• Title/Summary/Keyword: 건조 밀도

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Optimization of powder compaction parameters for the pressureless sintered ZTA (상압소결 ZTA의 분말 성형 공정 최적화)

  • 신동우;김경도;박삼식;임창성;이수완
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.8 no.2
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    • pp.356-364
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    • 1998
  • The dependence of green and sintered densities of Zirconia-Toughened Alumina ($ZTA:\;Al_2O_3/\;15\;vol{%}\;ZrO_2$) on the properties of spray-dried granules was studied thoroughly to establish the optimum compaction condition leading to high reproducibility in the light of sintered density. The sphericity, mean size, degree of hollow occurrence and moisture content of spray-dried granules were largely different in between the granule containing binder and the ones with no binder. The effect of these differences in the characteristic of granules on the compaction behavior was examined in terms of the compaction pressure from 80 MPa to 120 MPa 10 MPa increment and the compaction method, i.e., uniaxial and cold isostatic pressing. This work confirmed that the reproducibility of sintered density caused by the variation of granule property could be improved by the optimization of compaction process. The variation of sintered density was controlled within 1 % deviation by compacting the granules under a relatively low pressure of 80 MPa in an uniaxial forming and subsequent cold isostatic pressing at high pressure of 500 MPa.

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마직물의 태에 관한 연구 -주관적 태 평가 방법과 객관적 태 측정을 통한 산출식의 개발을 중심으로-

  • 박성혜;유효선
    • Proceedings of the Korean Society for Emotion and Sensibility Conference
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    • 1999.03a
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    • pp.219-219
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    • 1999
  • 마직물은 통기성, 흡수성, 투습성이 좋고 건조가 빠른 편이므로 여름철 직물로 많이 사용되어 왔다. 마직물은 또한 뻣뻣하며 몸에 감기지 않고 촉감이 깔깔하여 시원한 느낌을 주며 다른 직물에 비해 강직하고 표면이 거칠고 드레이프성이 떨어지는 등의 독특한 태를 가지고 있다. KES-F 시험기에 의해 여러 물성량들을 종합적으로 계측할 수 있게 됨에 따라 의복의 착용감에 만족을 주는 소재의 성능에 대한 연구가 종래의 주관적평가에서 KES-F 시스템을 이용하여 객관적으로 태를 예측하는 방법으로 진행되고 있다. 그러나 태를 평가하는 객관적 방법에서는 일반적으로 Kawabata와 Niwa에 의해 만들어진 평가식들이 주로 사용되나 이런 식들은 주로 모직물이나 합성섬유직물들을 평가하기에는 적합하지만 마직물의 독특한 태를 평가하기에는 부족하다고 생각된다. 마직물의 태가 기존의 객관적 평가방법만으로는 규명되지 않기 때문에 주관적 태평가방법을 아울러 실시해야 할 필요가 있다고 생각된다. 따라서 본 연구에서는 마직물의 태를 평가하는 방법의 하나로 주관적 평가척도를 개발하고 이 척도를 사용하여 마직물의 주관적인 태 특성을 살펴보았다. 그리고 KES-FB 시스템을 사용한 객관적인 태를 측정하여 주관적 평가치와 객관적 측정치로부터 태 평가의 산출식을 유도하였다. 실험에 사용된 직물은 혼방률, 밀도, 두께 등이 다양한 암, 저마 그리고 마혼방직물과 한산모시, 중국마, 신합섬 직물 등 총 54종을 사용하였다. 마직물의 주관적 태 평가를 위해 26문항의 형용사쌍으로 구성된 9점의 의미미분척도를 개발하였으며 이 척도를 사용해 주관적 평가를 실시하였다. 또 객관적 평가를 위해 KES-FB 시스템을 통해 역학적 특성치를 구하였다. 주관적 평가를 실시한 결과 마직물의 태에 영향을 미치는 7개의 요인이 추출되었다. 이 요인들은 표면성질, 신축성/드레이프성, 중량감, 강연성, 회복성, 수분특성, 밀도감이었으며, 요인들로 설명되는 누적분산값은 67.18%였다.주관적 평가의 결과와 객관적 평가 결과를 이용해 마직물의 태를 평가하는 산출식을 제시하였다. 태 평가치의 경우 16가지 특성치를 모두 넣는 방법과 stepwise 방법, 또 Kawabatark 사용한 순차적 군 회귀법의 세가지 방법의 회귀식 중 16가지 특성치를 모두 넣는 방법의 결정계수가 가장 높았다.

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Fabrication of Organic-Inorganic Nanocomposite Blade for Dicing Semiconductor Wafer (반도체 웨이퍼 다이싱용 나노 복합재료 블레이드의 제작)

  • Jang, Kyung-Soon;Kim, Tae-Woo;Min, Kyung-Yeol;Lee, Jeong-Ick;Lee, Kee-Sung
    • Composites Research
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    • v.20 no.5
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    • pp.49-55
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    • 2007
  • Nanocomposite blade for dicing semiconductor wafer is investigated for micro/nano-device and micro/nano-fabrication. While metal blade has been used for dicing of silicon wafer, polymer composite blades are used for machining of quartz wafer in semiconductor and cellular phone industry in these days. Organic-inorganic material selection is important to provide the blade with machinability, electrical conductivity, strength, ductility and wear resistance. Maintaining constant thickness with micro-dimension during shaping is one of the important technologies fer machining micro/nano fabrication. In this study the fabrication of blade by wet processing of mixing conducting nano ceramic powder, abrasive powder phenol resin and polyimide has been investigated using an experimental approach in which the thickness differential as the primary design criterion. The effect of drying conduction and post pressure are investigated. As a result wet processing techniques reveal that reliable results are achievable with improved dimension tolerance.

Construction and Application of an Automated Apparatus for Calculating the Soil-Water Characteristic Curve (자동 흙-함수특성곡선 시험장치 구축 및 활용)

  • Song, Young-Suk;Lee, Nam-Woo;Hwang, Woong-Ki;Kim, Tae-Hyung
    • The Journal of Engineering Geology
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    • v.20 no.3
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    • pp.281-295
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    • 2010
  • A new, automated apparatus is proposed for calculating the Soil-Water Characteristic Curve (SWCC), representing a simple and easily applied testing device for continuous measurements of the volumetric water content and suction of unsaturated soils. The use of this apparatus helps to avoid the errors that arise when performing experiments. Consequently, the apparatus provides greater accuracy in calculating the SWCC of unsaturated soils. The apparatus is composed of a pressure panel, flow cell, water reservoir, air bubble trap, balance, sample-preparation accessories, and measurement system, among other components. The air pressure can attain 300 kPa, and a general test can be completed in a short time. The apparatus can simply control the drying process and wetting process. The changes in volumetric water content that occur during the drying and wetting processes are shown directly in the SWRC program, in real time. As a case study, we performed an SWCC test of Joomunjin sand (75% relative density) to measure matric suction and volumetric water content during both the drying and wetting processes. The test revealed hysteresis behavior, whereby the water content on the wetting curve is always lower than that on the drying curve for a specific matric suction, during the wetting and drying processes. Based on the test results, SWCCs were estimated using the Brooks and Corey, van Genuchten, and Fredlund and Xing models. The van Genuchten model performed best for the given soil conditions, as it yielded the highest coefficient of determination.

Evaluation of Dietary Carbohydrate Sources for Juvenile Abalone (Haliotis discus hannai) (참전복 사료의 탄수화물원 평가)

  • 이상민;윤성종;유성규
    • Journal of Aquaculture
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    • v.11 no.2
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    • pp.133-140
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    • 1998
  • A 20-week growth trial was conducted in flow-through aquarum system to investigate the practical dietary carbohydrate sources for juvenile abalone (Haliotis discus hannai). Four replicate grops of the abalone averaging 0.125g were fed one of eight diets containing 24.2% wheat flour (WF), 20% dextrin (DEX), 20% sucorse (SUC), 10% $^{\alpha}$-potato starch+10% $^{\beta}$-potato starch (ab-S), 15% $^{\alpha}$-potato starch (a-S15), 20% $^{\alpha}$-potato starch (a-S20), 25% $^{\alpha}$-potato starch (a-S25), or mixture (MIX) with practical ingredients such as soybean meal, corn gluten meal, cotton seed meal and heat flour. In addition, these formulated diets were compare with macroalgae such as dried sea mustard Undaria (D-SM) or dried sea tangle Laminaria(D-ST). Survival rate, weight gain, shell growth and soft body weight of abalone were not significantly affected by the different dietary carbohydrate sources (P>0.05), whereas those fed a-S15 diet were slightly low. These values of abalone fed D-ST were lowest (P<0.05), followed by those fed D-SM. Lipid contents of soft body from abalones fed a-S25, D-ST or D-SM were significantly lower than those of abalone fed other diets (P<0.05). These data indicate that abalone can equally utilize any carbohydrate sources used in this study.

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Thermal Conductivity of Compacted Bentonite and Bentonite-Sand Mixture (압축 벤토나이트 및 벤토나이트-모래 혼합물의 열전도도)

  • Cho, Won-Jin;Lee, Jae-Owan;Kwon, Sang-Ki
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.6 no.2
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    • pp.101-109
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    • 2008
  • For the Kyungju bentonite which is considered as a candidate material for the buffer and backfill in the high-level waste repository, the thermal conductivities of compacted bentonite and a bentonite-sand mixture were measured. The thermal conductivities of the compacted bentonites with a dry density of 1.2 to $1.8\;Mg/m^3$ and the bentonite-sand mixture with a dry density of 1.6 and $1.8\;Mg/m^3$ were measured within the gravimetric water content range of 10wt% to 20wt% and the sand fraction range of 10 to 30wt%. The thermal conductivity of compacted bentonite and a bentonite-sand mixture increases with increasing dry density and sand weight fraction in the case of constant water weight fraction, and increases with increasing water weight fraction and sand weight fraction in the case of constant dry density. The empirical correlations to describe the thermal conductivity of compacted bentonite and a bentonite-sand mixture as a function of water fraction at each dry density were suggested. These correlations can predict the thermal conductivities of bentonite and a bentonite-sand mixture with a difference below 10%.

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Low-temperature aging and drying treatments of restorative rice to improve its microbial safety and texture (복원용 밥의 미생물 안전성 및 식감 향상을 위한 저온 숙성 및 건조 처리)

  • Cheon, Hee Soon;Cho, Won-Il;Chung, Myong-Soo;Choi, Jun-Bong
    • Korean Journal of Food Science and Technology
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    • v.51 no.1
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    • pp.29-34
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    • 2019
  • In this study, a commercial production stepwise method for restorative rice with high quality and microbial safety was developed. The stepwise treatment method included steaming, refrigerated aging, and low temperature drying. The soaking rice was steamed twice at $90-100^{\circ}C$, and then, the rice was aged at $0-10^{\circ}C$, frozen at $-20^{\circ}C$, and dried at low temperatures with 5 m/s wind speed at $1-20^{\circ}C$ and 85% relative humidity. Applying the three steps improved sensory qualities compared with the conventional hot air drying and made storage at room temperature for 3 months possible. Specifically, the moisture content of the restorative rice was increased to 30%, which was 4.3 times higher than the 7% of the conventional air dried rice, and the rice grain shape was well maintained. The texture and appearance of the three-step rice were significantly improved (p<0.05) in a sensory evaluation.

The Density and Strength Properties of Lightweight Foamed Concrete Using Stone-Powder Sludge in Hydrothermal Reaction Condition (수열반응 조건에서 석분 슬러지를 사용한 경량 기포 콘크리트의 밀도와 강도 특성)

  • Kim, Jin-Man;Jeong, Ji-Yong;Choi, Se-Jin;Kim, Bong-Joo
    • Journal of the Korea Concrete Institute
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    • v.18 no.5 s.95
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    • pp.687-693
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    • 2006
  • The Stone Powder Sludge(below SPS) is the by-product from the process that translates stone power of 8mm under as crushed fine aggregate. It is the sludge as like cake that has average particle size of $7{\mu}m$, absorbing water content of 20 to 60%, and $SiO_2$ content of 60% over. Because of high water content of SPS, it is not only difficult to handle, transport, and recycle, but also makes worse the economical efficiency due to high energy consuming to drying. This study is aim to recycle SPS as it is without drying. Target product is the lightweight foamed concrete that is made from the slurry mixed with pulverized mineral compounds and foams through hydro-thermal reaction of CaO and $SiO_2$. Although in the commercial lightweight foamed concrete CaO source is the cement and $SiO_2$ source is high purity silica powder with $SiO_2$ of 90%, we tried to use the SPS as $SiO_2$ source. From the experiments with factors such as foam addition rate and replacement proportion of SPS, we find that the lightweight foamed concrete with SPS shows the same trends as the density and strength of lightweight foamed concrete increases according to decrease of foam addition rate. But in the same condition, the lightweight foamed concrete with SPS is superior strength and density to that with high purity silica. This trends is distinguished according to increase of replacement proportion of SPS, also the analysis of XRF shows that the hydro thermal reaction translates SPS to tobermorite. Although SPS has low $SiO_2$ contents, the lightweight foamed concrete with SPS has superior strength and density, because it reacts well with CaO due to extremely fine particles. We conclude that it is possible to replace the high purity silica as SPS in the lightweight foamed concrete experimentally.

Determination of Equivalent Hydraulic Conductivity of Rock Mass Using Three-Dimensional Discontinuity Network (삼차원 불연속면 연결망을 이용한 암반의 등가수리전도도 결정에 대한 연구)

  • 방상혁;전석원;최종근
    • Tunnel and Underground Space
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    • v.13 no.1
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    • pp.52-63
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    • 2003
  • Discontinuities such as faults, fractures and joints in rock mass play the dominant role in the mechanical and hydraulic properties of the rock mass. The key factors that influence on the flow of groundwater are hydraulic and geometric characteristics of discontinuities and their connectivity. In this study, a program that analyzes groundwater flow in the 3D discontinuity network was developed on the assumption that the discontinuity characteristics such as density, trace length, orientation and aperture have particular distribution functions. This program generates discontinuities in a three-dimensional space and analyzes their connectivity and groundwater flow. Due to the limited computing capacity In this study, REV was not exactly determined, but it was inferred to be greater than 25$\times$25$\times$25 ㎥. By calculating the extent of aperture that influences on the groundwater flow, it was found that the discontinuities with the aperture smaller than 30% of the mean aperture had little influence on the groundwater flow. In addition, there was little difference in the equivalent hydraulic conductivity for the the two cases when considering and not considering the boundary effect. It was because the groundwater flow was mostly influenced by the discontinuities with large aperture. Among the parameters considered in this study, the length, aperture, and orientation of discontinuities had the greatest influence on the equivalent hydraulic conductivity of rock mass in their order. In case of existence of a fault in rock mass, elements of the equivalent hydraulic conductivity tensor parallel to the fault fairly increased in their magnitude but those perpendicular to the fault were increased in a very small amount at the first stage and then converged.

플라즈마 표면 처리를 이용한 ZnO 습식성장 패터닝 기술 연구

  • Lee, Jeong-Hwan;Park, Jae-Seong;Park, Seong-Eun;Lee, Dong-Ik;Hwang, Do-Yeon;Kim, Seong-Jin;Sin, Han-Jae;Seo, Chang-Taek
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.330-332
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    • 2013
  • 소 분위기에서 플라즈마 표면 처리의 경우 기판 표면에 존재하는 수소와 탄소 유기물들이 산소와 반응하여 $H_2O$$CO_2$ 등으로 제거되며 표면에 오존 결합을 유도하여 표면 에너지를 증가시키는 것으로 알려져 있다. ZnO 나노구조물을 성장시키는 방법으로는 MOCVD (Metal-Organic Chemical Vapor Deposited), PLD (Pulsed Laser Deposition), VLS (Vapor-Liquid-Solid), Sputtering, 습식화학합성법(Wet Chemical Method) 방법 등이 있다. 그중에서도 습식화학합성법은 쉽게 구성요소를 제어할 수 있고, 저비용 공정과 낮은 온도에서 성장 가능하며 플렉서블 소자에도 적용이 가능하다. 그러므로 본 연구에서는 플라즈마 표면처리에 따라 표면에너지를 변화하여 습식화학합성법으로 성장시킨 ZnO nanorods의 밀도를 제어하고 photolithography 공정 없이 패터닝 가능성을 유 무를 판단하는 연구를 진행하였다. 기판은 Si wafer (100)를 사용하였으며 세척 후 표면에너지 증가를 위한 플라즈마 표면처리를 실시하였다. 분위기 가스는 Ar/$O_2$를 사용하였으며 입력전압 400 W에서 0, 5, 10, 15, 60초 동안 각각 실시하였다. ZnO nanorods의 seed layer를 도포하기 위하여 Zinc acetate dehydrate [Zn $(CH_3COO)_2{\cdot}2H_2O$, 0.03 M]를 ethanol 50 ml에 용해시킨 후 스핀코팅기를 이용하여 850 RPM, 15초로 5회 실시하였으며 $80^{\circ}C$에서 5분간 건조하였다. ZnO rods의 성장은 Zinc nitrate hexahydrate [$Zn(NO_3)_2{\cdot}6H_2O$, 0.025M], HMT [$C6H_{12}N_4$, 0.025M]를 deionized water 250 ml에 용해시켜 hotplate에 올리고 $300^{\circ}C$에서 녹인 후 $200^{\circ}C$에서 3시간 성장시켰다. ZnO nanorods의 성장 공정은(Fig. 1)과 같다. 먼저 플라즈마 처리한 시편의 표면에너지 측정을 위해 접촉각 측정 장치[KRUSS, DSA100]를 이용하였다. 그 결과 0, 5, 10, 15, 60 초로 플라즈마 표면 처리했던 시편이 각각 Fig. l, 2와 같이 $79^{\circ}$, $43^{\circ}$, $11^{\circ}$, $6^{\circ}$, $7.8^{\circ}$로 측정되었으며 이것을 각각 습식화학합성법으로 ZnO nanorods를 성장 시켰을 때 Fig. 3과 같이 밀도 차이를 확인할 수 있었다. 이러한 결과를 바탕으로 기판의 표면에너지를 제어하여 Fig. 4와 같이 나타나며 photolithography 공정없이 ZnO nanorods를 패터닝을 할 수 있었다. 본 연구에서는 플라즈마 표면 처리를 통하여 표면에너지의 변화를 제어함으로써 ZnO nanorods 성장의 밀도 차이를 나타냈었다. 이러한 저비용, 저온 공정으로 $O_2$, CO, $H_2$, $H_2O$와 같은 다양한 화학종에 반응하는 ZnO를 이용한 플렉시블 화학센서에 응용 및 사용될 수 있고, 플렉시블 디스플레이 및 3D 디스플레이 소자에 활용 가능하다.

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