• Journal of Powder Materials
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• v.22 no.5
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• pp.356-361
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• 2015

Fe-30 wt% TiC composite powders are fabricated by in situ reaction synthesis after planetary ball milling of (Fe, $TiH_2$, Carbon) powder mixture. Two sintering methods of a pressureless sintering and a spark-plasma sintering are tested to densify the Fe-30 wt% TiC composite powder compacts. Pressureless sintering is performed at 1100, 1200 and $1300^{\circ}C$ for 1-3 hours in a tube furnace under flowing argon gas atmosphere. Spark-plasma sintering is carried out under the following condition: sintering temperature of $1050^{\circ}C$, soaking time of 10 min, sintering pressure of 50 MPa, heating rate of $50^{\circ}C/min$, and in a vacuum of 0.1 Pa. The curves of shrinkage and its derivative (shrinkage rate) are obtained from the data stored automatically during sintering process. The densification behaviors are investigated from the observation of fracture surface and cross-section of the sintered compacts. The pressureless-sintered powder compacts are not densified even after sintering at $1300^{\circ}C$ for 3 h, which shows a relative denstiy of 66.9%. Spark-plasma sintering at $1050^{\circ}C$ for 10 min exhibits nearly full densification of 99.6% relative density under the sintering pressure of 50 MPa.

• Journal of Bio-Environment Control
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• v.18 no.3
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• pp.200-207
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• 2009

This study was conducted to analyze the variations of air temperature, relative humidity and pressure in a low pressure chamber for plant growth. The low pressure chamber was composed of an acrylic cylinder, a stainless plate, a mass flow controller, an elastomer pressure controller, a read-out-box, a vacuum pump, and sensors of air temperature, relative humidity, and pressure. The pressure leakage in the low pressure chamber was greatly affected by the material and connection method of tubes. The leakage rate in the low pressure chamber with the welding of the stainless tubes and a plate decreased by $0.21kPa{\cdot}h^{-1}$, whereas the leakage in the low pressure chamber with teflon tube and rubber O-ring was given by $1.03kPa{\cdot}h^{-1}$. Pressure in the low pressure chamber was sensitively fluctuated by the air temperature inside the chamber. An elastomer pressure controller was installed to keep the pressure in the low pressure chamber at a setting value. However, inside relative humidity at dark period increased to saturation level.. Two levels (25 and 50kPa) of pressure and two levels (500 and 1,000sccm) of mass flow rate were provided to investigate the effect of low pressure and mass flow rate on relative humidity inside the chamber. It was concluded that low setting value of pressure and high mass flow rate of mixed gas were the effective methods to control the pressure and to suppress the excessive rise of relative humidity inside the chamber.

• Journal of Korean Society of Occupational and Environmental Hygiene
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• v.3 no.2
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• pp.188-193
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• 1993

Toluene in air and blood and hippuric acid in urine were checked for the 41 female workers who are exposed to toluene and have normal liver function in shoe making factories in July, 1993. Toluene in air was sampled with charcoal by personal air sampler at least 4 times and analyzed by gas chromatography. At the end of shift, blood and spot urine were collected with a vacuum tube containing EDTA and a polyethylene bottle for detecting blood toluene and urine hippuric acid and analyzed by gas chromatography and high performance liquid chromatography. Means of air and blood toluene and urine hippuric acid concentrations were 34.35ppm, 0.360mg/L, and 1.78g/g creatinine, respectively. Toluene in air showed a good correlation with hippuric acid in urine(r=0.4503) and toluene in blood(r=0.4596). The hippuric acid in urine and toluene in blood corresponded 10 exposure of 100ppm toluene in air were 2.628g/g creatinine and 0.481mg/L. Blood toluene and urine hippuric acid expected ratio were not correlated to the obesity index and working duration, however increased with age.

• Journal of Powder Materials
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• v.22 no.4
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• pp.283-288
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• 2015

Two sintering methods of a pressureless sintering and a spark-plasma sintering are tested to densify the Fe-TiC composite powders which are fabricated by high-energy ball-milling. A powder mixture of Fe and TiC is prepared in a planetary ball mill at a rotation speed of 500 rpm for 1h. Pressureless sintering is performed at 1100, 1200 and $1300^{\circ}C$ for 1-3 hours in a tube furnace under flowing argon gas atmosphere. Spark-plasma sintering is carried out under the following condition: sintering temperature of $1050^{\circ}C$, soaking time of 10 min, sintering pressure of 50 MPa, heating rate of $50^{\circ}C$, and in a vacuum of 0.1 Pa. The curves of shrinkage and its derivative (shrinkage rate) are obtained from the data stored automatically during sintering process. The densification behaviors are investigated from the observation of fracture surface and cross-section of the sintered compacts. The pressureless-sintered powder compacts show incomplete densification with a relative denstiy of 86.1% after sintering at $1300^{\circ}C$ for 3h. Spark-plasma sintering at $1050^{\circ}C$ for 10 min exhibits nearly complete densification of 98.6% relative density under the sintering pressure of 50 MPa.

• Journal of Korea Foundry Society
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• v.29 no.5
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• pp.220-224
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• 2009

In order to investigate the microstructural morphology of the sulfide expected from the Fe-FeS phase diagram, a vacuum-sealed quartz tube where pure iron (99.9%) and sulfur (99.99%) powders were charged was heated upto $1000^{\circ}C$ in the electric resistance furnace, held for 96 hours and quenched in cold water and then, rod specimen was produced. Compositional difference of the sulfur between upper and lower parts of the rod was 7.5wt.% and segregation of the sulfur was gradually increased from the lower part to the upper one of the rod. The rod specimen was divided into three parts by the microstructural morphology of the sulfide. The upper part of the rod specimen revealed single phase FeS intermetallic. In the middle part of the specimen, hyper-eutectic microstructure where primary FeS was precipitated first and then, eutectic of $\alpha$-Fe and FeS was formed in the inter-dendritic region of the FeS. Especially, hypo-eutectic microstructure was appeared in the lower part of the specimen. After primary dendrite of $\alpha$-Fe solidified, FeS dendrite which included small amount of $\alpha$-Fe and FeS eutectic in the inter-dendritic region was formed.

• Current Photovoltaic Research
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• v.2 no.3
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• pp.115-119
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• 2014

$Cu(In,Ga)Se_2$ (CIGS) thin films have been used as a light absorbing layer in high-efficiency solar cells. In order to improve the quality of the CIGS thin film, often selenization step is applied. Especially when the thin film was formed by non-vacuum powder process, selenization can help to induce grain growth of powder and densification of the thin film. However, selenization is not trivial. It requires either the use of toxic gas, $H_2Se$, or expensive equipment which raises the overall manufacturing cost. Herein, we would like to deliver a new, simple method for selenization. In this method, instead of using a costly two-zone furnace, use of a regular tube furnace is required and selenium is supplied by a mixture of selenium and ceramic powder such as alumina. By adjusting the ratio of selenium vs. alumina powder, selenium vaporization can be carefully controlled. Under the optimized condition, steady supply of selenium vapor was possible which was evidently shown by large grain growth of CIGS within a thin powder layer.

• Journal of the Korean Solar Energy Society
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• v.30 no.6
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• pp.28-33
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• 2010

Solar collectors to be applied are mainly flat-plate or vacuum tube collector which is used for hot water supply of house because of low heat value and low temperature. There are a necessity to expand applicable scope of solar collector into the industrial process heat source and air conditioner for coping with renewable energy policy of government and industrial trend. This study is to analysis the performance of PTC solar collector of concentrating type and flat-plate of non-concentrating. For this, temperature difference and heating value as insolation of air outside is measured from these two collectors mounted on 2-axial solar tracking system. It is investigated that temperature profile obtained from PTC solar collector is uniform and collecting heat per unit area is 6.8kcal/$m^2$ min which is about 3 times with compare to flat-plate collector of 2kcal/$m^2$min. Also the amount of heat to be produced from PTC solar collector is 3 Mcal/$m^2$ which is about 2 times with compare to flat-plate collector of 1.5Mcal/$m^2$ as a result of operating these two collectors during one month. Therefore, it is obtained that heat collecting performance of PTC solar collector is superior to flat-plate.

• Korean Journal of Materials Research
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• v.5 no.6
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• pp.682-689
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• 1995

In order to refine the grain size of Mg-Zn alloy 0.5 to 6wt.%Cu or Si elements were added. Alloy ingot was made under vacuum atmosphere of 4 ${\times}$ 10$\^$-4/ Torr in the quartz tube coated by BN. Grain size and hardness were measured after solution treatment for 8 hours at 435$^{\circ}C$. Optimal condition for grain size refining effect was obtained at the minimum composition of 2wt.%Cu or 1.5wt.%Si addition to Mg-6wt%Zn alloy. Age hardening behavior was experimented at the optimal compositions of the Mg-6wt.%Zn, Mg-6wt.% Zn-2wt.%Cu and Mg-6wt.% Zn-1.5wt.%Si. The hardness increment due to fine grain size was higher at the Mg-Zn-Cu alloy system, but that due to age hardening was higher at the Mg-Zn-Si alloy system.

• Journal of Korean Society on Water Environment
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• v.22 no.3
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• pp.534-539
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• 2006

The supply of oxygen for aeration is the largest energy consumer at activated sludge wastewater treatment plants. Replacement of less efficient aeration systems with fine pore aeration devices can save up to 50 percent of aeration energy costs. The purpose of this study was the diagnosis and evaluation of a domestic wastewater aeration system by the off-gas method which had been studied by US EPA and ASCE. For this study, an off-gas analyzer and its hood were made to collect off-gas. Also, a vacuum pump was connected to the analyzer to make suction of off-gas. Experiments were conducted at a domestic activated sludge wastewater treatment plant which had a single spiral roll aeration system installed with P.E tube diffuser. Data on OTE(f), SOTE(pw), OUR, and air flow rate were obtained from these experiments. In case of replacing an aeration system, it is recommended that it should be replaced with perforated membrane disc or ceramic disc fine bubble diffusers installed in a full floor coverage or grid pattern.

• Journal of the Korean Solar Energy Society
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• v.28 no.5
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• pp.21-27
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• 2008

In this study, the design of the solar heating system for district heating as well as it's operating characteristics and the performance analysis was carried out. This solar district heating system was composed of two different types of solar collector circuit, flat plate and vacuum tube solar collector, in a system. This system supply constant temperature of hot water without solar buffer tank. For this, the proportional(variable flow rate) control was used. The experimental facility for this study was used the Bundang district solar heating system which was installed in the end of 2006. The operating characteristics and behaviour of each collector circuits are investigated especially for the system design and control. The yearly solar thermal efficiency is 47.5% on the basis of aperture area and 39.8% on the basis of gross area of collector. As a result this solar heating system without solar buffer tank and with proportional controller was testified a very effective and simplified system for district heating. It varied especially depend on the weather condition like as solar radiation and ambient temperature.