YAKHAK HOEJI (약학회지)
- Volume 37 Issue 3
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- Pages.286-289
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- 1993
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- 0377-9556(pISSN)
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- 2383-9457(eISSN)
Micro-Analysis of Methyl 5-Hydroxydinaphtho[1, 2-2', 3'] furan-7, 12-dione-6-carboxylate
메틸 5-히드록시 디나프토 [1, 2-2', 3'] 푸란-7, 12 디온 6-카복시레이트의 미량분석
Abstract
UV and high performance liquid chromatographic methods for the quantitative analysis of methyl 5-hydroxy-dinaphtho [1,2-2',3'] furan-7,12-dione-6-carboxylate(MHDDC) in urine and blood were developed. The correlation coefficients of the calibration curves of MHDDC in chloroform, methanol and dioxane solution were 0.999, 0.997 and 0.998, respectively. MHDDC was resolved within 15 min and had a detection limit of 2-5ng at S/N=3 by using a reversed-phase column with two solvents (MeOH, HAc).
Keywords
- Methyl 5-hydroxy-dinaphtho[1,2-2',3']furan-7;
- 12-dione-6-carboxylate;
- Paulownia tomentosa stem;
- UV;
- HPLC;
- urine;
- blood