• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2001.10a
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• pp.244-247
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• 2001

Lubricanting characteristics in the warm forging have influence on forgeability of products. but Research on deformation characteristic of warm forging on the lubricant and lubricating method lack. This paper deform a bevel gear by warm forging and evaluate deformation loads and quality of products by each lubricants and lubricating method using oil-based lubricants(Soy, Oildag) and water-based lubricants(Deltaforge $\#31$, Renite S-26-X, Deltaglaze $\#151$). In conclusion, the less a deformation load by lubricants the more improvement a quality of product in manufacture of a bevel gear and water-based lubricants in the warm forging reduce a deformation load and improve a quality of products. Especially, Deltaforge $\31$ have excellent characteristic in the warm forging.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1998.03a
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• pp.107-112
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• 1998

The semi-solid materials(SSMs) fabricated under electric-magnetic stirring condition are necessary to be applicated in the thixoforging process. The optimal reheating conditions to thixoforging process were investigated with changing the reheating time, holding time, reheating temperatures, capacity, and adiabatic material size. In the case of solid fraction fs=50%, the microstructure of SSM (specimen size:d76X 190) at the condition of the first reheating time 4min, holding time lrnin and reheating temperature 350%, the second reheating time 3min, holding time 3min and reheating temperature 575C, the thlrd reheating time lmin, holding time 2min and reheating temperature 584'C, capacity Q=8.398KW, and adiabatic material size 53mm is obtained with globular microstructure and finest.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2008.05a
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• pp.57-60
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• 2008

The studies for internal void closure have been conducted experimentally and numerically for open die forging. The FEM analysis is performed to investigate the deformation behavior of some internal voids in cast ingots during two upsetting stages. The calculated results of void closure behavior are compared with the measured results before and after upsetting. The shapes and sizes of each internal void are scanned by the X-ray scanner. From this result, the criteria for deformation amounts effect on the void closure can be investigated by the types of void. Closed voids could be compressed and eliminated after forging when the applied deformation amounts were larger than the critical effective strains. On the other hand, open voids could not be compressed and removed.

• Journal of the Korean Society of Industry Convergence
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• v.22 no.6
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• pp.649-655
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• 2019

Fracture behaviors of SCM435 high strength bolt have been studied including macroscopic and microscopic fracture observation, Energy Dispersive X-ray Spectroscopy, Vickers hardness test and applied stress evaluation. cracks (ratchet marks) were generated by the repetitive loads acting on the bolts, initial stress of bolt and the stress concentration. The applied stress was found to be slightly higher than the fatigue limit of the material. The initial stress of bolt must be removed, and the mold temperature during the process must be maintained by room temperature. Bolts are recommended to be peened to improve fatigue limit.

• Korean Journal of Metals and Materials
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• v.47 no.12
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• pp.797-810
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• 2009

A study was made of the effects of a Sn addition on the microstructure and microfracture mechanism of squeeze cast AZ51-xSn magnesium alloys. Microstructural observation, in situ fracture testing, and fractographic observations were conducted on these alloys to clarify the microfracture process. The microstructural analyses indicated that $Mg_2Sn$ particles as well as $Mg_{17}Al_{12}$ particles precipitated mainly along the solidification cell boundaries; the volume fraction of these hard particles increased as the amount of added Sn increased, with increased the strength. From in situ fracture observations of the AZ51-7Sn alloy, coarse precipitates located on the cell boundaries worked as easy crack propagation sites and caused abrupt intercellular fracturing. On the other hand, the overall fracture properties of the AZ51-3Sn alloy improved because crack propagation proceeded into the Mg matrix rather than into the cell boundaries as twins developed actively, as confirmed by an R-curve analysis. These findings suggest that the addition of 3~5 wt.% Sn is effective in improving both the tensile and fracture properties on the basis of well-developed twins, the blocking of crack propagation, and crack blunting.

• Journal of the Korean Applied Science and Technology
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• v.37 no.3
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• pp.516-525
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• 2020

The densities of aqueous solutions of the amphiphile 2-(2-hexyloxyethoxy)ethanol (C₆E₂) were measured at 279.15 K and 282.15 K by vibrating-tube densitometry. Then using the density data of the binary C₆E₂ (1)/water(2) system, the excess volumes and partial molar volumes were determined at various compositions. Excess volume V^E exhibits negative deviation for the whole region of composition, which implies relatively stronger attraction between molecules. At the C₆E₂ mole fraction of around 0.45, V^E was at its minimum. Partial molar volume ${\bar{V}}_1$ increases monotonously with the mole fraction x₁(=x) and ${\bar{V}}_2$ decreases with x. Any particular point in ${\bar{V}}_1$ and ${\bar{V}}_2$, which may point to molecular association, was unobserved.

• Journal of the Korean Magnetics Society
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• v.14 no.2
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• pp.76-82
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• 2004

Crystallographic and magnetic properties for Brownmillerite-type oxides $Ca_{1-x}$Sr$_{x}$FeO$_{2.5}$ (x = 0, 0.3, 0.5, 0.7, 1.0) were investigated using x-ray diffraction (XRD) and Mossbauer spectroscopy. Polycrystalline samples were prepared by conventional solid-state reaction method. Information on exact crystalline structures, lattice parameters, bond lengths and bond angles were obtained by refining their XRD profiles using a Rietveld method. The crystal structures were found to be all orthorhombic with space group Icmm (x = 0, 0.3) and Icmm (x = 0.5, 0.7, 1.0) The lattice parameters increased monotonically with increasing Sr concentration. Both the tetrahedral and the octahedral sites were considerably distorted and elongated along b-axis. While bond lengths and bond angles O-Fe-O tend to increase minutely with the increase of Sr content, bond angles Fe-O-Fe decreased accordingly. The Mossbauer spectra showed two sets of sharp sextets originating from ferric ions occupying the tetrahedral and the octahedral sites under the magnetic transition temperature T$_{N}$. Regardless of the compositions x, the electric quadrupole splittings were -0.3 mm/s and 0.4 mm/s for the octahedral and the tetrahedral site, respectively. Above T$_{N}$, the Mossbauer spectra showed the paramagnetic doublets whose electric quadrupole splittings were about 1.6 mm/s, irrespective of compositions x. T$_{N}$ was found to decrease monotonically with the increase of Sr concentration. Ratios of absorption area for the two sites were almost 1:1 up to as high as 0.95 T$_{N}$ for all x. The result of the Debye temperature indicated that the inter-atomic binding force for the Fe atoms in the tetrahedral site was stronger than that for the octahedral site.hedral site.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2000.04a
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• pp.67-70
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• 2000

Mechanical properties of (10%$AI_20_3{\cdot}SiO_2$+5%Ni)/Al hybrid composites fabricated by the reaction squeeze casting were compared with those of (15%$AI_20_3{\cdot}SiO_2$)/Al composites. Intermetallic compound formed by reaction between molten aluminum and reinforcing powder was uniformly distributed in the Al matrix. These intermetallic compounds were identified as $Al_3$NI using EDS and X-ray diffraction analysis. Microhardness and flexural strength of hybrid composites were higher than that of (15%$AI_20_3{\cdot}SiO_2$)/Al Composite. In-Situ fracture tests were Conducted on (15%$AI_20_3{\cdot}SiO_2$)/Al Composites and (10%$AI_20_3{\cdot}SiO_2$+5%Ni)/Al hybrid composites to identify the microfracture process. It was identified from the in-situ fracture test of (10%$AI_20_3{\cdot}SiO_2$+5%Ni)/Al composites, microcracks were initiated mainly at the short fiber / matrix interfaces. As the loading was continued, the crack propagated mainly along the separated interfacial regions and the well developed shear bands. It was identified from the in-situ fracture test of (10%$AI_20_3{\cdot}SiO_2$+5%Ni)/Al hybrid composites, microcracks were initiated mainly by the short fiber/matrix interfacial debonding. The crack proceeded mainly through the intermetallic compound clusters

• Journal of Korea Foundry Society
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• v.14 no.5
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• pp.419-428
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• 1994

The microvickers hardness and microstructure of Fe/Al composite fabricated by squeeze casting method were investigated. Pure Al and A356 Alloy were chosen for the matrix composition and Fe preform was fabricated with sintered Fe powder at $1000^{\circ}C$ for 30min. under hydrogen atmosphere. Experimental variables were included preheating temperature, melt temperature and applied pressure. Analysing the experimental result concerning microstructure of fabricated composites, Fe/A356 composite showed improved microstructure at $600^{\circ}C$ melt temperature and $350^{\circ}C$ preform preheating temperature in Fe distribution and Infiltrated distance. The results of EDX and XRD showed that the interfacial zones of Fe/Al composite were composed of non-equilibrium intermetallic layers[$(Al_5Fe_2)_x$, $Al_{13}Fe_4m\;Fe_3Al$, FeAl]. The microvickers hardness of Fe/Al composite showed higher value than Fe/A356 composite in interface.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.10a
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• pp.50-52
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• 2007

Large size forged parts usually were made by hot open die forging because of the die cost, high applied load and small manufacturing quantities. Cast ingots were used in open die forging and the ingots almost included the cavities in its inside. Therefore, one of the aims for forging processes is to close and remove the cavities. However, its criteria were well not defined since the studies have many difficulties to investigate the cavity behaviors because of its large size. In this study, the cavity closure behavior was investigated by experimental and FE analysis. The FEM analysis is performed to investigate the overlap defect of cast ingots during free forging stage. The measured flow stress data were used to simulate the forging process of cast ingot using the practical material properties. Also the analysis of cavity closure is performed by using the $DEFORM^{TM}$-3D. The calculated results of cavity closure behavior are compared with the measured results before and after forging, which are scanned by the X-ray scanner. From this result, the criteria for deformation amounts effect on the cavity closure can be investigated by the comparison between practical experiment and numerical analysis.