• Journal of the Korean Wood Science and Technology
• /
• v.50 no.1
• /
• pp.31-45
• /
• 2022

After manufacturing the natural dyed actual size Hanji using 11 kinds of plant natural dyeing materials and 2 kinds of animal natural dyeing materials, the color characteristics and color change and color fastness after post-mordanting were compared and discussed. The hues of 13 types of natural dyed Hanji were black, PB, and RP, each with 1 type, YP with 3 types, and Y with 7 types. Among the natural dyeing materials, Chinese ink, indigo and Lac showed high color yield and color difference, and violet-root cromwell and gardenia seeds showed low color yield. The color fastness of Hanji dyed with turpentine diluted Ottchil, Pagoda tree seeds, Chinese ink and indigo was excellent, while that of gardenia seeds and violet-root cromwell were very poor. After post-mordanting of natural dyed Hanji with Al, Cu, and Fe mordants, the hue changes were show up the Alnus firma, clove, lac and cochineal. In addition, the color difference was very diverse and was overall the most biggest due to Fe mordant. After 72 hr. of UV irradiation on post-mordanting natural dyed Hanji, hue change was observed in 3 types and color fastness was improved in 8 types by post-mordanting. The Hue and color fastness are significantly different depending on the type of natural dying materials and post-mordants. Therefore, when dyeing Hanji with natural dyes, it is necessary to dye with sufficient knowledges and informations about the desired color and fastness.

• Journal of the Korean Wood Science and Technology
• /
• v.37 no.6
• /
• pp.566-577
• /
• 2009

The modification of wood color occurs rapidly during the service period at indoor. It is crucial to investigate the characteristics of color change, chemical and microscopical modification of wood at indoor. Wood products made of Japanese cedar at different years were used for this work. The tests were performed in order to evaluate the degree of color change of wood surface, breakpoint of brightness from surface to inside of wood, chemical analysis with FT-IR, and microscopical characteristics using the LM and TEM. Surface color of cedar wood stored indoor were rapidly changed at early stage, particularly ${\Delta}a$ (yellow), and ${\Delta}b$ (red) values were steeply decreased for one year old indoor wood, ${\Delta}L$ (white) value was dropped until 5 years old indoor wood compared with control sample. Decrease of peaks related to polysaccharide and lignin was noticed, especially, lignin was severely degraded. Although degradation of cell wall limited only to surface layers of indoor wood, degradation pattern of indoor wood showed similar degradation pattern to natural weathering of wood during outdoor weathering or wood behavior under artificial UV irradiation.

• Fashion & Textile Research Journal
• /
• v.11 no.6
• /
• pp.968-973
• /
• 2009

To get a variety of colors on silk fabrics with natural dyes, mordanting and combination dyeing were carried out. Gromwell, sappan wood, safflower were used as the three primary colors for combination dyeing. Metal compounds containing alum and iron were used as mordanting agents. In combination dyeing of safflower and sappan wood, safflower and gromwell, gromwell and sappan wood, various colors were obtained according to the content of dyes used. Safflower/sappan wood dyeing showed different colors between yellow red and red purple of Munsell color circle such a YR, R and RP. And safflower/gromwell dyeing showed R, RP, P and PB Munsell color circle and then gromwell/sappan wood showed R, RP and P. As the result of these experiments, wide range of colors (YR-R-RP-P-PB-B) were obtained according to various mixing portion of safflower, gromwell, sappan wood, dyebath pH and repetition dyeing.

• Journal of the Korea Furniture Society
• /
• v.23 no.1
• /
• pp.68-74
• /
• 2012

In this study domestic thinning and small diameter woods of Giant dogwood (Cornus controversa Hemsl) was used. To increase the utilizability of wood, the utilizability was proposed after manufacturing laminated wood by pressing and heating. The physical and mechanical characteristics of Laminated wood were investigated and the color change was measured, using a Chromaticity coordinates, after being pressed at 10% (45 mm), 20% (40 mm), 30% (35 mm) for 5 minutes, using Stopper, and then heated at $180^{\circ}C$ for 6, 12, 24 and 48 hours. The results were as follows. Wood density, compressive strength, MOR, MOE are increased with increasing pressing rate but decreased as heating time is increased after pressing. However, Color change is clear, dimensional stability is improved after pressing and heating.

• Journal of the Korean Wood Science and Technology
• /
• v.40 no.6
• /
• pp.370-377
• /
• 2012

This study was conducted to investigate the color change of heat-treated wood made of Korean pine (Pinus koraiensis S. et Z.), and lodgepole pine (Pinus contorta Dougl). The wood samples were heat-treated at 9 different treatment combinations of temperature (170, 180, 200, 220, and $230^{\circ}C$), and time (90, 120, 180, 240, 270 min.) set up by a response surface method. Wood color was measured using a colorimeter, and the samples were installed for evaluating the resistance of termite in the field test sites set up in Jinju. The lightness decreased with the increase of treatment temperature and treatment time. The color differences were evaluated by the method of National Bureau of Standards (NBS), and response surface models to predict the color change were fitted as a function of treatment temperature and treatment time. The $R^2$ values of the fitted models of heat-treated Korean pine and lodgepole pines were 0.92, and 0.88, respectively, showing the potential way for the prediction of color changes. Severe damage was found from the samples in the field test site, which means that the manufactured heat-treated wood did not show the termite resistance enough for the outdoor use.

• Journal of the Korean Wood Science and Technology
• /
• v.46 no.5
• /
• pp.511-526
• /
• 2018

Effects of heat treatment on the characteristics of Royal paulownia (Paulownia tometosa) wood were investigated. The results were compared with those of Suwon silver poplar (Populus tementiglandulosa) and Korean red pine (Pinus densiflora) woods. The wood samples of the three species were treated at $160^{\circ}C$, $180^{\circ}C$, $200^{\circ}C$ and $220^{\circ}C$ in an electric furnace for 2 hours. The changes of color, density, mass loss, and relative crystallinity were investigated before and after heat treatment. The lightness ($L^*$) decreased rapidly from $200^{\circ}C$ in all species. There were no change in red-green chromaticity($a^*$) and yellow-blue chromaticity($b^*$) of Royal paulownia and poplar woods with increasing temperature. Whereas, yellow-blue chromaticity($b^*$) of Korean red pine wood decreased sharply from $200^{\circ}C$. Royal paulownia wood showed appreciable color change(${\Delta}E^*$) after heat treatment above $180^{\circ}C$. Poplar and pine woods, however, presented significant color change from $160^{\circ}C$. Color change of the three wood species increased rapidly with increasing temperature. Mass loss of the three wood species by heat treatment was the highest in the Royal paulownia wood and the lowest in the pine wood. Mass loss and relative crystallinity increased and density decreased slightly with increasing temperature. Consequently, it is revealed that Royal paulownia wood showed considerable differences in the temperature of color change, weight loss and change of relative crystallinity compared to the other wood species.

• Journal of Conservation Science
• /
• v.32 no.2
• /
• pp.155-165
• /
• 2016

This study aimed at verifying the effect of hydroxypropyl cellulose(HPC) treatment on polyethylene glycol(PEG)-treated waterlogged wood for surface stabilizing. This research investigated macroscopic and microscopic appearance, color change, weight change, and dimensional change. And effect of HPC was verified through variance analysis (ANOVA) and least significant difference test(LSD). HPC formed thin layer on the surface of wood specimen, and blocked the pore of tracheid and the gap between the crack. Specimens without deterioration showed no invisible change except HPC 1,000,000 treatment group. Whitening was appeared at the sound surface of HPC 1,000,000 treated wood. Specimens with deterioration showed a little color difference change by external moisture adsorption. Thin layer of HPC on the surface of wood specimen was maintained after the deterioration, and this HPC layer significantly suppressed the weight and dimensional change by moisture adsorption.

• Journal of the Korean Wood Science and Technology
• /
• v.47 no.3
• /
• pp.311-323
• /
• 2019

The number of newly constructed traditional Korean houses, i.e., Hanoks, and light-frame buildings is increasing. However, related research is limited owing to the lack of awareness regarding safety evaluations. Therefore, this study conducted an outdoor exposure test to accurately evaluate wooden constructions. Spruce, pine, and fir (SPF) material was monitored for a year, wherein the SPF material was artificially dried under 18% moisture content, and its physical properties and color differences were measured once a month. Large differences were observed in the material's weight and moisture content, which are indexes sensitive to daily range and rainfall; however, no significant difference was found for other basic properties in the pre and post test results. Herein, $L^*$, $a^*$, and $b^*$ values represent color differences; these values exhibited a general decrease after the test. Such differences were attributed to the loss of lignin in the wood. The color difference value was high between the months of May and July, when the daily range and rainfall significantly fluctuated. Multiple regression analysis was performed on the $a^*$ value (redness indicator), daily range, rainfall, and ultraviolet index. The results indicated that the daily range influenced redness the most. According to the estimated regression equation, the daily range and redness are positively correlated. Based on the results, the types and influence of independent variables on color difference are expected to change as the wood's duration of outdoor exposure and the amount of data obtained both increase.

• Journal of the Korean Wood Science and Technology
• /
• v.50 no.4
• /
• pp.283-298
• /
• 2022

Wood has always been used for various day-to-day applications such as interior or exterior construction materials, and household products. However, it can undergo photodegradation and discoloration by environmental factors including ultraviolet (UV) light, and thus has shortened its service life. Bleaching or delignification of wood surfaces is a suitable solution to stabilize wood against weathering by UV because these techniques can alter or remove the chromophores in lignin, which is a main factor of wood discoloration. To improve the color stability of wood surface according to the lifespan, surface delignification was conducted using peracetic acid (PAA) and hydrogen peroxide (HP) on the woods of Larix kaempferi and Quercus mongolica. After the PAA treatment, L^* increased considerably from 60-70 to 90-95. Furthermore, wood surface color did not change significantly after UV exposure. The color differences (𝜟E^*) between before and after PPA treatment of wood showed the 4.8-12.2 of L. kaempferi, and 1.7-3.7 of Q. mongolica, respectively. The lignin-related peaks in Fourier transform infrared spectroscopy (FT-IR) spectra disappeared with increased duration of PAA treatment. These results confirmed that the lignin component was partially or completely removed after the PAA treatment; the color differences (𝜟E^*) clearly showed that there was a reduction in redness (a^*) and yellowness (b^*), and an increase in lightness (L^*) owing to the removal of lignin. Based on these results, this study demonstrated that the partial removal of lignin from wood surfaces is a fundamental method for resolving photo-degradation.

• Journal of the Korean Society of Clothing and Textiles
• /
• v.23 no.6
• /
• pp.788-799
• /
• 1999

This study was performed to investigate the effect of mordants on the dyeability colorfastness to light and to laundering and biological properties of mordanted and natural-dyed cotton and silk substrates. Natural red dyes were extracted from Caesalpinia Sappan L. (Sappan wood) and Rubia Akane Nakai (Madder) by boil water Five different compounds of Al, Cr, Cu, Fe and Sn were used as mordanting agents. The result of this study are sumarized as follows ; 1. In the of the fabrics mordanted and dyed with sappan wood K/S value increases and λmax shifts to the longer wavelength as mordant concentration increases. Color of the fabrics dyed with sappan wood and madder change to redder bluer and lighter after mordanting. 2. As the number of repetition of dyeing-mordnating process increase the color of the dyed fabrics tend to be redder bluer and darker. Mordanted dyes with Al and Sn make chroma increase. The quantity of mordant absorbed in the silk fabric increase as mordant concentration increase. More Fe is absorbed in silk than Cr is. 3. After being exposed to light the fabrics dyed with sappan wood and madder change to less red Fe and Cu mordanting yeild better colorfastness to light than others does. Natural-dyed fabrics exposed to light tend to be faded and whitened in CIELAB chromaticity co-ordinates. So we might trace back the original color of ancient faded fabrics by changes in color of natural dyes. 4. After washing the colors of natural dyes change to more blue, Fe and Cu mordanting give better colorfastness to wash than others do. 5. The soil-burial cotton is more susceptible to mildew and rot than the silk is. Antimicrobial activity of the natural-dyed cotton can be enhanced by Cu and silk can be enhanced by Cu and Cr mordanting respectively.