• Nuclear Engineering and Technology
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• 제32권1호
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• pp.77-87
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• 2000

It is reported that the toughness and safety margins of the SA106 Gr.C main steam line piping steel is reduced due to dynamic strain aging (DSA) at the reactor operating temperature for Leak-Before-Break (LBB) application. In this study, intercritical annealing in two-phase ($\alpha$+${\gamma}$）region was performed to investigate the possibility of improving the toughness and reducing DSA susceptibility. The manifestations of DSA were still observed in the tensile tests of the annealed specimens. However, the ductility loss caused by DSA was smaller than that in the as-received material. Furthermore, the intercritical annealing was able to increase the Charpy impact toughness by 1.5 times compared to as-received. With the heat treatment, we could obtain microstructural changes such as the cleaner retained ferrite, increased ferrite content and somewhat finer grain size. It is considered that the reduced DSA was induced by cleaner retained ferrite, which in turn resulted in higher impact toughness in addition to the general toughening due to finer grain sizes and increased ferrite content.

• 한국주조공학회지
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• 제19권1호
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• pp.77-83
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• 1999

Strip casting process, a new casting technology which makes thin strip of $0.5{\sim}5\;mm$ thickness directly from molten metal, has been dramatically developed for past 10 years and faced commercialization in the case of STS304 strip. In this study, ductile cast iron strip which is 1.1 mm thick and 100 mm wide is manufactured by the twin roll strip caster. Graphite and matrix structure of the strip can be controlled through heat treatments and the mechanical properties are examined. The microstructure of the as-cast strip consists of cementite and pearlite. Especially the equiaxed crystal zone of pearlite exists in the center region of the thickness due to the characteristics of the strip casting process. Matrix structure can be transformed into fully ferrite or ferrite/pearlite mixed structures by the different graphitization heat treatments. The heat-treated strip with ferrite/pearlite matrix structure showed higher hardness and tensile strength than that with full ferrite matrix structure.

• 한국재료학회지
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• 제24권11호
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• pp.610-616
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• 2014

In this study, we investigated the precipitation behavior of the R-phase precipitated at the initial stage of aging and its effect on the pitting corrosion of 25%Cr-7%Ni-4%Mo super duplex stainless steel. The R-phase in super duplex stainless steel was mainly precipitated at the interface of ferrite/austenite phases and inside of the ferrite phase during the initial stage of aging, and it was transformed into the ${\sigma}$-phase with an increase in aging time. The ferrite phase was decomposed into a new austenite phase and ${\sigma}$-phase. The R phase was an intermetallic compound, which represented a lower Ni and higher Mo than the matrix, and also had a higher Mo and Cr concentration than the ${\sigma}$ phase. With an increasing aging time, the pitting potential $E_p$ was increased slowly by the precipitation of the R-phase, and it was then steeply decreased by the precipitation of the ${\sigma}$-phase. The R-phase was decreased the pitting potential, but its effect was smaller than effect of ${\sigma}$-phase.

• 한국재료학회지
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• 제24권8호
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• pp.401-406
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• 2014

In this study, we investigated the precipitation behavior of the R-phase precipitated at the initial stage of aging and its effects on the mechanical properties of 25%Cr-7%Ni-2%Mo-4%W super duplex stainless steel. The R-phase was mainly precipitated at the interface of ferrite/austenite phases and inside of the ferrite phase during the initial stage of aging. It was transformed into the ${\sigma}$-phase with an increase of the aging time. The ferrite phase was decomposed into a new austenite(${\gamma}_2$)phase and the ${\sigma}$-phase by an aging treatment. The R phase was an intermetallic compound showing higher molybdenum and tungsten concentrations than the matrix and also showed higher molybdenum and tungsten concentrations than the ${\sigma}$ phase. In the initial stage of aging, precipitation of the R-phase did not change the hardness, the strength and the elongation. The hardness and the strength increased upon a longer aging time, but the elongation rapidly decreased. These results show that the R-phase did not significantly affect the hardness and the strength, though it did influence the elongation.

• 대한금속재료학회지
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• 제49권3호
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• pp.197-202
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• 2011

This study was carried out to investigate the precipitation behavior of ${\chi}$ phase and effect of ${\chi}-phase$ which precipitated at the initial stage of aging on mechanical properties of 25%Cr-7%Ni-4%Mo-0.2%N super duplex stainless steel. ${\chi}-phase$ was precipitated mainly at the interface of ferrite / austenite phases and inside of the ferrite phase at the initial stage of aging, and it was transformed into ${\sigma}-phase$ with an increase of aging time. The ferrite phase was decomposed into new $austenite({\gamma}_2)phase$ and ${\sigma}-phase$ by aging treatment. The hardness and tensile strength of the initial stage of aging when ${\chi}-phase$ was precipitated did not changed considerably, while elongation rapidly decreased. Accordingly, it is considered that ${\chi}-phase$ didn't affect the hardness and strength significantly, but it affected the elongation.

• Journal of Welding and Joining
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• 제27권3호
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• pp.52-59
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• 2009

Flash butt welding is applied in many industries. New technology was developed recently for joining billets which called "EBROS (Endless Bar Rolling System)". After reheating billets in furnace, two billets were joined using flash butt welding. The objective of this study was to investigate the effect of alloying elements on mechanical properties of flash butt welded zone of hot rolled steel bar. The tensile properties on welded zone of Fe-Mn steel and Fe-Mn-V steel were dropped as compared with non-welded zone. Fe-Mn-Nb steel was opposed to the former. It was found that the white band at the welded zone had high ferrite volume fraction and large ferrite grain size. The vertical white band between flash butt welded billets was transformed into an arrowhead it of steel bar. According to this band, softening has been appeared. There was a interesting phenomenon with HAZ of Fe-Mn-Nb Steel, 40nm scale of particles were observed and hardness of HAZ was higher than non-welded zone.

• Journal of Welding and Joining
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• 제31권6호
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• pp.37-43
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• 2013

This study targets to make clear the connection between MS (Martensite start) point and welding shrinkage. We approved that a Martensite-transformed weldment may not yield state under low MS point, but also admitted the limitation of numerical calculation by inherent strain approach or thermal strain approach. Therefore, new thermal strain formulae during cooling stages were made. As a thermal strain is obtained by integrating thermal extension coefficient, a constant of integration should be decided. In our suggested formulae, the origin was based on totally remained austenite, and added strain from volume changes in Martensite transformation was based on totally transformed ferrite. Through the suggested methodology, It is verified that an MS point under a critical temperature can let weld shrinkage relax and the critical value can be obtained. For supporting this process, 15 weld-consumables were made, were tested by fillet type and were measured. As a result, a positive correlation between MS point and level of weld-distortion was obtained, but it was rather weak.

• 한국표면공학회지
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• 제37권1호
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• pp.53-57
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• 2004

Austenitic stainless steel AISI 304 was nitrided in a low-pressure RF plasma using pure nitrogen. With a treatment of time of 4.0h at $400^{\circ}C$, the nitrogen-rich layer on the sample was $3\mu\textrm{m}$thick and had a hardness of approximately 4.4 times higher than that of untreated material. XRD data showed that as the process temperature rose from 350∼$450^{\circ}C$, the expanded austenite peaks became more prominent while the austenite peaks became weaker. Expanded austenite was transformed to ferrite and CrN at the treatment of$ 500^{\circ}C$. Langmuir probe measurements showed that electron density decreased above $450^{\circ}C$.

• Steel and Composite Structures
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• 제39권4호
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• pp.401-417
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• 2021

This study experimentally reveals the influence of welding on grade S690Q high strength steel (HSS) butt joints from both micro and macro levels. Total eight butt joints, taking plate thickness and welding heat input as principal factors, were welded by shielded metal arc welding. In micro level, the microstructure transformations of the coarse grain heat affected zone (CGHAZ), the fine grain heat affected zone (FGHAZ) and the tempering zone occurred during welding were observed under light optical microscopy, and the corresponding mechanical performance of those areas were explored by micro-hardness tests. In macro level, standard tensile tests were conducted to investigate the impacts of welding on tensile behaviour of S690Q HSS butt joints. The test results showed that the main microstructure of S690Q HSS before welding was tempered martensite. After welding, the original microstructure was transformed to granular bainite in the CGHAZ, and to ferrite and cementite in the FGHAZ. For the tempering zone, some temper martensite decomposed to ferrite. The performed micro-hardness tests revealed that an obvious "soft layer" occurred in HAZ, and the HAZ size increased as the heat input increased. However, under the same level of heat input, the HAZ size decreased as the plate thickness increased. Subsequent coupon tensile tests found that all joints eventually failed within the HAZ with reduced tensile strength when compared with the base material. Similar to the size of the HAZ, the reduction of tensile strength increased as the welding heat input increased but decreased as the thickness of the plate increased.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2001년도 춘계학술대회 논문집
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• pp.156-160
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• 2001

The effects of TRansformation Induced Plasticity(TRIP) phenomena on the plastic deformation of 0.2C-1.5Si-1.5Mn multiphase steels have been investigated at various heat treatment and stress conditions. In order to estimate the formability, the hole expansion(HE) tests and the tensile tests were carried out. The formability evaluated from the uni-axial tensile tests was quite different from the formability measured from multi-axial HE-tests. Consequently, the formability in the multi-axial stress state decreased due to the extinction of the retained austenite relatively at earlier deformation stage and the production of irregular α' martensite. However, the defects of TRIP-steels were initiated exactly at the boundary between transformed martensite and ferrite matrix regardless of stress state. In addition, new experimental formula is proposed in order to predict the multi-axial formability of the TRIP steels from the results of uniaxial tensile test.