• Title/Summary/Keyword: volatile component

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Distinguishing Aroma Profile of Highly-Marbled Beef according to Quality Grade using Electronic Nose Sensors Data and Chemometrics Approach

  • Utama, Dicky Tri;Jang, Aera;Kim, Gur Yoo;Kang, Sun-Moon;Lee, Sung Ki
    • Food Science of Animal Resources
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    • v.42 no.2
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    • pp.240-251
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    • 2022
  • Fat deposition in animal muscles differs according to the genetics and muscle anatomical locations. Moreover, different fat to lean muscle ratios (quality grade, QG) might contribute to aroma development in highly marbled beef. Scientific evidence is required to determine whether the abundance of aroma volatiles is positively correlated with the amount of fat in highly marbled beef. Therefore, this study aims to investigate the effect of QG on beef aroma profile using electronic nose data and a chemometric approach. An electronic nose with metal oxide semiconductors was used, and discrimination was performed using multivariate analysis, including principal component analysis and hierarchical clustering. The M. longissimus lumborum (striploin) of QG 1++, 1+, 1, and 2 of Hanwoo steers (n=6), finished under identical feeding systems on similar farms, were used. In contrast to the proportion of monounsaturated fatty acids (MUFAs), the abundance of volatile compounds and the proportion of polyunsaturated fatty acids (PUFAs) decreased as the QG increased. The aroma profile of striploin from carcasses of different QGs was well-discriminated. QG1++ was close to QG1+, while QG1 and QG2 were within a cluster. In conclusion, aroma development in beef is strongly influenced by fat deposition, particularly the fat-to-lean muscle ratio with regard to the proportion of PUFA. As MUFA slows down the oxidation and release of volatile compounds, leaner beef containing a higher proportion of PUFA produces more volatile compounds than beef with a higher amount of intramuscular fat.

Comparative Analysis of Volatile Flavor Compounds from Zanthoxylum pipperitum A.P. DC

  • Chang, Kyung-Mi;Kim, Gun-Hee
    • Preventive Nutrition and Food Science
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    • v.13 no.1
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    • pp.33-39
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    • 2008
  • The volatile flavor components of Zanthoxylum pipperitum A.P. DC. produced in Korea and China were isolated using a Clevenger-type apparatus by steam distillation extraction, and analyzed by gas chromatography-mass spectrometry (GC/MS). The yields of oils from Korean and Chinese Z. pipperitum A.P. DC. were 2.0 and 1.2% (w/w), respectively. From the two Z. pipperitum A.P. DC. oils, sixty and fifty-four volatile flavor compounds were tentatively identified, and they constituted 94.78 and 87.34% of the total peak area, respectively. Piperitone(p-menth-1-en-3-one) (13.48%) was the most abundant compound in the Chinese Zanthoxylum pipperitum A.P. DC. oil, followed by $\beta$-phellandrene, sabinene, terpinen-4-ol and linalool (each >5%). Whereas, the most abundant compound in the Korean Zanthoxylum pipperitum A.P. DC. oil was limonene (18.04%), followed by geranyl acetate, cryptone, citronellal, cuminal and phellandral (each >5%).

Analysis of Volatile Flavor Compounds in Milk Using Electronic Nose System (전자코 시스템을 이용한 우유의 품질에 따른 휘발성 향기성분 분석)

  • Kang, Nae Kyung;Jun, Tae-Sun;Yang, Yoon Seok;Kim, Yong Shin
    • Journal of Sensor Science and Technology
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    • v.23 no.5
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    • pp.320-325
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    • 2014
  • Volatile flavor compounds from milk were analyzed and identified by using the analysis methods of headspace solid phase microextraction gas chromatography/mass spectrometry (HSPME-GC/MS) and electronic nose (E-Nose) system. About 30 volatile compounds were identified by HSPME-GC/MS for the fresh and off-flavor milk samples. Also, the correlation between rancidity and ageing days of milk was obtained by the aid of principal component analysis algorithm. It shows that the E-Nose system can identify the various types of milk flavor. These results imply that the analysis method based on the E-nose system can apply to the quality control of milk flavor and the rancidity.

Volatile Components of Perillae folium (자소엽의 휘발성 성분)

  • Jang, Hee-Jin;Park, Jun-Young;Kim, Yong-Tae
    • Korean Journal of Food Science and Technology
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    • v.23 no.2
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    • pp.129-132
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    • 1991
  • The volatile components of Perillae folium were isolated by simultaneous steam distillation-extraction method, and analyzed by combined GC and GC-MS. Among seventeen components indentified 6 alcohols (3-octanol, 1-octen-3-ol, linalool, nerolidol, supathuleol and phytol), 2 ketones, 1 aldehyde, 1 phenol and 7 hydrocarbons were confirmed. The most abundant component was myristicin comprising about 53.4%.

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Volatile components of Du-Chung barks (두충껍질의 휘발성 성분)

  • Jang, Hee-Jin;Ra, Do-Young;Kim, Ok-Chan;Park, Jun-Young
    • Applied Biological Chemistry
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    • v.33 no.2
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    • pp.116-119
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    • 1990
  • The volatile components of the barks of Eucommia ulmoides Oliver were extracts simutaneous steam distillation-extraction apparatus, and analyzed by combined GC and GC-MS. Forty nine componets, including 4 acids, 11 alcohols, 9 aldehydes, 4 esters, 3 ketones, 16 hydrocarbons, 1 lactone were confirmed in Eucommiae cortexs. Among total volatiles the most component was caproic acid comprising about 18.1%.

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Studies on the Volatile Compounds of Du-Chung Leaves (두충엽의 휘발성 성분에 관한 연구)

  • Jang, Hee-Jin;Kim, Ok-Chan
    • Korean Journal of Food Science and Technology
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    • v.22 no.3
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    • pp.261-265
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    • 1990
  • The volatile components of Eucommiae foliums were extracted by simultaneous steam distillation-extraction apparatus, and analyzed by combined gas chromatography (GC) and gas chromatography-mass spectrometry(CC-MS). Thirty five components, including 7 alcohols, 3 aldehydes, 4 ketones, 2 esters. 18 hydrocarbons and 1 phenol were confirmed in Eucommiae foliums. Among total volatiles the main component it appeared to be 2-ethyl furyl acrolein, comprising about 31.4%.

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Volatile Aroma Composition of Chrysanthemum indicum L. Flower Oil

  • Chang, Kyung-Mi;Kim, Gun-Hee
    • Preventive Nutrition and Food Science
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    • v.13 no.2
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    • pp.122-127
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    • 2008
  • The aroma constituents of Chrysanthemum indicum L. were separated by the hydro distillation extraction method using a Clevenger-type apparatus, and were analyzed by gas chromatography-mass spectrometry (GC/MS). The yield of Chrysanthemum indicum L. flower oil was 2.0% (w/w) and the color was light golden yellow. Sixty-three volatile flavor components, which make up 89.28% of the total aroma composition of the flower oil, were tentatively characterized. This essential oil contained 35 hydrocarbons (48.75%), 12 alcohols (19.92%), 6 ketones (15.31%), 3 esters (4.61%), 5 aldehydes (0.43%), 1 oxide (0.22%), and 1 miscellaneous component (0.04%). ${\alpha}$-Pinene (14.63%), 1,8-cineol (10.71%) and chrysanthenone (10.01%) were the predominant volatile components in Chrysanthemum indicum L., an aromatic medicinal herbaceous plant.

Removal Rates of VOCs(Volatile Organic Compounds) for Treatment Condition using DAF(Dissolved Air Flotation) in Water Treatment (DAF(Dissolved Air Flotation)를 이용한 정수처리에서 처리조건에 따른 VOCs(Volatile Organic Compounds)의 처리효율에 대한 연구)

  • Kim, Mi-Jeong;Jun, Se-Jin
    • Journal of Korean Society of Water and Wastewater
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    • v.13 no.3
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    • pp.91-100
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    • 1999
  • Treatment conditions of DAF(Dissolved Air Flotation) and removal rates of VOCs(Volatile Organic Compounds) in mixed water of H raw water and VOCs were investigated. The used VOCs were benzene, toluene, ethylbenzene, and xylene in aromatic compounds and iso propyl mereaptan, n-butyl mereaptan, dimethyl disulfide, and iso butyl mercaptan in odors. The related parameters include water type, treatment method, clay concentration, pH condition, flocculation time, flotation time, per-cent recycle, water temperature, pressure. The removal rates of VOCs were different on treatment process and water condition. Treatment time was longer, removal rates of VOCs was higher. Water temperature was more important than pressure in DAF parameters. Molecular weight was related with removal rate in several kinds of VOCs were decraesed by competition of each component in II raw water. When algac blooming D water was treated by DAF, TCOD(Total chemical Oxygen Demand) and chorophyll a was removed over 96%.

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Changes of Aroma and Volatile Components of Korean Leaf Tobaccos from a Different Stalk Positions (국산 원료잎담배의 착엽위치에 따른 향기성분 및 휘발성 성분의 변화)

  • Hwang Keon- Jung;Rhee Moon-Soo;Kim Chung Ryul
    • Journal of the Korean Society of Tobacco Science
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    • v.27 no.1 s.53
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    • pp.127-133
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    • 2005
  • This study was conducted to determine the aroma and volatile component changes from a different stalk positions of Korean flue-cured tobacco. Eight different stalk positions of flue-cured leaf tobaccos harvested in 2001 were used for this study. Thermal extraction method at two different treatment temperature($50\;amp;\;80^{\circ}C$) was applied for this experiment. Forty eight kinds of aroma and volatile components such as 2,4-heptadienal, hexadecane, 1-methyl-1H- pyridine, 2,5-dimethyl-1H-pyrrole were analyzed by using thermal extraction method. All of aroma and volatile components of leaf tobaccos were changed from a different stalk positions and treatment temperature. Leaf tobaccos in middle stalk position have a higher concentration of aroma and volatile components such as norsolanidione, 4-pyridinecarboxaldehyde, 4-methyl-4-OH-2-pentanone, acetic acid, propylene glycol, 1-methyl-2-pyrrolidinone, 2,5-dimethyl-1H-pyrrole. Also, Megastigmatrienone 1, 3-oxo-[alpha]­ionol, 6,10,14-trimethyl-2-pentadecanone, heptadecane, 6-methyl-2-isohexyl-l-heptene concentration were low in the middle stalk position and high in both bottom and upper position. Treatment temperature affected on the changes of many aroma and volatile components in leaf tobacco. Most of aroma and volatile components such as, 2,4-Heptadienal, dodecanoic methylester, famesol isomer and 3-acetylpyridine were sharply increased as increasing treatment temperature. This results can be used to estimate the aroma characteristics of cigarette blend using a different stalk position of leaf tobacco.

Major volatile components of cooked glutinous rice (찹쌀밥의 주요 휘발성 성분)

  • Lee, B.Y.;Son, J.R.;Yoon, I.H.;Ushio, Matsukura;Imai, Toru;Akio, Maekawa
    • Applied Biological Chemistry
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    • v.36 no.2
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    • pp.111-114
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    • 1993
  • The volatile components of cooked glutinous rice were investigated. Among more than 100 volatile components of fresh cooked rice, the predominant one was hexanal followed by pentanal, butanal, octanal, heptanal, noananal, acetone and toluene. These eight components comprised about 85% of the total volatiles, and the hexanal comprised about 86% total amount of the eight volatile components. the amount of the eight volatile components and hexanal in cooked glutinous rice were six and nine times more than that of cooked nonglutinous rice, respectively. The amount of volatile components in cooked glutinous rice stored for 72 hours at $70^{\circ}C$ was same with that of in nonglutinous rice immediately after cooking.

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