• Journal of the Korean Vacuum Society
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• v.2 no.3
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• pp.374-383
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• 1993

필라멘트와 Si 기판 사이의 기전력을 20, 80, 140, 200V로 증가시키면서 EACVD에 의하여 성장된 다이아몬드 박막에 대하여 다이아몬드/Si 계면분석 및 계면강도를 측정하였다. 주사형전자현미경(SEM), 고분해능투과형전자현미경(HRTEM), 오제이전자분석기(AES)에 의해 계면상태를 분석한 결과, 기전력 증가에 따라 활성탄화수소 이온(CmHn-)에너지가 증가되어져 CmHn-이 Siso로 침투(Impringement)가 증가되고 침투된 높은 에너지의 CmHn-이 Si과 화학결합하여 생성되는 SiC층 깊이 및 농도 분포도 증가된다. 풀 시험(Pull test)에 의한 계면강도 측정 결과, SiC층 깊이 및 농도분포가 증가할수록 계면강도가 증가하였다. 관찰된 파면과 파면의 X-선 메핑 결과 및 HRTEM과 AES에 의한 분석 결과, 기전력 증가에 따라 공극율이 적고 치밀한 다이아몬드 박막이 성장된다. 그리고 생성되는 SiC층 농도 및 깊이 분포가 증가함에 따라 다이아몬드/Si 계면이 강화되고, 상대적으로 파괴는 다이아몬드/Si 계면이 아닌 SiC층이나 Si 내부에서 발생된다. 결국, 기전력을 증가하여 활성탄화수소이온의 에너지를 증가함으로써 계면강도가 우수하며 공극율이 매우 적고 치밀한 다이아몬드 박막을 성장할 수 있다.

• Journal of Power System Engineering
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• v.7 no.1
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• pp.25-33
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• 2003

섬유강화 복합재료의 계면 강도는 강화재와 메트릭스간의 계면특성, 강화용 섬유의 표면처리 및 섬유간의 거리 등에 많은 영향을 받는다. 본 연구에서는 섬유간의 거리가 섬유강화 복합재료의 계면특성에 미치는 영향을 고찰하기 위해, E glass fiber/epoxy 복합재료의 시험편을 제작하고, 섬유의 표면처리 및 섬유파괴가 이웃하는 섬유파괴에 영향을 미치는 거리에 대해 고찰하였다. E glass fiber/epoxy 복합재료의 계면 전단강도는 섬유간 거리 $0{\sim}50{\mu}m$ 사이에서는 섬유의 표면처리와는 관계없이 섬유간 거리가 증가할수록 증가하였고, 섬유간 거리 $50{\mu}m$ 이상에서는 섬유간거리에 관계없이 계면전단강도는 일정하였다.

• Composites Research
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• v.34 no.5
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• pp.305-310
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• 2021

Mechanical properties of fiber reinforced composites were affected to fiber volume fractions (FVF) and interfacial property by sizing agent conditions. An optimum interface can relieve stress concentration by transferring the mechanical stress from the matrix resin to the reinforcements effectively, and thus can result in the performance of the composites. The interfacial properties and wettability between the epoxy resin and glass fiber (GF) were evaluated for different sizing agent conditions and FVFs. The surface energies of epoxy resin and different sizing agent treated GFs were calculated using dynamic and static contact angle measurements. The work of adhesion, W_a was calculated by using surface energies of epoxy matrix and GFs. The wettability was evaluated via the GF tow capillary test. The interfacial shear strength (IFSS) was evaluated by microdroplet pull-out test. Finally, the optimized GFRP manufacturing conditions could be obtained by using wettability and interfacial property.

• Elastomers and Composites
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• v.34 no.1
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• pp.31-44
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• 1999

Interfacial adhesive strength between the fully-crosslinked and partially-crosslinked rubber layers were Investigated at the temperature range of $30{\sim}120^{\circ}C$ for four different rubbers(NR, SBR, EPDM, BIMS). The surfaces of interfacial failure were also investigated using a scanning electron microscopy(SEM). The physical interlinking played a major role in the adhesive strength between the fully-crosslinked rubber layers. When a partially-crosslinked rubber layer was bonded to the fully-crosslinked one, the chemical as well as the physical interlinking affected the adhesive strength. NR showed a "interfacial knotty tearing" pattern, while EPDM showed a typical "cross-hatched" one when the adhesive strength approached to the cohesive tear strength of each material.

• Journal of the Korea institute for structural maintenance and inspection
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• v.19 no.3
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• pp.149-160
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• 2015

This study reports the interfacial bond strength between Ultra High Performance Concrete (UHPC) and Normal Strength Concrete (NSC). While previous studies have focused on the interfacial strength between NSC substrate and UHPC overlay, this study use precast UHPC for enhanced constructability and replacement of formwork. The factors affecting the interface strength are comprehensively reviewed. It can be classified into: interface shape, degree of hardening and moisture condition of UHPC before combining with NSC, and curing condition of composite materials. Conducted experiments verify the effects of each factor on the interface strength and, accordingly show different failure modes. In particular, a new failure mode of the failure of a part of UHPC was firstly found in the case of sample with rough interface between UHPC and NSC. The other factors of the degree of hardening and the moisture and curing conditions of UHPC were discussed. This research will provide a valuable foundation to utilize the UHPC as a composite material.

• Polymer(Korea)
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• v.24 no.1
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• pp.23-28
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• 2000

Autoadhesion strength of PS/PS Interfaces in solvent welding was determined as a function of processing conditions by butt joint test. It was verified that the chain mobility and surface roughness at PS/PS interface were enhanced by the applied solvent having a similar solubility parameter as PS and resulted in the dramatic improvement of autoadhesion strength at PS/PS interface. It was found that the mechanism of solvent welding is dependent upon the chain mobility due to the diffusion of solvent to PS interface and the contact area at interface. When the welding temperature is lower than the boiling point of applied solvent, the effect of chain mobility on autoadhesion strength was dominated, while contact area took more important role when welding temperature is above the boiling point of solvent. Autoadhesion strength increased with increasing contact time and contact temperature but :he effect of solvent on autoadhesion strength became smaller.

• Composites Research
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• v.24 no.4
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• pp.11-16
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• 2011

Retention of interfacial shear strength (IFSS) of polymer composites at cryogenic temperature application is very important. In this work, single carbon tiber reinforced epoxy compositc was used to evaluate IFSS and apparent modulus under room and cryogenic temperatures. The property change of carbon and selected epoxy for particularly cryogenic temperature application were tested in tension and compression. Tensile strength and elongation of carbon fiber decreased at cryogenic temperature, whereas tensile modulus was almost same. On the other hand, epoxy matrix showed the increased tensile strength but decreased elongation. It can be due to maximum thermal contraction existing free volume in cryogenic temperature. IFSS increased up to $-10^{\circ}C$ and then decreased steadily. However, IFSS at cryogenic temperature was still similar to that at room temperature. This result is very useful to cryogenic application since selected epoxy toughness and interfacial adhesion can keep at such low temperature.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.17 no.8
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• pp.449-455
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• 2016

This study is a part of research to develop a steel-concrete hybrid girder using ultra high-performance concrete with a compressive strength of 80 MPa. To this end, the Eurocode design formula for the shear resistance developed in a concrete-to-concrete interface was examined for the interface between concrete layers of different strengths. To examine the effect of the surface roughness on the shear resistance, a push-out test was conducted on specimens while considering the parameters of the Eurocode design equation. The actual behavior was evaluated with respect to the compressive strength of the concrete, the reinforcement ratio of the shear rebar, and the interfacial surface condition. The specimen with a rough interface shows 20-50% higher shear strength than that estimated by the design equation. In the case of failure mode, abrupt failure tends to occur at the interface of the concrete layer for the specimen with a low reinforcement ratio. It is expected that the shear strength of the concrete layer will increase according to the strength differential in the concrete layers.

• Journal of the Korean Recycled Construction Resources Institute
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• v.9 no.3
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• pp.268-275
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• 2021

The three factors that determine the strength of concrete are the strength of cement paste, aggregate and ITZ(Interfacial Transition Zone) between aggregate and cement paste. Out of these, the strength of ITZ is the most vulnerable. ITZ is formed in 10~50㎛, the ratio of calcium hydroxide is high, and CSH appears low ratio. A high calcium hydroxide ratio causes a decrease in the bond strength of ITZ. ITZ is due to further weak area. The problem of ITZ appears as a more disadvantageous factor when it used lightweight aggregate. The previous study of ITZ properties have measured interfacial toughness, identified influencing factors ITZ, and it progressed SEM and XRD analysis on cement matrix without using coarse aggregates. also it was identified microstructure using EMPA-BSE equipment. However, in previous studies, it is difficult to understand the microstructure and mechanical properties. Therefore, in this study, a method of measuring electrical resistance using EIS(Electrochemical Impedance Spectroscopy) measuring equipment was adopted to identify the ITZ between natural aggregate and lightweight aggregate, and it was tested the change of ITZ by surface coating of lightweight aggregate with ground granulated blast furnace slag. As a result, the compressive strength of natural aggregate and lightweight aggregate appear high strength of natural aggregate with high density, surface coating lightweight aggregate appear strength higher than natural aggregate. The electrical resistivity of ITZ according to the aggregate appeared difference.

• Composites Research
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• v.21 no.4
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• pp.15-21
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• 2008

Interfacial shear strength between epoxy and carbon fiber was analyzed utilizing a hemi-spherical microbond specimens adhered onto single carbon fiber. The hemi-spherical microbond specimen showed high regression coefficient and small standard deviation in the measurement of interfacial strength as compared with a droplet and an inverse hemi-spherical one. This seemed to be caused by the reduced meniscus effects and the reduced stress concentration In the region contacting with a pin-hole loading device. Finite element analysis showed that the stress distributions along the fiber/matrix interface in the hemi-spherical specimen had a stable shear stress distribution along the interface without any stress mode change. The experimental data was also different according to the kinds of loading device such as the microvise-tip and the pin-holed plate.