• Plant Journal
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• v.9 no.4
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• pp.31-36
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• 2013

In order to extend a hot gas parts replacement cycle of a gas turbine, blade row 1 from low pressure turbine, which has a significant impact on the cycle, has been selected from stored set after one cycle use. Taking into account the status of the first stage moving blade in LP turbine operated more than 27,000 equivalent operating hours(EOH) and the replacement cycle in the same type of gas turbine, the replacement of the high temperature components installed on the GT, a study subject, can be extended from 24,000 to 27,000 EOH.

• Journal of the Korean Society of Propulsion Engineers
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• v.26 no.1
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• pp.1-11
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• 2022

In a gas turbine, fuel is exposed to a high temperature environment until it is fed to the combustor through the injector. Hydrocarbon fuels can coke under high temperature conditions, which can cause coking material to deposit on fuel lines or block the injector passages. In this study, a specimen simulating a fuel line located inside a gas turbine and Jet A-1 were heated using electric devices. Jet A-1 coking tests were performed by changing the wall temperature of the stainless steel specimen and the temperature of Jet A-1 supplied to the specimen. After the coked specimens were cut, the coking material and the inner surface were analyzed using an energy dispersive X-ray spectrometer and a field emission scanning electron microscope.

• Journal of the Korean Institute of Gas
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• v.17 no.5
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• pp.64-68
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• 2013

Non destructive testing(NDT) methods of electrofusion(EF) joints of thermoplastics pipes are required for fusion joint safety and for the long term reliability of a pipe system. Electrofusion joints, which are joined at the proper fusion process and procedures, may encounter defects due to the difference of ovality between pipes and coupling, improper fusion process or porosity result from electrofusion joining. These defects can cause the failure of pipeline and by extension, they can be caused the limit to expand the use of plastics pipes. This paper studies inspection results using ultrasonic imaging method for damaged polyethylene electrofusion joints. Gas was leaking from 250mm diameter polyethylene electrofusion joints at February 2004 which was electrofused at December 1994 and operation pressure was 2.45kPa. First, surface inspection was conducted and then in order to find the types of defects examination using ultrasonic imaging method was performed. Lack of fusion and inappropriate inserting for polyethylene pipes into electrofusion coupling were found and causes of the gas leak were judged that misalignment and insert defect. Cutting inspection was performed and each inspection results were compared to. Results of ultrasonic imaging method and cutting inspection were the same.

• Journal of the Korean Institute of Gas
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• v.20 no.3
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• pp.73-77
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• 2016

This paper presents the displacement behavior safety of hollow shafts with an equivalent volume for various cross sectional area using a finite element method. The FEM results indicate that the hollow shafts with X-type or Y-type columns between outer tube, middle tube and inner tube may reduce a maximum displacement at the middle length of hollow shafts. Especially, the load-bearing column of X-type or Y-type hollow shaft is directly connected between outer tube and inner tube without a shift for reducing the vertical displacement. And increased thickness of a load-bearing column is recommended for reducing the vertical displacement and increasing the displacement behavior safety for an equivalent volume of a hollow shaft.

• Journal of the Korean Vacuum Society
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• v.11 no.1
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• pp.16-21
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• 2002

Selective epitaxial growth(SEG) of silicon were performed at low temperature under an ultraclean environment below $1000^{\circ}C$ using ultraclean $Si_2H_6$ and $H_2$ gases ambient in low pressure chemical vapor deposition(LPCVD). As a result of ultraclean processing, epitaxial Si layers with good quality were obtained for uniform and SEG wafer at temperatures range 600~$710^{\circ}C$ and an incubation period of Si deposition only on $SiO_2$ was found. Low-temperature Si selectivity deposition condition and epitaxy on Si were achieved without addition of HCl. The epitaxial layer was found to be thicker than the poly layer deposited over the oxide. Incubation period prolonged for 20~30 sec can be obtained by $O_2$addition. The surface morphologies & cross sections of the deposited films were observed with SEM, The structure of the Si films was evaluated XRD.

• Journal of the Korean Institute of Gas
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• v.20 no.4
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• pp.33-43
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• 2016

Grinding, weld deposition, type A sleeve, type B sleeve, composite sleeve, hot tapping and clamp are used as the method to repair the buried pipelines in the United States, UK and Europe. In the event of defect to the pipeline, they have repaired the pipeline through the fitness-for-service assessments. In addition, they have guidelines for the possible repair methods to apply to each type of damage, which is occurred due to the 3rd party construction or corrosion. According to the KGS FS551, Safety Validation in Detail including ECDA(External Corrosion Direct Assessment) as one method of integrity management should be carried out for the old pipeline which supply natural gas as the middle pressure in Korea. Where a defect on the pipelines is found, on the result of Safety Validation in Detail, the pipelines should be repaired or replaced by new piping. However, there are no guidelines or regulations regarding the repair and reinforcement of pipeline, so that, cutting the damaged pipeline and replacing it as a segment of new pipe is the only way in Korea until now. We have suggested pipeline repair methods including type A, B sleeve, composite sleeve, after the survey of foreign repair method and standards including the method of United States and the United Kingdom, and after analysis of the results on pipeline repair test including type A, type B sleeve and composite sleeve.

• Fire Science and Engineering
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• v.18 no.2
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• pp.20-26
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• 2004

The purpose of this study is to investigate the transition mechanism and prevention mechanism of gas explosion to fire. Transition phenomena of explosion to fire of LPG in the explosion vessel of its size of TEX>$100 cm {\times} 60 cm {\times} 45 cm$ was visualized using the high speed video camera and the mechanism was analysed from the videograph. Newspaper size of $30cm {\times} 20cm$ was used for combustible sample in this experiments and LPG-air mixture was ignited by 10 ㎸ electric spark. Experimental parameter was gas concentration, size of vent area and position of combustible solid. Size of vent area were varied as $10cm {\times} 9cm, 13cm {\times} 10cm, 27cm {\times} 20cm, 40cm {\times} 27cm$, and the position of combustible was varied in 4 point. Carbon dioxide was used to study the prevention mechanism of explosion to fire transition of LPG. Based on this experiment we can find that transition possibility of explosion to fire on solid combustible from explosion is depends on concentration of LPG-air mixture and the exposure time of solid combustibles in high temperature atmosphere of flame and burnt gas. And cooling or inerting of the atmosphere after explosion can be prevent the transition of explosion to fire on solid combustibles from gas explosion.

• Proceedings of the Materials Research Society of Korea Conference
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• 2009.05a
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• pp.39.1-39.1
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• 2009

본 실험은 연성과 광 투명도가 뛰어난 아크릴 (PMMA) 과 폴리카보네이트 (Polycabonate) 기판의 축전 결합형 플라즈마 (CCP) 건식 식각 연구에 관한 것이다. 특히 식각 반응기 내부의 압력 변화에 따른 두 기판의 건식 식각 특성 분석에 초점을 맞추었다. 실험에 사용된 기판은 두께 1mm의 아크릴 (PMMA) 과 폴리카보네이트 (Polycabonate)를 $1.5\times1.5\;cm^2$로 절단하여 Photo-lithography 공정을 통하여 감광제 (Photo-resist)로 패턴하였다. 식각 반응기 내부에 패턴 된 아크릴(PMMA) 과 폴리카보네이트 (Polycabonate)를 넣은 후 반응기 내부 진공 상태로 만들었다. 그 후 5 sccm $O_2$ 가스를 유량조절기 (Mass flow controller)를 통하여 식각 반응기 내부로 유입하여 실험을 하였다. 이때 식각 공정 변수는 식각 반응기 내부 압력과 샘플 척 파워이다. 특성평가 항목은 식각 후 기판 (Substrate)의 식각율 (Etch rate), 식각 선택비 (Selectivity) 그리고 기판 표면 거칠기 (RMS roughness)이다. 실험 결과는 표면 단차 분석기(Surface profiler)를 이용하여 기판 (Substrate)의 표면을 분석 하였다. 또한 OES (Optical Emission Spectroscopy) 를 이용하여 식각 중 내부 플라즈마의 상태를 분석하였다. 본 실험 결과에 따르면 5 sccm $O_2$ 가스와 100 W 척 파워를 고정한 후 반응기 내부의 압력을 25 mTorr에서 180 mTorr까지 변화시켜 실험한 결과 40 mTorr의 반응기 내부 압력에서 실험 자료 중 가장 높은 식각율로 아크릴 (PMMA)은 $0.46\;{\mu}m/min$, 폴리카보네이트 (Polycabonate)는 $0.28\;{\mu}m/min$의 결과를 얻었다. 또한 이 자료를 바탕으로 5 sccm $O_2$ 가스와 반응기 내부 압력을 40 mTorr로 고정시키고 RIE 척 파워를 25 W에서 150 W로 증가시켰을 때 아크릴 (PMMA)의 식각율은 $0.15\;{\mu}m/min$에서 $0.72\;{\mu}m/min$까지 증가하였고, 폴리카보네이트 (Polycabonate) 의 식각율은 $0.1\;{\mu}m/min$에서 $0.36\;{\mu}m/min$까지 증가하였다.

• Proceedings of the Korean Vacuum Society Conference
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• 2015.08a
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• pp.93.2-93.2
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• 2015

플라즈마를 포함한 반응성 가스 공정 분석용 사중극자 질량분석기의 필라멘트의 파손양상을 조사하였다. 또한 유전체 증착층이 이온원 성능에 미치는 영향을 분석하기 위하여 이온원의 일반적인 가동 전압 조건에서 Poisson방정식을 이용하여 전위를 수치 해석으로 구하였다. 사용중 파손된 필라멘트의 파단면을 주사전자현미경으로 관찰결과, 수직으로 절단되는 양상과 직경이 점차 작아지면서 erosion되는 두가지 양상을 보였다. 또한 파단면은 표면균열과 패시팅(faceting) 현상을 보였다. 필라멘트 사용시 가장 큰 문제는 패시팅(faceting)이다. 대부분의 결정에서는 다른 결정면보다 에너지 준위가 낮은 결정면이 존재한다. W 원자는 고온에서 확산 또는 증발하여 표면에서 다시 응축할 때 표면 에너지를 최소화하기 위한 독특한 평형 형상이 만들어 지는데 이것이 패시팅의 구동력이다. 이때 국부적으로 단면적이 감소하는 곳이 생기는데, 이 지점이 집중적으로 가열되고 증발이 가속화하여 파손된다. 파단면을 EDS 분석결과, 산화물을 포함한 F, Fe 및 C이 검출되었다. 이 F과 C는 공정중 사용된 CF4의 분해에 의한 것으로 생각되며, 파손된 필라멘트를 Ar 유도결합 플라즈마로 처리한 결과 이 F, Fe 및 C의 양이 감소하였다.

• Proceedings of the Korean Institute of Resources Recycling Conference
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• 2005.10a
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• pp.308-313
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• 2005

실리콘 잉고트의 절단공정에서 발생하는 폐실리콘 슬러지는 실리콘과 실리콘카바이드 등의 유가자원이 함유되어 있으며, 이 중 실리콘 분말은 실리콘 화합물인 알콕시실란 등을 제조하는데 원료로 사용이 가능하다. 본 연구에서는 폐실리콘 슬러지로부터 분리, 합성된 사에 톡시실란(TEOS)을 원료로 이용하여 실리카 나노분말을 합성하였다. TEOS 원료물질을 외부 혼합형 이류체 노즐을 이용하여 미세액적으로 분무하고 화염 속으로 도입시키고 화염열분해 반응을 진행시켜 실리카 나노분말을 합성하였다. 합성된 실리카 나노입자의 특성은 투과형 전자현미경 및 BET에 의하여 입자형상 및 평균 입자크기가 분석되었다. 주요 공정변수인 분산공기의 압력, 반응가스의 조성을 변화시켜 실험한 결과 평균크기가 $9{\sim}68nm$인 실리카 나노분말을 제조하였다.