• Journal of Welding and Joining
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• 제14권5호
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• pp.49-58
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• 1996

In Korea Gas Corporation, as one of the pipeline repairing methods, damaged pipelines are sometimes treated with a temporally employment of split sleeve. On conducting the repair process, circumferential fillet and longitudinal groove welding usually must be included. For the case of groove welding, a considerable amount of R&D have been carried out related to property changes, while few study on the property change in fillet welding has been conducted. In this paper, so as to confirm the specification of fillet welding in terms of safety and reliability, properties changed by fillet welding were investigated for two welding processes. Qualifying tests such as reviewing macrostructure and nick-break tests were performed according to API 1104 and ASME section IX. In addition, tensile properties and hardness were evaluated according to KS B0841 and BS 4515. The fillet weld prepared by the qualified procedure showed melting depth of 0.8∼1.3mm and heat affected zone of 2.8∼3.4mm length. No crack and lack of penetration were observed. And the results of hardness and nick-break tests satisfied code requirements. The area crossed by fillet and groove welding line was found to have minimal tensile strength.

• Steel and Composite Structures
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• 제28권6호
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• pp.759-766
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• 2018

Friction Stir Welding (FSW) is a solid-state process, where the objects are joined together without reaching their melting point. It has been shown that this method is a suitable way to join dissimilar aluminium alloys. The current article employed hole drilling technique to measure the residual stress distribution experimentally in different zones of dissimilar aluminium alloys AA6061-T6 and AA7075-T6 Butt welded using FSW. Results are compared with those of similar AA6061-T6 plates joined using a conventional fusion welding method called tungsten inert gas (TIG). Also, the evolution of the residual stresses in the thickness direction was investigated, and it was found that the maximum residual stresses are below the yield strength of the material in the shoulder region. It was also revealed that the longitudinal residual stresses in the joint were much larger than the transverse residual stresses. Meanwhile, Vickers micro hardness measurements were performed in the cross-section of the samples. The largest hardness values were observed in the stir zone (SZ) adjacent to the advancing side whereas low hardness values were measured at the HAZ of both alloys and the SZ adjacent to the retreating side.

• 한국레이저가공학회지
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• 제18권4호
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• pp.17-22
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• 2015

In this paper, ablation rate of $Al_2O_3$ ceramics by femtosecond laser fluence is derived with experimental method. The automatic three axis linear stage makes laser optics to move with high spatial resolution. With 10 times objective lens, minimal pattern width of $Al_2O_3$ is measured in the focal plane. Ablated surface area is shown as linear tendency increasing number of machining times with various laser power conditions. Machining times is most sensitive condition to control $Al_2O_3$ pattern width. Also, the linear increment of pattern width with laser power change is investigated. In high machining speed, the ablation volume rate is more linear with fluence because pulse overlap is minimized in this condition. Thermal effect to surrounding medium can be minimized and clean laser process without melting zone is possible in high machining speed. Ablation volume rate decelerates as increasing machining times and multiple machining times should be considered to achieve proper ablation width and depth.

• 한국재료학회지
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• 제2권3호
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• pp.180-190
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• 1992

ZMR공정에서 발생하기 쉬운 폴리실리콘의 엉김현상(agglomeration), 슬림, 그리고 실리콘기판이 국부적으로 녹는 현상 등을 방지하기 위한 방법과 재결정화된 박막의 질을 향상시키기 위하여 폴리실리콘과 보호 산화막(capping oxide)두계를 변화시킨 실험 결과를 서술한다. 폴리실리콘의 엉김현상은 폴리실리콘과 보호 산화막 그리고 폴리실리콘과 매몰 산화막(buried oxide)의 계면에서의 wetting각과 관계되는데, 엉김현상을 방지하기 위해서는 암모니아 가스 분위기에서 $1100^{\circ}$C, 3시간 동안 열처리하여 폴리실리콘과 보호 산화막 그리고 폴리실리콘과 매몰 산화막의 계면에 질소를 주입시키면 된다. 실리콘 기판의 뒷면이 국부적으로 녹아 SOI구조가 파괴되는 현상과 슬립은 실리콘 기판의 뒷면을 모래타격(sandblast)하여 약 $20{\mu}m$의 거칠기를 가지도록 했을때 방지할 수 있었다. 재결정화된 폴리실리콘의 두께가 두꺼워짐에 따라 재결정화된 박막에서 subboundary의 간격은 넓어지고, 재결정화된 실리콘 두께의 균일성은 보호 산화막이 두꺼울수록 향상된다. 폴리실리콘의 두께를 $1{\mu}m$로 하였을때 subboundary의 간격은 약 $70-120{\mu}m$정도였고 폴리실리콘의 두께가 $1{\mu}m$이고 보호산화막의 두께가 $2.5{\mu}m$일때, 재결정화 후 실리콘의 두게 균일도는 약 ${\pm}200{\AA}$정도였다.

• 마이크로전자및패키징학회지
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• 제26권2호
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• pp.45-49
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• 2019

높은 신뢰성의 n형 Bi-Te-Se계 열전소자 제조를 위한 열간압출 공정을 확립하였다. 용융-응고 공정을 이용하여 Bi-Te-Se 원료잉곳을 합성하였으며, 고에너지 볼밀을 이용하여 평균 ${\sim}30{\mu}m$ 크기의 분말로 분쇄하였다. 일축가압 공정으로 분말을 직경 20 mm의 디스크 형태로 성형한 후 압출용 몰드 설계-제작 및 열간압출 공정 온도와 압력을 제어하여 성형체로부터 00l 방향으로 결정 배향된 지름 1.8 mm의 원통형 고밀도 압출체를 제조하였다. 상온에서 최대 ${\sim}4.1mW/mK^2$의 높은 파워팩터를 나타냈으며, zone melting 공정으로 제조한 상용 열전소재와 비교하여 2배 이상 향상된 기계적 강도 (~50 MPa)를 구현하였다.

• 한국결정성장학회지
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• 제21권5호
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• pp.199-204
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• 2011

존멜팅법을 이용해서 $(YSmNd)_{1.8}Ba_{2.4}Cu_{3.4}O_{7-x}$계 고온초전도체를 대기 중에서 용융성장실험을 하였다. 존멜팅법의 최적용융온도는 $1100^{\circ}C$였으며 성장속도는 3.5 mm/h 였다. 한 방향으로 용융성장 된 (YSN)1.8 초전도체는 XRD, 광학현미경, TEM을 이용하여 미세구조를 관찰하였으며 SQUID magnetometer와 직접전류수송법을 이용해 초전도특성을 평가하였다. 특히 용융성장 된 (YSN)1.8 초전도체의 광학현미경에 의한 미세구조 관측 결과 초전도상인 (YSN)123 matrix내에 비초전도상인 (YSN)211 inclusions이 균질하게 분포되어 있는 것이 관측되었다. 또한 용융성장 된 (YSN)1.8 초전도체는 90 K 이상의 임계온도 특성을 보였으며 액체질소 안에서 직접전류수송법으로 측정한 결과 수송전류 830 A에서 $3.93{\times}10^4$(A/$cm^2$)를 갖는 높은 임계전류밀도 특성을 보였다.

• 한국해양공학회지
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• 제21권3호
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• pp.71-76
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• 2007

Recently, many industries have been employing the application of laser beam welding, due to the resulting high welding quality, such as smaller width of melting and heat affective zone, smaller welding deformation, and fine grains of weldment, compared to arc welding. However, in order to appropriately utilize this welding process with steel structure, the characteristics of welding residual stresses and fracture toughness in welded joints are to be investigated for reliability. Therefore, in this study, the mechanical properties of weldments by arc and laser welding are investigated using FEM to confirm the weldability of laser welding to the general structural steel (HT50). The Charpy impact test and 3-points bending CTOD test are carried out in the range of temperatures between $-60^{\circ}C\;and\;20^{\circ}C$, in order to understand the effect on the fracture toughness of weldments. From the research results, it has been found that the maximum residual stress appears at the center of plate thickness, and that the fracture toughness is influenced by strength mis-match.

• 한국결정성장학회지
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• 제1권2호
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• pp.23-33
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• 1991

Mn-Zn Ferrite는 단결정을 성장하기 위하여 용융하는 동안 불균질 용융과 ZnO휘발의 고유특성을 갖는 재료이다. 그 결과로, 결정성장축을 따라 양이온의 분포가 불균일 하게 된고 또한 기존의 Bridgman법에서는 도가니내에서 용융대가 장시간 유지됨으로써 백금입자가 결정안으로 침입하게된다. 이들은 훼라이트의 자기적 성질을 저하시키는 성질을 갖고 있다. 그러나 새로운 성장법에서는 이러한 단점들을 극복하고 양질의 단결정을 얻기 위하여 결정성장 인자들의 관계를 고찰하였으며 그 인자들은 다음과 같다 : 도가니내의 melt 높이, melt의 표면장력과 밀도, 계면에서의 melt거동, 도가니와 고액계면의 형상, 원료공급속도, 결정성장속도. 아울러, 성장된 결정의 조성을 분석하였을 때 초기조성과 비교하여 $\textrm{Fe}_2\textrm{O}_3$ 1.5 mol%, MnO, Zn 2.0 mol% 이내로 조성 변동은 각각 억제되었고 성장결정면 (110)에서 화확적인 etching 법을 이용하여 광학현미경을 통해 결정내부등을 관찰하였으며, 자기적 특성등을 측정하였다.

• Journal of Welding and Joining
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• 제18권2호
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• pp.213-213
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• 2000

This study was performed to investigate types and formation mechanism of cracks in two Al alloy welds, A5083 and A7NO1 spot-welded by pulse Nd: YAG laser, using SEM, EPMA and Micro-XRD. In the weld zone, three types of crack were observed: center line crack($C_{C}$), diagonal crack($C_{D}$), and U shape crack($C_{U}$). Also, HAZ crack($C_{H}$), was observed in the HAZ region, furthermore, mixing crack($C_{M}$), consisting of diagonal crack and HAZ crack was observed.White film was formed at the hot crack region in the fractured surface after it was immersed to 10%NaOH water. In the case of A5083 alloy, white films in C crack and $C_D crack region were composed of low melting phases, Fe₂Si$Al_8$ and eutectic phases, Mg₂Al₃ and Mg₂Si. Such films observed near HAZ crack were also consist of eutectic Mg₂Al₃. In the case of A7N01 alloy, eutectic phases of CuAl₂, $Mg_{32}$ (Al,Zn) ₃, MgZn₂, Al₂CuMg and Mg₂Si were observed in the whitely etched films near $C_{C}$ crack and $C_{D}$ crack regions. The formation of liquid films was due to the segregation of Mg, Si, Fe in the case of A5083 alloy and Zn, Mg, Cu, Si in the case of A7N01 aooly, respectively.The $C_{D}$ and $C_{C}$ cracks were regarded as a result of the occurrence of tensile strain during the welding process. The formation of $C_{M}$ crack is likely to be due to the presence of liquid film at the grain boundary near the fusion line in the base metal as well as in the weld fusion zone during solidification. The $C_{U}$ crack is considered a result of the collapsed keyhole through incomplete closure during rapid solidification. (Received October 7, 1999)

• 한국광물학회:학술대회논문집
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• 한국광물학회.한국암석학회 2003년도 공동학술발표회 논문집
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• pp.66-66
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• 2003

King George island, Antarctica, is mostly covered by ice sheet and glaciers, but the land area is focally exposed for several thousand years after deglaciation. For a mineralogical study of chemical weathering in the polar environment, glacial debris was sampled at the well-developed patterned ground which was formed by long periglaclal process. As fresh equivalents, recently exposed tills were sampled at the base of ice cliff of outlet glaciers and at the melting margin of ice cap together with fresh bedrock samples. Fresh tills are mostly composed of quartz, plagioclase, chlorite, and illite, but those derived from hydrothermal alteration zone contain smectite and illite-smectite. In bedrocks, chlorite was the major clay minerals in most samples with minor illite near hydrothermal alteration zone and interstratified chlorite-smectite in some samples. Smectite closely associated with eolian volcanic glass was assigned to alteration in their source region. Blocks with rough surface due to chemical disintegration showed weathering rinds of several millimeter thick. Comparision between inner fresh and outer altered zones did not show notable change in clay mineralogy except dissolution of calcite and some plagioclase. Most significant weathering was observed in the biotite flakes, eolian volcanic glass, sulfides, and carbonates in the debris. Biotite flakes derived from granodiorite were altered to hydrobiotite and vermiculite of yellow brown color. Minor epitactic kaolinite and gibbsite were formed in the cleaved flakes of weathered biotite. Pyrite was replaced by iron oxides. Calcite was congruently dissolved. Volcanic glass of basaltic andesite composition showed alteration rim of several micrometer thick or completely dissolved leaving mesh of plagioclase laths. In the alteration rim, Si, Na, Mg, and Ca were depleted, whereas Al, Ti, and Fe were relatively enriched. Mineralization of lichen and moss debris is of much interest. They are rich of A3 and Si roughly in the ratio of 2:1 to 3:1 typical of allophane. In some case, Fe and Ti are enriched in addition to Al and Si. Transmission electron microscopy of the samples rich of volcanic glass showed abundant amorphous aluminosilicates, which are interpreted as allophane. Chemical weathering in the King George Island is dominated by the leaching of primary phyllosilicates, carbonates, eolian volcanic glass, and minor sulfides. Authigenesls of clay minerals is less active. Absence of a positive evidence of significant authigenic smectite formation suggests that its contribution to the clay mineralogy of marine sediments are doubtful even near the maritime Antarctica undergoing a more rapid and intenser chemical weathering under more humid and milder climate.