• 제목/요약/키워드: $2^{nd}$ step(T2)

검색결과 28건 처리시간 0.027초

3단계 막효소반응기에서 연속적으로 생산된 어피 및 우피 젤라틴 가수분해물의 항산화활성 비교 (Comparison of Antioxidative Activity on Fish and Bovine Skin Gelatin Hydrolysates Produced in a Three-Step Membrane Enzyme Reactor)

  • 김세권;박표잠;송병권;김종배
    • KSBB Journal
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    • 제15권6호
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    • pp.635-643
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    • 2000
  • To compare the antioxidative activities of fish skin and bovine skin gelatin hydrolysate, gelatin hydrolysates from Alaska pollack and bovine skin were prepared by various enzymatic hydrolysis methods (1st step, Alcalase; 2nd step, pronase E; 3rd step, collagenase) using a continuous three-step membrane reactor. The molecular weight distributions of the 1st, 2nd and 3rd step hydrolysates were 7∼10 kDa, 2∼5 kDa and 0.7∼0.9 kDa, respectively. The antioxidative activity of fish skin gelatin hydrolysate was stronger than that of bovine skin gelatin hydrolysate, and in particular, both of 2nd step hydrolysates showed more antioxidative activity than hydrolysates of any other step. The optimum antioxidative activity concentration of the 2nd step hydeolysates of fish and boving skin were 1% (w/w) in a linoleic acid water-alcohol emulsion. In cultured cells exposed to t-butyl hydroperoxide (t-BHP), the 2nd step hydrolysate of fish skin gelatin delayed cell death most. These results suggest that the antioxidative activity of fish skin gelatin hydrolysate is higher than that of bovine skin gelatin hydrolysate because of their different amino acid contents.

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대보-구룡포-감포 지역의 해안단구(II) (Marine Terrace of Daebo-Guryongpo-Gampo, SE Korea(II))

  • 최성자
    • 자원환경지질
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    • 제37권2호
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    • pp.245-253
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    • 2004
  • 우리나라 남동해안의 대보-감포간 해안단구는 6개의 단구면으로 분류되며 이들은 각각 하위로부터 1단구(T1,0.5m), 2단구(T2, 10m), 3단구(T3, 30m), 4단구(T4, 40m), 5단구(T5, 60m), 6단구(T6, 75m)이다. 이가운데 3단구(T3)는 두개의 단구로 분류되며, 하위면을 T3b, 상위면을 T3a 정하였다. 3단구 하위면 (T3b)의 구정선을 보여주는 해식애의 발달이 뚜렷하지 않아 단구 세분이 어려운 곳은 통합하여 3단구(T3)로 정하였다. 단구형성시기를 직접적으로 지시해주는 화석은 없으나, 2단구의 퇴적층에서 OSL 연대 자료가 다량 도출되어 있으며, 이 자료를 통하여 단구 형성시기를 정할 수 있다. 2단구(T2) 퇴적층의 OSL 연대는 60-7Oka에 수렴하고 있어, 2단구의 형성시기는 MIS(산소동위원소에 의한 시대 분류)의 5a로. 추정할 수 있다. 따라서 3단구는 MIS 5e, 4단구는 MIS 7에 대비된다. 본 연구지역에서 MIS 5e인 3단구 상위면(T3a)은 현해수면으로부터 30m높게 융기되어 있으며, 따라서 이지역의 융기율은 약 0.19m/ka로 계산된다. 이와 같은 융기율은 국지적인 지구조운동에 기인한 것으로 해석되며, 이에 대한 추가 연구가 필요하다.

7050 Al 합금의 RRA 처리에 관한 연구 (A Study on the RRA(Retrogression and Reaging) treatment of 7050 Al alloy)

  • 최중환;김장량;이상래;김인배
    • 한국재료학회지
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    • 제10권7호
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    • pp.493-498
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    • 2000
  • 7050 AI합금을 RRA 처리하였을 때 경도, 전기전도도 및 미세조직의 변화를 조사하였다. 120도씨에서 24시간 동안 1차 시효처리한 후 175도씨에서 2차 퇴화처리하였을 때 경도값의 변화는 초기에 감소하다가 피크 경도를 보인 다음 다시 감소하였으며, 3차 재시효처리재가 2차 시효처리재 보다 큰 경도값을 나타내었다. 2차 퇴화처리시 초기 경도 감소는 T6의 주 강화상인 GP zone의 부분적인 분해에 의한 것이며, 3차 재시효 처리하였을 때 강화상은 GP zone과 파이상이었다. 120도씨에서 24시간 동안 1차 시효처리한 후 175도씨에서 2차 퇴화처리하였을 때 전기전도도 변화는 퇴화 쵤부터 연속적으로 증가혀였으며, 3차 재시효처리에 의해 2차 퇴화처리시 보다 %IACS가 0.5 ~ 2.7 증가하였다. 3단시효에 의해 T6정도의 강도를 유지하면서 38%IACS값 이상의 전기전도도를 얻을 수 있는 최적 퇴화처리 조건은 $175^{\circ}C$ 50분이었다. 이는 퇴화처리 경도곡선의 극소점 또는 극대점과 무관하며 오히려 약간 과시효 조건이다.

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Effect of 1,3-Diphenyl-guanidine (DPG) Mixing Step on the Properties of SSBR-silica Compounds

  • Lim, Seok-Hwan;Lee, Sangdae;Lee, Noori;Ahn, Byeong Kyu;Park, Nam;Kim, Wonho
    • Elastomers and Composites
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    • 제51권2호
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    • pp.81-92
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    • 2016
  • 1,3-Diphenylguanidine (DPG) is commonly used as a secondary accelerator which not only acts as booster of cure but also activating silanization reaction. The aim of this study is to increase the interaction between silica and rubber by using DPG. In this study, mixing was proceeded in two steps. The T-1 compound is mixed DPG with silica and silane coupling agent in the kneader at high temperature which is named as $1^{st}$ mixing step. T-3 compound is mixed DPG with curatives in the two-roll mill at low temperature which is named as $2^{nd}$ mixing step. The T-2 compound is mixed a half of DPG in $1^{st}$ mixing step and the remainder is mixed in $2^{nd}$ mixing step. Total DPG content was equal for all compounds. When DPG is mixed with silica, silane coupling agent during the $1^{st}$ mixing step, a decrease in cure rate and an increase in scorch time can be seen. This indicates that DPG is adsorbed on the surface of silica. during rubber processing. However, bound rubber content is increased and dynamic properties are improved. These results are due to the highly accelerated silanization reaction. However, there are no significant difference in 100%, 300% modulus.

Fabrication of Nd-Substituted Bi4Ti3O12 Thin Films by Metal Organic Chemical Vapor Deposition and Their Ferroelectrical Characterization

  • Kim, Hyoeng-Ki;Kang, Dong-Kyun;Kim, Byong-Ho
    • 한국세라믹학회지
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    • 제42권4호
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    • pp.219-223
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    • 2005
  • A promising capacitor, which has conformable step coverage and good uniformity of thickness and composition, is needed to manufacture high-density non-volatile FeRAM capacitors with a stacked cell structure. In this study, ferroelectric $Bi_{3.61}Nd_{0.39}Ti_3O_{12}$ (BNdT) thin films were prepared on $Pt(111)/TiO_2/SiO_2/Si$ substrates by the liquid delivery system MOCVD method. In these experiments, $Bi(ph)_{3}$, $Nd(TMHD)\_{3}$ and $Ti(O^iPr)_{2}(TMHD)_{2}$ were used as the precursors and were dissolved in n-butyl acetate. The BNdT thin films were deposited at a substrate temperature and reactor pressure of approximately $600^{\circ}C$ and 4.8 Torr, respectively. The microstructure of the layered perovskite phase was observed by XRD and SEM. The remanent polarization value (2Pr) of the BNdT thin film was $31.67\;{\mu}C/cm^{2}$ at an applied voltage of 5 V.

HD 처리 및 열처리공정 개선에 의한 (Nd, Dy)-Fe-B 소결자석의 자기특성 향상 (Improvement of the Magnetic Properties of (Nd, Dy)-Fe-B Sintered Magnets by Modification of HD and Annealing Processes)

  • 남궁석;이연호;김문갑;장태석
    • 한국분말재료학회지
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    • 제17권5호
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    • pp.359-364
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    • 2010
  • In an attempt to optimize the magnetic properties of (Nd, Dy)-Fe-B sintered magnets, hydrogenation and post-sintering heat treatment processes were investigated at various hydrogenation temperatures and heat treatment temperatures. The coercivity of (Nd, Dy)-Fe-B sintered magnets hydrogenated at $400^{\circ}C$ increased to about 1.2 kOe without any detrimental effect on the remanence. Moreover, the coercivity of the magnets was enhanced further by a consecutive $2^{nd}$ and $3^{rd}$ step heat treatment. These results eventually leaded to the reduction of the Dy content in a high coercive (> 30 kOe) (Nd, Dy)-Fe-B sintered magnets, as much as 10%.

단계별(段階別) 가압(加壓)에 따른 좌관부위(左關部位) 맥파(脈波) 변화(變化) (A Study on the Waveform Analysis of Left KWAN Pulse Dignosis by the Pressure)

  • 김경철;이정원;류경호;김종환;박주연
    • 대한한의진단학회지
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    • 제13권1호
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    • pp.19-35
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    • 2009
  • Objectives : In the study on the waveform analysis of radial artery pulse diagnosis, we need to establish fundamentals of contemporary pulse diagnosis research. To achieve certain experimental basis on traditional pulse diagnosis, we have to research the differences of pulse waveform according to pressure (in 5 level) and position (Chon, Gwan, Cheok in radial artery). As a first step, in present thesis, we tried to find the differences of pulse waveform according to pressure. Methods and Results : In this research, we analyzed seven parameters of the waveform at five levels of pressure. The parameters are E(so called 'energy', a representative of pulse strength), h1(height of percussion wave) and h2(height of subincisura). The results were as follows. 1. When we analyzed the change of the waveform according to pressure in the left Gwan, E, hl, h2 and A differed between 1st and 2nd grade, between 1st and 3rd grade, between 1st and 4th grade, between 1st and 5th grade, between 2nd and 3rd grade, between 2nd and 5th grade, between 3rd and 5th grade and between 4th and 5th grade in 95% confidence interval. 2. And t2, t4 differed between 1st and 2nd grade, between 1st and 5th grade, between 2nd and 4th grade, between 2nd and 4th grade, between 2nd and 5th grade, between 3rd and 4th grade, between 3rd and 5th grade and between 4th and 5th grade in 95% confidence interval. 3. W differed between 1st and 3rd grade, between 1st and 4th grade, between 2nd and 3rd grade, between 2nd and 4th grade, between 2nd and 5th grade, between 3rd and 4th grade, between 3rd and 5th grade, and between 4th and 5th grade in 95% confidence interval. 4. And h2/h1 differed between 1st and 4th grade, between 1st and 5th grade, between 2nd and 4th grade, between 2nd and 5th grade, between 3rd and 4th grade & between 3rd and 5th grade in 95% confidence interval. 5. There were differences between 1st and 2nd grade & between 2nd and 5th grade in the case of t4/t2 in 95% confidence interval. And there were differences between 1st and 5th grade, between 3rd and 4th grade, between 3rd and 5th grade & between 4th and 5th grade in the case of W/A in 95% confidence interval. And were differences between 1st and 2nd grade, between 2nd and 3rd grade, between 2nd and 4th grade, between 3rd and 4th grade, between 3rd and 5th grade & between 4th and 5th grade in the case of A/E in 95% confidence interval. Conclusions : As mentioned above, we conclude that the waveform analysis according to five grade pressure in the left Gwan shows the difference of waveform in each grade pressure.

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Influence of Roller Speed on Magnetic Properties and Structures of α-Fe/Nd2Fe14B Nanocomposite Magnets Prepared by Melt-spinning

  • Pei, Wenli;Lian, Fazeng;Fu, Meng;Zhou, Guiqin;Takahashi, M.
    • Journal of Magnetics
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    • 제9권4호
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    • pp.101-104
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    • 2004
  • The crystallization behaviours of nanocomposite made by a function of quenching rate (roller speed) were studied. The results showed that there was one step c$\mathbb{r}$ystallization process for the alloy quenched at roller speed of 32 m/s, which could be shown as, Am (amorphouse) + ${\alpha}-Fe/Nd_2Fe_{14}B$ ${\rightarrow}$ ${\alpha}-Fe/Nd_2Fe_{14}B$ . For the alloy quenched at roller speed of 40 m/s, there was steps crystallization process taking place at different temperatures, which could be shown as, Am ${\rightarrow}$ ${\alpha}-Fe/Nd_2Fe_{23}B_3+Nd_2Fe_{14}B+Am`$ ${\rightarrow}$ ${\alpha}-Fe/Nd_2Fe_{14}B$. The presence of transition phase ($Nd_2Fe_{23}B_3$) was harmful to get fine and uniform grain size during crystallization process. Uniform microstructures and high magnetic properties could be attained for the as-quenched alloy containing less amorphous phase and no presence of transition phase during annealing treatment. For the alloy prepared at roller speed of 32 m/s, the following properties were obtained, $B_r= 0.904 T,_iH_c = 801 kA/m, (BH)_{max} = 122 kJ/m^3 and M_r/M_s = 0.6$.

7050Al 합금의 열처리공정 개발에 관한 연구 (A study on the heat treatment processing of 7050 aluminum alloy)

  • 이효수;남태운;이병권
    • 열처리공학회지
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    • 제9권2호
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    • pp.139-146
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    • 1996
  • The aero-industry is union industry which includes a research development type, a knowledge accumulation type and a developed country type. The aero-industry of Korea is in semi-developed type stage but departed later than that of other country such as Taiwan, Indonesia etc. Therefore, the necessity of domestic airplane material is required. This study on 7050Al extruded alloy aims to suggest an adequate heat treatment conditions of T73, T74 and T76. The results of this study show that; 1. The optimum conditions of T7x heat treatment in extruded 7050Al alloy show this; $$T73:121^{\circ}C{\times}7hr+177^{\circ}C{\times}14hr$$. $$T74:121^{\circ}C{\times}7hr+177^{\circ}C{\times}10hr$$. $$T76:121^{\circ}C{\times}7hr+163^{\circ}C{\times}21hr$$. 2. The 2nd step aging heat treatment such as T73, T74 and T76 etc. is efective in 7050Al alloy but the variation otf microstructure and mechanical property with dispersive inclusions produced for extrusion process causes some troubles. Accordingly, in order to produce a good 7050Al alloy, a careful attention is needed in manufacturing process.

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선박 자동조타기 설계를 위한 퍼지모델링 (Fuzzy modelling for design of ship's autopilot)

  • 안종갑;이창호;이윤형;손정기;이수룡;소명옥
    • Journal of Advanced Marine Engineering and Technology
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    • 제34권1호
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    • pp.102-108
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    • 2010
  • 본 연구에서는 설계사양과 경제성을 고려한 퍼지형 자동조타기를 설계하기 위한 이전 단계로 Bech와 Wagner Smith의 Nomoto 2차 비선형 확장모델을 퍼지모델로 구현하는 것을 다룬다. 우선 퍼지형 자동조타기를 얻기 위해 선박의 동적 특성을 효과적으로 표현 가능한 T-S 퍼지모델을 얻는다. T-S 퍼지모델은 선박의 회두각속도를 설계변수로 간주하고 이것의 변화에 따라 다수개의 지역 선형모델(서브시스템)을 구한 후, "IF-THEN" 퍼지규칙으로 결합한 것이다. 이때 선형모델의 파라미터와 퍼지모델의 소속함수는 선박의 동적인 특성과 일치하도록 입 출력 데이터와 실수코딩 유전알고리즘이 결합된 모델 조정기법을 이용하여 최적으로 추정한다.