni-base superalloy Ren6 80 were investigated. Creep rupture tests were performed at $760^{\circ}C$, 657MPa and 982%, 157MPa under Ar gas atmospheres. Creep rupture mode and rupture properties (rupture life and elongation) were similar in two different atmospheres under the condition of $760^{\circ}C$, 657MPa. However, the results at $982^{\circ}C$, 157MPa showed different creep rupture mode and life between air and Ar gas atmospheres. In air, it was shown that creep cracks were initiated at surface-exposed grain boundaries and propagated along grain boundaries. In Ar gas atmosphere, the cracks were initiated at inner grain boundaries and coalesced to surface cracks which cause cup-and-cone type fracture. Due to protective oxide layer formation, air test showed longer rupture life than Ar test.

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Comparison of Crack Growth Test Results at Elevated Temperature and Design Code Material Properties for Grade 91 Steel (Grade 91 강의 고온 균열진전 실험 결과와 설계 물성치의 비교)

  • Lee, Hyeong-Yeon;Kim, Woo-Gon;Kim, Nak-Hyun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.39 no.1
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    • pp.27-35
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    • 2015
  • The material properties of crack growth models at an elevated temperature were derived from the results of numerous crack growth tests for Mod.9Cr-1Mo (ASME Grade 91) steel specimens under fatigue loading and creep loading at an elevated temperature. These crack growth models were needed for defect assessment under creep-fatigue loading. The mathematical crack growth rate models for fatigue crack growth (FCG) and creep crack growth (CCG) were determined based on the test results, and the models were compared with those of the French design code RCC-MRx to investigate the conservatism of the code. The French design code RCC-MRx provides an FCG model and a CCG model for Grade 91 steel in Section III Tome 6. It was shown that the FCG model of RCC-MRx is conservative, while the CCG model is non-conservative compared with the present test data. Thus, it was shown that further validation of the property was required. Mechanical strength tests and creep tests were also conducted, and the test results were compared with those of RCC-MRx.

고온고습 환경에서 태양전지 모듈의 성능 향상을 위한 연구

  • Kim, Ju-Hui;O, Won-Uk;Bae, Su-Hyeon;Kim, Dong-Hwan;Park, No-Chang
    • Proceedings of the Korean Vacuum Society Conference
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    • 2014.02a
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    • pp.494.1-494.1
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    • 2014
  • 태양광은 세계적으로 유망한 에너지 중의 하나이며, 태양광 모듈은 실제 옥외 조건에 따라 다르지만 장기 신뢰성과 수명을 보장하기 위해 최소 20년 이상을 안정적으로 작동될 필요성이 있다. 하지만 실제 태양전지는 옥외에 장기 노출됨에 따라 성능이 저하되며, 그 원인으로는 셀 균열, 부식, 접착 강도 손실 및 박리, 그리고 변색 등이 있다. 본 논문에서는 부식으로 인한 성능 저하를 완화하기 위해 희생금속을 이용하여 태양전지 모듈의 성능 향상에 대해 연구하였다. 태양전지는 4 cell 결정질 실리콘 태양전지 미니 모듈을 이용하였고, 희생금속의 영향을 확인하기 위해 두 종류의 시료를 준비하였다. 한 시료에는 Al 희생금속을 태양전지 리본 위에 부착하였으며, 나머지 한 시료는 비교 시료로 Al 희생금속을 부착하지 않았다. 시료는 $85^{\circ}C$ 85%의 상대습도인 고온고습 조건에서 2500시간을 진행하였다. 그리고 2500시간의 고온고습 시험이 진행된 시료의 전기적 특성을 분석하였다. 시험 결과, 희생금속이 없을 경우 28.8%의 출력 저하가 있었으며, 희생금속이 있을 경우 19.3%의 출력 저하가 확인되었다. 또한, 희생금속이 없을 경우, 충실도는 21.5% 감소하였으며, 단락전류 역시 약 6% 정도 감소하였다. 반면, 희생금속이 있을 경우, 충실도는 16.1%로 감소하였고, 단락전류는 거의 변화가 없었다.

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Type 347 stainless steel 피로시험 데이터의 통계처리

  • Min, Gi-Deuk;Kim, Seon-Jin
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.11a
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    • pp.35.2-35.2
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    • 2009
  • 최근 전세계적으로 저탄소, 녹색성장으로 인하여 원자력발전이 주목받고 있다. 또한 에너지의 고효율로 인한 발전소의 설비가 대형화가 됨에 따라 발전소의 수명평가와 건전성평가가 중요해지고 있다. 일반적으로 구조물 내에 존재하는 균열의 크기와 형상을 파악하여 피로균열전파속도를 평가함으로써 건전성평가를 확인하고 있다. 그리고 고온, 고압에서의 피로균열전파속도는직류전위차 (Direct Current Potential Drop : DCPD)법을 사용하고 있다. DCPD법은 균열의 정밀한 측정방법으로써 측정시 오차가 발생하기 때문에 ASTM에서 제시된 incremental polynomial 법을 권고하고 있다. 따라서 본 연구에서는 피로균열전파전파속도의통계적처리를 통해서 합리적인 곡선을 구하여 건전성평가에 활용하고자 한다. 실험에 사용된 시편은 두께 5mm, 폭 25.4mm CT시편을 사용하였으며, 1mm의 예비균열을 주었다. 그리고 실험온도는 상온에서 실시 하였으며, 주파수는 10Hz를 주었다. 그리고 DCPD 측정을 위해 5A의 전류를 주었으며, 이때 측정된 전압값을 ASTM에 제시된 관계식에넣어 균열길이로 환산하였으며, 데이터처리는 ASTM에 제시된 incremental polynomial법을 기본적으로 사용하였다. 또한 ASTM에 제시된 2n+1을 이용하여 데이터의 수 n을 1~7 까지 변화를 주어 3~15 point 까지 데이터를 처리하여곡선을 제시하였다. 분석결과 $R^2$값이 1을 기준으로 했을 때 3~7 point 까지는큰 차이를 보이지 않았지만 9-point 이후부터는 $R^2$ 감소함을 알 수 있었다. 또한 적용된 데이터의수에 따라 피로군열전파속도 곡선에서 측정된 Paris law의 n값과 C 값은 큰차이를 보이지 않았다.

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Evaluation of Fatigue Crack Propagation Behavior of Nickel-based Powder Metallurgy Superalloy for Aircraft at Elevated Temperature (항공기 터빈 디스크용 니켈기 초내열 분말야금 합금의 고온 피로균열진전 거동 비교 평가)

  • Yoon, Dong Hyun;Na, Seong Hyeon;Kim, Jae Hoon;Kim, Hongkyu;Kim, Donghoon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.41 no.8
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    • pp.751-758
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    • 2017
  • The behavior of fatigue crack growth of nickel-based powder metallurgy superalloy that could be used in aircraft turbine disc is investigated at room temperature, and $650^{\circ}C$ considering real operating conditions. The direct current potential drop(DCPD) method was used to measure the crack length of material in real time according to ASTM E647. Tests were performed with various stress ratios (0.1 and 0.5). Experimental results show that stress ratio, and temperature all affect the behavior of fatigue crack growth. As the stress ratio and temperature increase, the fatigue crack growth rate of nickel-based powder metallurgy superalloy also increases. Results were compared and reviewed with fatigue crack growth rates of other nickel-based superalloy materials (Inconel-100) that were studied in previous papers. Fractography analysis of the fractured specimens was performed using as SEM.

A study of comparative experiment process for heat resistance of brake disk materials (제동디스크 소재의 내열성 비교시험방법 연구)

  • Lim, Choong-Hwan;Goo, Byeong-Choon
    • Proceedings of the KSR Conference
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    • 2008.06a
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    • pp.941-947
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    • 2008
  • In the braking of a railroad car, mechanical brake systems using wheel tread and brake disk are applied as well as electrical brake systems by regenerator and rheostat. During disk braking, kinetic energy of the vehicle is converted into thermal energy through friction between disk and brake pad. And it causes high temperature concentration and generates thermal crack on the brake disk surface. In this study, comparative test process for heat-resistance of candidate materials was designed for development of brake disk materials having high heat-resistance. We also verified the efficiency of the process by experiments using conventional brake disk materials.

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Correlation Between Transient Regime and Steady-State Regime on Creep Crack Growth Behavior of Grade 91 Steel (Grade 91 강의 크리프 균열성장 거동에 대한 천이영역과 정상상태영역의 상관 관계)

  • Park, Jae-Young;Kim, Woo-Gon;Ekaputra, I.M.W.;Kim, Seon-Jin;Kim, Eung-Seon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.39 no.12
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    • pp.1257-1263
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    • 2015
  • A correlation between the transient regime and steady state regime on the creep crack growth (CCG) for Grade 91 steel, which is used as the structural material for the Gen-IV reactor systems, was investigated. A series of CCG tests were performed using 1/2" CT specimens under a constant applied load and at a constant temperature of $600^{\circ}C$. The CCG rates for the transient and steady state regimes were obtained in terms of $C^*$ parameter. The transient CCG rate had a close correlation with the steady-state CCG rate, as the slope of the transient CCG data was very similar to that of the steady state data. The transient rate was slower by 5.6 times as compared to the steady state rate. It can be inferred that the steady state CCG rate, which is required for long-time tests, can be predicted from the transient CCG rate obtained from short-time tests.

Surface crack growth behaviors of 304 stainless steel at elevated temperatures (304 스테인리스 鋼의 高溫에서의 表面균열 成長特性에 관한 硏究)

  • 서창민;신형섭;권영태
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.11 no.3
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    • pp.355-361
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    • 1987
  • Creep and fatigue tests were carried out on crack growth properties of small surface cracks in 304 stainless steel at 538.deg.C, 593.deg. C and 650.deg. C in air, by using small plate specimens with a small artificial pit. All the data of the crack growth rate per hour obtained in the present tests were correlated with the maximum stress intensity factor, so that the applicability of linear fracture mechanics to the crack growth of surface cracks at elevated temperature was investigated. In the creep test, relatiion of .sigma.$\^$n/.t$\_$f/=C is obtained between failure time and nominal stress at each temperature level, where n has the value of 11-14 depending on the temperature level. In the creep and fatigue crack growth properties of surface cracks at the elevated temperatures, the maximum stress intensity factor, $_{4}$$\_$max/, is some extent applicable parameter to describe the surface crack growth rate under the present experimental conditions. The crack growth rate per hour increases when the holding time decreases, and creep crack growth rate per hour becomes the lowest limit of crack growth rate per hour in this tests.