• Title/Summary/Keyword: vacuum pressure

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Effects of pressure during the synthesis of petroleum pitch precursors in open and closed systems

  • Choi, Jong-Eun;Ko, Seunghyun;Kim, Jong Gu;Jeon, Young-Pyo
    • Carbon letters
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    • v.25
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    • pp.95-102
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    • 2018
  • We examined the pressure effects on petroleum pitch synthesis by using open and closed reaction systems. The pressure effects that occur during the pitch synthesis were investigated in three pressure systems: a closed system of high pressure and two open systems under either an atmosphere or vacuum. A thermal reaction in the closed system led to the high product yield of a pitch by suppressing the release of light components in pyrolysis fuel oil. Atmospheric treatment mainly enhanced the polymerization degree of the pitch via condensation and a polymerization reaction. Vacuum treatment results in a softening point increase due to the removal of components with low molecular weights. To utilize such characteristic effects of system pressure during pitch preparations, we proposed a method for synthesizing cost-competitive pitch precursors for carbon materials. The first step is to increase product yield by using a closed system; the second step is to increase the degree of polymerization toward the desired molecular distribution, followed by the use of vacuum treatment to adjust softening points. Thus, we obtained an experimental quinoline insolubles-free pitch of product yield over 45% with softening points of approximately $130^{\circ}C$. The proposed method shows the possibility to prepare cost-competitive pitch precursors for carbon materials by enhancing product yield and other properties.

New calibration apparatus for a precise barometer (초정밀 기압계 교정을 위한 새로운 압력계 교정장치 개발)

  • 우삼용;이용재;최인묵;김부식;최종운
    • Journal of the Korean Vacuum Society
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    • v.12 no.3
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    • pp.157-161
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    • 2003
  • Nowadays there are increasing demands for more accurate measurement of atmospheric pressure according to the development of environmental industries. One of the most important pressure gauges for satisfying these demands is a quartz resonance barometer. In order to calibrate such an accurate barometer, laser/ultrasonic mercury manometers have been used. However, complexity and cost of mercury manometers made it out of use gradually. As a substitute, a gas-operated pressure balance is used for calibration of precise barometers. In such a case, commercially available pressure balances cannot be entirely suitable because consequent exposure of the piston, cylinder and masses to the atmosphere causes the problem of contamination. In this paper a device for changing the masses in situ without breaking the vacuum is described. This device made it possible to add or remove weights in the absolute mode, thereby greatly reducing the time between observations. At the same time, we investigated the characteristics of a commercial precise barometer using this new apparatus.

Consolidation Behaviour of Dredged Clay Ground Improved by Horizontal Drain Method (수평배수공법에 의해 개량된 준설점토지반의 압밀거동에 관한 연구)

  • 김형주;원명수
    • Geotechnical Engineering
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    • v.13 no.1
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    • pp.137-146
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    • 1997
  • In this study, a large consolidation test was carried out to estimate the consolidation behaviour of dredged clay ground improved by horizontal drain using plastic board drain with a vacuum pressure. The test results were analyzed by a numerical simulation using potential consolidation theory applied to a hollow cylinder. The rapid decreases in pore pressure and the drain speed in the plastic board indicate that the consolidation occurred quickly after the vacuum state was applied to the test soil. According to the numerical analysis obtained by applying the linear potential consolidation theory to a clay hollow cylinder with external radial drainage, the pore pressure is affected by the strain and the permeability of the soil rather than by the diffusion types. Therefore, measured surface settlement agreed with the numerical solution at the point where consolidation pressure increasing rate u: -0.5. Also the behaviour of the clay layer settlement in the place where the drain was installed was similar to that shown in Barron's consolidation theory. Finally, the design and construction procedure including the selection of the appropriate arrangement of horizontal drains were discussed based on the results of the laboratory tutsts. It is also shown that the potential consolidation theory make it possible to predict consolidation behaviour in the field using horizontal drains exactly.

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A Review on the Performance Criteria of Equipment Required for Asbestos Removal (석면 해체.제거 작업에서 사용되는 장비의 성능 기준에 관한 고찰)

  • Lee, Naroo
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.23 no.3
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    • pp.212-221
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    • 2013
  • Objectives: Asbestos fibers are accumulated in negative pressure unit (NPU) or vacuum cleaner in asbestos removal. Failure of operation or poor use performance of the NPU or vacuum cleaner causes asbestos fibers to spread in the air. Asbestos contractors should have an NPU fitted with a HEPA , vacuum cleaner, decontamination area, respirators, wetting equipment, and differential pressure manometer to register with the Ministry of Employment and Labor. There should be performance criteria of equipment used in asbestos removal. But there are none such criteria used in asbestos removal. This study was performed to investigate international or national performance criteria of equipment used in asbestos removal. Methods: Regulations, approved code of practice, guidance and national standards of the UK, USA and Korea were reviewed. A survey was done to investigate the requirements for equipment used in asbestos removal in Korea. Results: Air flow of NPUs used in Korea usually covers from$500m^3/h$ to over $3000m^3/h$. Some requirements for NPUs used in Korea were missing compared to the requirements of British standards for NPUs. All NPUs have different missing requirements. The UK also has separate British standard for leak tests for NPUs. Highly hazardous class vacuum cleaners should be used in asbestos removal in the UK. It has national standards on the operation of vacuum cleaners used in asbestos removal. There is only a certification system for less than 2.5kw rated voltage vacuum cleaners for home use in Korea. Powered (-assisted) respirators with mask are recommended in asbestos removal. Type 5 coveralls should be used in asbestos removal in the UK. There are international standards for requirements and leak tests of type 5 coveralls. A manometer for measuring differential pressure is needed in asbestos removal. The manometer's measuring range should cover less than ${\pm}125$ Pa and the gradation of manometer should be less than 2.5 Pa. The definition of decontamination area should be corrected. Installation of airlock and minimum area should be considered in decontamination area. Conclusions: Equipment should be used in asbestos removal proper performance and no leaks. There should be a certification system for equipment used in asbestos removal. This study can help to a certification system for equipment used in asbestos removal in Korea.

Assessment of DTVC Operation Efficiency for the Simulation of High Vacuum and Cryogenic Lunar Surface Environment (고진공 및 극저온 달의 지상 환경 재현을 위한 지반열진공챔버 운영 효율성 평가)

  • Jin, Hyunwoo;Chung, Taeil;Lee, Jangguen;Shin, Hyu-Soung;Ryu, Byung Hyun
    • Journal of the Korean Geotechnical Society
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    • v.38 no.12
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    • pp.125-134
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    • 2022
  • The Global Expansion Roadmap published by the International Space Exploration Coordination Group, which is organized by space agencies around the world, presents future lunar exploration guidance and stresses a lunar habitat program to utilize lunar resources. The Moon attracts attention as an outpost for deep space exploration. Simulating lunar surface environments is required to evaluate the performances of various equipment for future lunar surface missions. In this paper, an experimental study was conducted to simulate high vacuum pressure and cryogenic temperature of the permanent shadow regions in the lunar south pole, which is a promising candidate for landing and outpost construction. The establishment of an efficient dirty thermal vacuum chamber (DTVC) operation process has never been presented. One-dimensional ground cooling tests were conducted with various vacuum pressures with the Korean Lunar Simulant type-1 (KLS-1) in DTVC. The most advantageous vacuum pressure was found to be 30-80 mbar, considering the cooling efficiency and equipment stability. However, peripheral cooling is also required to simulate a cryogenic for not sublimating ice in a high vacuum pressure. In this study, an efficient peripheral cooling operation process was proposed by applying the frost ratio concept.

Development of the Dual Cyclone System for a High Efficient Vacuum Cleaner (사이클론 집진 원리를 적용한 진공청소기 개발에 관한 연구)

  • Lee, Jae-Keun;Lee, Jung-Eun;Kim, Seong-Chan;Cho, Min-Chul;Hyun, Choong-Nam;Kwack, Dong-Jin;Lim, Kyung-Suk;Lee, Sung-Hwa;Yang, Byung-Sun;Ji, Heon-Pyung;Jeong, Hoi-Kil;Park, Deog-Bae;Liu, Benjamin Y.H.
    • Proceedings of the KSME Conference
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    • 2000.04b
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    • pp.644-649
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    • 2000
  • A new cyclone system for the vacuum cleaner to collect dusts has been studied experimentally and numerically to meet the constant suction power, hygienic exhaust and a reduction of maintenance cost. The cyclone system of the vacuum cleaner consists of twin cyclones for improving dust collection efficiency. The first. cyclone catches large dust particles and the second one having two separated flows to decrease pressure drop collects small dust particles. The optimal design factors such as dust collection efficiency, pressure drop, and cut-size are investigated from the experimental results by the Taguchi method. Cyclone cleaner systems designed in this study has a good Performance taking into account the dust collection efficiency of 93% and the cut-size of $1.6{\mu}m$ in mass median diameter at the flow rate of 1 CMM. The cyclone vacuum cleaner showed the potential to be an effective method to collect dusts generated in the household.

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An Experimental Study of a Diffuser Starting Characteristics for Simulating High-Altitude Environment by using a Liquid Rocket (액체로켓엔진 연소기를 이용한 고고도 환경 모사용 디퓨저 시동특성 연구)

  • Lee, Yang-Suk;Jeon, Jun-Su;Ko, Young-Sung;Kim, Yoo;Kim, Sun-Jin
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.38 no.12
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    • pp.1195-1201
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    • 2010
  • Performance tests of a supersonic exhaust diffuser were conducted by using a liquid rocket engine for simulating high-altitude environment. The experimental setup consisted of a combustion chamber, a vacuum chamber and a diffuser. The combustion tests for simulating high-altitude environment were carried out at three cases by chamber pressure variation(26, 29, 32barg). The test results showed that the diffuser was started at all case and vacuum chamber pressures were approximately 140torr. The starting pressure using combustion gas was similar with that of cold gas, but the vacuum chamber pressure was relatively high because of high temperature in the vacuum chamber. The results of this test can be used as an essential database for the design of real-scale high-altitude simulation test facility in the future.

Effects of Base Vacuum Level on Discharge Characteristics in Vacuum In-Line Sealing Process for High Efficient PDP

  • Kwon, Sang-Jik;Jang, Chan-Kyu
    • Journal of Information Display
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    • v.5 no.4
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    • pp.7-11
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    • 2004
  • Effects of base vacuum level on the electrical and optical characteristics of the plasma display panel (PDP) were investigated. The relationship between efficiency and base vacuum level before filling discharge gas was analyzed. For the base vacuum level of $1{\times}10^{-4}$ torr, firing voltage of a 2-inch diagonal PDP panel was 232 V at the discharge gas pressure of 400 torr and luminous efficiency was 1.5 lm/W at 180V sustaining pulse. On the other hand for $1{\times}10^{-6}$torr, the firing voltage was reduced to 215 V and luminous efficiency was improved considerably to 2.5 lm/W. We successfully demonstrated the smooth operation of tip-less PDP fabricated using vacuum in-line sealing method.

Development of the Cryostat Vessel for KSTAR Tokamak (KSTAR 토카막용 저온용기 개발)

  • Her, Nam-Il;Kim, Byung-Chul;Hong, Kwen-Hi;Kim, Geun-Hong;Shin, Hoon;Park, Kyung-Ho;Park, Joo-Shik
    • Proceedings of the KSME Conference
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    • 2004.11a
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    • pp.545-550
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    • 2004
  • KSTAR cryostat is a 8.8 m diameter vacuum vessel that provides the necessary thermal barrier between the ambient temperature test cell and the supercritical helium cooled superconducting magnet providing the base pressure of 1 ${\times}$ $10^{-3}Pa$. The cryostat is a single walled vessel consisting of central cylindrical section and two end closures, a flat base structure with external reinforcements and a dome-shaped lid structure. The base structure has 8 equally spaced support legs anchored on the concrete base. The cryostat vessel design was executed to satisfy the performance and operation requirements. The major loads considered in the structural analysis were vacuum pressure, dead weight, electromagnetic load driven by plasma disruption, and seismic load. Based on the fabrication and inspection procedures for the vessel, cryostat vessel was fabricated and inspected. It was confirmed that the inspection results were acceptable.

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Experimental Study of High-Altitude Simulation using Small-Scale Supersonic Diffuser (소형 초음속 디퓨저를 이용한 고고도환경 모사에 대한 시험적 연구)

  • Lee Ji-Hyung;Oh Jong-Yun;Byun Jong-Ryul
    • Journal of the Korea Institute of Military Science and Technology
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    • v.7 no.4 s.19
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    • pp.138-145
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    • 2004
  • Experimental study was conducted on cylindrical supersonic diffuser in order to investigate the effects of the ratios of diffuser area to nozzle throat area (Ad/At), diffuser area to nozzle exit area (Ad/Ae), nozzle exit area to its throat area (Ae/At), and diffuser length to its diameter (L/D), the free volume of vacuum chamber, and the relative distance between nozzle exit and diffuser inlet on the diffuser performance. The study showed that the minimum diffuser starting pressure (Po/Pa)st increased monotonically with increase in (Ad/At) as predicted by the normal shock and momentum theory models and the volume of vacuum chamber affected vacuum pressure level during diffuser operation at lower value of (Ad/Ae). The results of this investigation will be utilized in the design of real-scale high-altitude simulation test facility.