• 제목/요약/키워드: wetting angle

검색결과 177건 처리시간 0.022초

$Al/Al_2O_3$ 계면의 젖음특성 및 계면반응 (Wetting Characteristics and Interfacial Reaction at $Al/Al_2O_3$ Interface)

  • 권순용;정대영;최시경;구형회;이종수
    • 한국세라믹학회지
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    • 제31권8호
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    • pp.815-822
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    • 1994
  • Sessile drop studies of molten Al on single crystal sapphire substrate were conducted to understand the wetting behavior and interfacial reaction at Al/Al2O3 interface. To investigate the wetting mechanism, the variation in contact angle was determined with time. The contact angle obtained in this study decreased exponentially with time. This result means that the driving force for wetting is the reduction in interfacial energy between liquid Al and sapphire caused by the interfacial reaction. The closer examination revealed that the reaction was the dissolution of sapphire by molten Al. Ti has been frequently used to improve wetting on ceramic materials. Therefore, the influence of Ti content on the wetting behaviour was investigated in this work. The equilibrium wetting angles of pure Al, Al-0.3 wt%Ti, and Al-1.0 wt%Ti at 100$0^{\circ}C$ were 63$^{\circ}$, 59$^{\circ}$, and 54$^{\circ}$respectively. The difference is considered as the result of the change in interfacial energy caused by the reaction between Ti and sapphire and the interfacial reaction formed the reaction products of varying stoichiometry (TiO, Ti2O3, TiO2 etc.).

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표면형상이 젖음각과 마이크로/나노 트라이볼로지 특성에 미치는 영향 (Effect of surface topography on wetting angle and micro/nano-tribological characteristics)

  • 윤의성;오현진;양승호;공호성
    • 한국윤활학회:학술대회논문집
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    • 한국윤활학회 2002년도 제35회 춘계학술대회
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    • pp.25-33
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    • 2002
  • Effect of surface topography on the water wetting nature and micro/nano tribological characteristics of Si-wafer and PTFE was experimentally studied. The ion beam treatment was performed with a hollow cathode ion gun in different argon don dose conditions in a vacuum chamber to change the surface topography, Micro/nano tribological characteristics, water wetting angles and roughness were measured with a micro tribo tester, SPM (scanning prove microscope), contact anglemeter and profilometer, respectively. Results showed that surface roughness increased with the argon ion dose. The water wetting angle of tile ion beam treated samples also increased with the ion dose. Results also showed that micro-adhesion and micro-friction depend on the wetting characteristics of the PTFE samples. However, nano-triboloSical characteristics showed little dependence on the wetting angles. The water wetting characteristics of modified PTFE samples were discussed in terms of the surface topographic characteristics.

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웨팅밸런스법을 통한 젖음성 평가와 솔더의 젖음 특성 (Wettability Evaluation by Wetting Balance Test and Wetting Characteristics of Solders)

  • 전욱상;;정재필
    • 마이크로전자및패키징학회지
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    • 제26권3호
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    • pp.1-6
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    • 2019
  • Wettability is an important factor to decide solderability of solder, flux, other soldering-related materials and soldering conditions. The wettability also affects the reliability of solder joint. Wetting balance test is a good method for quantitatively measuring wettability between solder and substrate. The wetting balance test is easy to reproduce the wetting experiment and to measure the wetting time and force. And this test provides wetting curve to calculate the surface tension of the molten solder. Development of new solder has been continued in accordance with various and harsh environment in the electronics industry. In this paper, the principle of wetting balance test and recent research issues including nano-composite solder are explained.

A hysteresis model for soil-water characteristic curve based on dynamic contact angle theory

  • Liu, Yan;Li, Xu
    • Geomechanics and Engineering
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    • 제28권2호
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    • pp.107-116
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    • 2022
  • The steady state of unsaturated soil takes a long time to achieve. The soil seepage behaviours and hydraulic properties depend highly on the wetting/drying rate. It is observed that the soil-water characteristic curve (SWCC) is dependent on the wetting/drying rate, which is known as the dynamic effect. The dynamic effect apparently influences the scanning curves and will substantially affect the seepage behavior. However, the previous models commonly ignore the dynamic effect and cannot quantitatively describe the hysteresis scanning loops under dynamic conditions. In this study, a dynamic hysteresis model for SWCC is proposed considering the dynamic change of contact angle and the moving of the contact line. The drying contact angle under dynamic condition is smaller than that under static condition, while the wetting contact angle under dynamic condition is larger than that under static condition. The dynamic contact angle is expressed as a function of the saturation rate according to the Laplace equation. The model is given by a differential equation, in which the slope of the scanning curve is related to the slope of the boundary curve by means of contact angle. Empirical models can simulate the boundary curves. Given the two boundary curves, the scanning curve can be well predicted. In this model, only two parameters are introduced to describe the dynamic effect. They can be easily obtained from the experiment, which facilitates the calibration of the model. The proposed model is verified by the experimental data recorded in the literature and is proved to be more convenient and effective.

가솔린엔진용 포트분사식 인젝터의 분무특성에 관한 연구 (Study on the Spray Characteristics of a Port Fuel Injector for a Gasoline Engine)

  • 이상인;이성원;박성영
    • 한국분무공학회지
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    • 제15권2호
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    • pp.61-66
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    • 2010
  • Fuel spray characteristics of the gasoline engine injector has been studied experimentally. To provide fundamental performance data of 4-hole and 12-hole injectors, spray fuel-mass distribution, wall wetting fuel amount and visualization of injectors have been tested and measured with various fuel supply pressure conditions. Spray visualization has been performed to analyze spray formation, spray angle, stream width and penetration length. Test result shows that wall wetting is greatly influenced by the induction air amount and spray atomization. Spray visualization shows that the 12-hole injector has robust performance characteristics with various fuel supply pressure conditions compared with the 4-hole injector. 4-hole injector generates relatively less wall-wetting fuel amount than 12-hole injector does.

EWOD(Electro-Wetting on Dielectric)에 의한 초소수성 표면에서의 액적 이동과 부유물의 영향 (The droplet movement on the super-hydrophobic surface by the electro-wetting on dielectric and the effect of particles)

  • 변도영;이영종
    • 유체기계공업학회:학술대회논문집
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    • 유체기계공업학회 2006년 제4회 한국유체공학학술대회 논문집
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    • pp.297-300
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    • 2006
  • This article discusses about the droplet movement on the super-hydrophobic surface by the electro-wetting on dielectric and the effect of particles on the contact angle as well as the movement is investigated. The movement of droplet, driven by the principle of electro-wetting on dielectric, and the effect of particles are experimentally verified according to the driving voltage and different particles concentrations (fluorescent, charged particles). To increase the contact angle, the super-hydrophobic surface is fabricated and applied to the dielectric layer for the EWOD device. Then its performance is verified and discussed.

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UBM(Under Bump Metallurgy)이 단면 증착된 Si-wafer의 젖음성에 관한 연구 (A Study on the Wetting Properties of UBM-coated Si-wafer)

  • 홍순민;박재용;박창배;정재필;강춘식
    • 마이크로전자및패키징학회지
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    • 제7권2호
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    • pp.55-62
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    • 2000
  • Si-wafer에 단면 코팅된 UBM(Under Bump Metallurgy)의 젖음성을 Sn-Pb 솔더에서 평가하기 위하여 wetting balance 법을 사용하였다. 단면 코팅된 UBM의 젖음곡선은 양면 코팅된 시편의 젖음 곡선과 비교할 때, 젖음곡선의 모양이 비슷하고 젖음곡선을 특징짓는 변수들의 온도에 대한 변화경향이 일치하였다. 단면 코팅된 금속층의 젖음성을 젖음곡선으로부터 정의한 새로운 젖음 지수 $F_{min}$, $F_{s}t_{s}$로 평가할 수 있었다. Au/Cu/Cr UBM은 젖음시간의 측면에서 Au/Ni/Ti UBM보다 젖음성이 우수하였다 Si-wafer에 단면 코팅된 UBM과 Sn-Pb 솔더의 접촉각을 $F_{s}$와 기울어짐각을 측정하고 메니스커스의 정적상태에서 힘의 평형으로부터 유도된 식을 이용하여 계산할 수 있었다.

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Effect of Improved Surface Wetability and Adhesion of Undulated Diamond-like Carbon Structure with r.f. PE-CVD

  • Jang, Young-Jun;Kim, Seock-Sam
    • KSTLE International Journal
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    • 제9권1_2호
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    • pp.22-25
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    • 2008
  • This paper investigated the wetting and adhesion property of undulated DLC film with surface morphology controlled for a reduced real area of contact. The undulated DLC Films were prepared by 13.56 MHZ radio frequency plasma enhanced chemical vapor deposition (r.f. PECVD) by using nanoscale Cu dots surface on a Si (100) substrate. FE-SEM, AFM analysis showed that the after repeated deposition and plasma induced damage with Ar ions, the surface was nanoscale undulated. This phenomenon changed the surface morphology of DLC surface. Raman spectra of film with changed morphology revealed that the plasma induced damage with Ar ions significantly suppressed the graphitization of DLC structure. Also, it was observed that while the untreated flat DLC surfaces had wetting angle starting ranged from $72^{\circ}$ and adhesion force of 333ni. Had wetting angle the undulated DLC surfaces, which resemble the surface morphology of a cylindrical shape, increased up to $104^{\circ}$ and adhesion force decreased down to 11 nN. The measurements agree with Hertz and JKR models. The surface undulation was affected mainly by several factors: the surface morphology affinity to cylindrical shape, reduction of the real area of contact and air pockets trapped in cylindrical asperities of the surface.

Wetting properties between silver-copper-titanium braze alloy and hexagonal boron nitride

  • Sechi, Yoshihisa;Matsumoto, Taihei;Nakata, Kazuhiro
    • 대한용접접합학회:학술대회논문집
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    • 대한용접접합학회 2009년 추계학술발표대회
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    • pp.205-209
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    • 2009
  • Wetting properties between silver-copper-titanium braze alloys with different titanium contents up to 2.8 mass% and hexagonal boron nitride ceramics were investigated using sessile drop method at 1123K in Argon. The final contact angle is less than $30^{\circ}$ when the Ti content was over 0.41 mass%. Meanwhile, the contact angle curves show different behavior. In case of using braze alloy containing 2.8 mass% of titanium, the initial contact angle is acute angle just after the melting of braze. In case of brazes containing titanium less than 2.26 mass%, the contact angle is larger than $90^{\circ}$ at the beginning and slowly decreases to acute angle. The reaction layer of titanium nitride is observed at the interface. In addition, the reaction of Ti in the braze and N in the bulk h-BN seemed to show diffusion limited spreading.

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비이온계 계면활성제 수용액에서 모직물의 표면적심과 액체보유력 향상 (Improvement of Liquid Wetting and Retention Properties of Wool Fabric in Nonionic Surfactant Solutions)

  • 김천희
    • 한국염색가공학회지
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    • 제21권2호
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    • pp.7-13
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    • 2009
  • The effects of 0.1g/dl nonionic surfactant solutions on liquid wetting and retention properties of wool fabric are reported. The 10 different nonionic surfactants (Span 20, Tween 20, 40, 60, 80, 21, 61, 81, 65, 85), wool cloth (EMPA 217), and wool soiled cloth (EMPA 107) are used in the study. Both EMPA 217 and 107 have water contact angle($\Theta$)>$90^{\circ}$, which indicates that water spreading over a fabric surface and penetration into the fabric rarely occur. However, EMPA 217 and 107 are easily wetted with perchloroethylene(PCE) having very low values of $\Theta$'s and high values of liquid retention. Water wetting properties are greatly improved by adding nonionic surfactants into the system. Generally, hydrophilic surfactants which have low number of carbon atoms or unsaturated hydrophobic structures are effective in improving water wetting of wool fabrics. The water retention of EMPA 217 and 107 in surfactant solutions have positive relations with $cos{\Theta}$, adhesion tension, and work of adhesion. 40.3% pore volume of EMPA 217 and 26.1% pore volume of EMPA 217 can be filled with water even when we assume $cos{\Theta}=1$ (${\Theta}=0^{\circ}$).