• Title/Summary/Keyword: $Al/Al_2O_3$ composite

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A Study on the Machinability and Machining properties of Composite Ceramics$(iC-Al_2O_3)$ by EDM (복합 세라믹스$(iC-Al_2O_3)$의 방전가공특성에 관한 연구)

  • 윤병주
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.4 no.4
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    • pp.61-68
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    • 1995
  • TiC-Al2O3 composite ceramics has high hardness, high strength, high wear and corrosion resistance. Therefore, composite ceramics have been concerned significantly with some excellent properties and many functions as new industrial materials to the industry at large. In present research, experiments are carried out to obtain the machinability and machining properties by EDM. As a result, the most suitable machining conditions of TiC-Al2O3 composite ceramics was that the pulse duration is 10-60$mutextrm{s}$, the peak current is 10-16A. The machining speed and the wear of the tool electrode increased with the increase in peak current.

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Effect of Plating Parameters on the Electrodeposition of Ni-alumina Nanocomposite

  • Gyawalia, Gobinda;Woo, Dong-Jin;Lee, Soo-Wohn
    • Journal of Surface Science and Engineering
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    • v.43 no.4
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    • pp.165-169
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    • 2010
  • $Ni-Al_2O_3$ nanocomposite coatings were fabricated by conventional electrodeposition technique using nickel sulfamate bath. Effect of plating parameters on electrodeposition of $Ni-Al_2O_3$ nanocomposite were studied. The properties of the nano composite were investigated by using SEM, XRD, and Vicker's microhardness test. The results demonstrated that $Al_2O_3$ incorporation in the composite coatings was found to be increased by increasing stir rate and $Al_2O_3$ content in plating bath. Microhardness of the composite coatings was also increased with increasing content of the nano particles in the plating bath. The surface morphologies of the nanocomposite coatings were found to be varied with varying pH, current densities as well as alumina content in the plating bath.

Synthesis and Characterization of CNTs/Metal/Al2O3 Nanocomposite Powders by Thermal CVD (열 CVD법에 의한 CNTs/Metal/Al2O3 나노복합분말의 합성 및 특성)

  • Choa Yong-Ho;Yoo Seung-Hwa;Yang Jae-Kyo;Oh Sung-Tag;Kang Sung-Goon
    • Journal of Powder Materials
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    • v.12 no.2 s.49
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    • pp.146-150
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    • 2005
  • An optimum route to synthesize $Al_2O_3$-based composite powders with homogeneous dispersion of carbon nanotubes (CNTs) was investigated. CNTs/Metal/$Al_2O_3$ nanocomposite powders were fabricated by thermal chemical vapor deposition of $C_2H_2$ gas over metal/$Al_2O_3$ nanocomposite catalyst prepared by selective reduction of metal oxide/$Al_2O_3$ powders. The FT-Raman spectroscopy analysis revealed that the CNTs have single- and multi-walled structure. The CNTs with the diameter of 25-43 nm were homogeneously distributed in the metal/$Al_2O_3$ powders, and their characteristics were strongly affected by a kind of metal catalyst and catalyst size. The experimental results show that the composite powder with required size and dispersion of CNTs can be realized by control of synthesis condition.

Synthesis and Properties of $Al_2$$O_3$-$TiO_2$Composites by Wet Method -1. Synthesis of $Al_2$$O_3$-$TiO_2$Composite Powders- (습식법에 의한 $Al_2$$O_3$-$TiO_2$복합체의 합성 및 특성연구 -1. $Al_2$$O_3$-$TiO_2$계 복합분체의 합성(1)-)

  • 류수착;엄지영
    • Journal of the Korean Ceramic Society
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    • v.38 no.5
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    • pp.412-417
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    • 2001
  • 본 연구는 습식법으로 수산화 알루미늄과 티타니아를 출발물질로 하여 $Al_2$O$_3$-TiO$_2$복합분체를 제조하였으며, 2 mol의 Al(OH)$_3$분말에 대하여 TiO$_2$분말량을 1, 3, 5, 7, 9, 11 wt%로 첨가하여 $Al_2$O$_3$-TiO$_2$복합분체의 특성을 조사하였다. 제조된 $Al_2$O$_3$-TiO$_2$계 복합분체는 $700^{\circ}C$~140$0^{\circ}C$까지 하소하여 XRD 분석을 한 결과 100$0^{\circ}C$까지는 TiO$_2$(rutile)상과 η-Al$_2$O$_3$상이 공존하다가 110$0^{\circ}C$부터 130$0^{\circ}C$까지는 η-Al$_2$O$_3$에서 $\alpha$-Al$_2$O$_3$로의 상전이가 일어나서 $\alpha$-Al$_2$O$_3$상과 TiO$_2$(rutile)상이 나타났으며 하소온도 140$0^{\circ}C$, TiO$_2$첨가량이 5 wt%일 때부터 $Al_2$TiO$_{5}$가 생성되기 시작하였다. TiO$_2$첨가량에 따른 비표면적값은 첨가량이 7 wt%까지는 감소하였으나 그 이상 첨가시 증가하였다. 입도분석 결과 평균입경은 15.74~23.21$mu extrm{m}$로서 TiO$_2$첨가량이 3 wt%일 때 가장 작은 값을 가졌으며 TiO$_2$첨가량은 5 wt% 이상부터 점차 감소하였다.

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Thermal Stability and Fracture Toughness of Epoxy Resins Modified with Epoxidized Castor Oil and Al2O3 Nanoparticles

  • Zhu, Lin;Jin, Fan-Long;Park, Soo-Jin
    • Bulletin of the Korean Chemical Society
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    • v.33 no.8
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    • pp.2513-2516
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    • 2012
  • This study examined the effects of the epoxidized castor oil (ECO) and $Al_2O_3$ content on the thermal stability and fracture toughness of the diglycidylether of bisphenol-A (DGEBA)/ECO/$Al_2O_3$ ternary composites using a range of techniques. The thermal stability of the composites was decreased by the addition of ECO and $Al_2O_3$ nanoparticles. The fracture toughness of the composites was improved significantly by the addition of ECO and $Al_2O_3$ nanoparticles. The composite containing 3 wt % $Al_2O_3$ nanoparticles showed the maximum flexural strength. Scanning electron microscopy (SEM) revealed tortuous cracks in the DGEBA/ECO/$Al_2O_3$ composites, which prevented deformation and crack propagation.

Mechanical Properties and Fabrication of Nanostructured 1.5TiAl-Al2O3 Composite by Pulsed Current Activated Sintering (기계적 합성된 분말로부터 펄스전류활성 소결에 의한 나노구조 1.5TiAl-Al2O3 복합재료 제조 및 기계적 특성)

  • Kim, Won-Baek;Wang, Hee-Ji;Roh, Ki-Min;Cho, Sung-Wook;Lim, Jae-Won;Shon, In-Jin
    • Korean Journal of Metals and Materials
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    • v.50 no.4
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    • pp.310-315
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    • 2012
  • Nano-powders of 1.5TiAl and $Al_2O_3$ were synthesized from $1.5TiO_2$ and 3Al powders by high energy ball milling. Nanocrystalline $Al_2O_3$ reinforced composite was consolidated by pulsed current activated sintering within 2 minutes from mechanochemically synthesized powders of $Al_2O_3$ and 1.5TiAl. The relative density of the composite was 99.5%. The average hardness and fracture toughness values obtained were $1250kg/mm^2$ and $10MPa{\cdot}m^{1/2}$, respectively.

Preparation of B4C-Al2O3 Composite Powder by Self-propagation High-temperature Synthesis(SHS) Process under High Pressure (고압 자전 고온반응 합성법에 의한 B4C-Al2O3복합분말 제조)

  • 임경란;강덕일;김창삼
    • Journal of the Korean Ceramic Society
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    • v.40 no.1
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    • pp.18-23
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    • 2003
  • Composite powder of$B_4C-A1_2O_3$was prepared from a mixed powder of$B_2O_3/A1/C$by SHS under argon pressure instead of using a chemical furnace. A mixture of$B_2O_3,$Al and C powder (equivalent amounts to the reaction,$2B_2O_3+4A1+C=B_4C+2A1_2O_3)$was ball milled for 2 h. The mixed powder was placed in a SHS reactor and filled with 10 atm of argon gas and ignited. The inner and outer products were the same by XRD analysis. It was consisted of a composite powder of$B_4C-A1_2O_3$without $AlB_{12}/C_2$which was always produced using a chemical furnace. The composite powder was about$60~100{mu}m$size which was composed of crystalline particles of about 0.3~l${mu}m$size. But when 15 atm of argon was employed, partial sintering took place to give rise hard composite powder of$15~25{mu}m$$B_4C$with $0.1~0.2{mu}m$$A1_2O_3.$

A Study on CH4-SCR Reaction Characteristics of Mg-added Composite Alumina Pt Catalysts (Mg이 첨가된 복합 알루미나 Pt촉매의 CH4-SCR 반응특성에 관한 연구)

  • Won, Jong Min;Hong, Sung Chang
    • Applied Chemistry for Engineering
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    • v.28 no.1
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    • pp.87-94
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    • 2017
  • In this study, a catalyst based on $Pt/Al_2O_3$ supported on Mg was prepared by a wet impregnation method to investigate the $CH_4-SCR$ reaction characteristics of various alumina supports. Alumina supported on $Pt/Al_2O_3$ catalyst was converted to an $Al_2O_3$ composite, and when Mg was added, oxygen species of the active metal Pt were controlled due to electrophobic characteristics. Oxygen-controlled Pt used as a reducing agent inhibited the oxidation of $CH_4$ to $CO_2$. The addition of Mg also promoted the adsorption of NO species and the conversion of NO to $NO_2$ due to the NOx storage property on the catalyst surface.

Rapid Sintering and Synthesis of Nanostuctured FeCrAlSi-Al2O3 Composite by High-Frequency Induction Heating (고주파유도 가열에 의한 나노구조의 FeCrAlSi-Al2O3 복합재료의 합성 및 급속소결)

  • Du, Song Lee;Cho, Sung-Hun;Ko, In-Yong;Doh, Jung-Mann;Yoon, Jin-Kook;Park, Sang-Whan;Shon, In-Jin
    • Korean Journal of Metals and Materials
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    • v.49 no.3
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    • pp.231-236
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    • 2011
  • Nanopowder of $Fe_2O_3$, Al, Cr and Si was fabricated by high energy ball milling. A dense nanostuctured $A_2O_3$ and $6.06Fe_{0.33}Cr_{0.16}Al_{0.23}Si_{0.29}$ composite was simultaneously synthesized and consolidated using high frequency induction heated sintering method within 1 minute from mechanically activated powders of $Fe_2O_3$, Al, Cr and Si. The grain sizes of $Al_2O_3$ and $Fe_{0.33}Cr_{0.16}Al_{0.23}Si_{0.29}$ in composite are 80 and 18 nm, respectively.