• Title/Summary/Keyword: toughness characterization

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Characterization of Fracture Toughness and Wear Behavior for Plasma Ceramic Coated Materials (플라즈마 코팅재료의 파괴인성과 마모 거동)

  • Ha, Sun-Ho;Lee, Dong-Woo;Rehman, Atta Ur;Wasy, Abdul;Song, Jung-Il
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.12 no.4
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    • pp.123-130
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    • 2013
  • Zirconia is well known in industrial applications for its mechanical characteristics. DLC (diamond-like carbon) have high elastic modulus, high electric resistivity, high dielectric constant, high wear resistance, low friction coefficient, bio compatibility, chemically inert and thermally stable. Because of all these physical and chemical properties these types of coatings have become key procedure for thin coating. Friction coefficient of DLC films is already evaluated and the current work is a further advancement by calculating the fracture toughness and wear resistance of these coatings. In the present study DLC thin film coatings are developed on $ZrO_2$ alloy surface using Plasma Enhanced Chemical Vapor Deposition (PECVD) method. Vicker hardness test is employed and it was concluded that, DLC coatings increase the Vickers hardness of ceramics.

Characterization of Ductile Metal-FRP Laminated Composites for Strengthening of Structures: Part-II Tensile Behavior (사회기반설물의 내진 보강을 위한 연성재-FRP적층복합체의 역학적 거동 특성 분석: Part-II휨 거동)

  • Park, Cheol-Woo
    • Journal of the Korean Society of Safety
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    • v.27 no.1
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    • pp.55-62
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    • 2012
  • Steel plate or FRP materials have been typically used for the seismic retrofit of civil infrastructures. In order to overcome the limitation of each retrofitting material, a composite material, which takes advantages from both metal and fiber polymer materials, has been developed. In the study herein, the composite retrofitting material consists of metal part(steel or aluminum) and FRP sheet part(glass or carbon fiber). The metal part can enhance the ductility and the FRP part the ultimate strength. As a preliminary study to investigate the fundamental mechanical characteristics of the metal-FRP laminated composite material this study performed the flexural fracture test with various experimental variables including the number, the angle and the combination of FRP laminates. From the aluminum-FRP composite tests no great increase in flexural strength and flexural toughness were observed. However, flexural toughness of steel-FRP laminate composite was increased so that its behavior can be considered in the retrofit design. In addition, the angle and the kind of fibers should be carefully considered in conjunction with the expected loading conditions.

Sintering Characterization of Alumina Powders by Hot Pressing after Cold Cyclic Compaction -Densification, Grain-Growth and Fracture Toughness- (상온 반복압축 후 가압소결에 의한 알루미나 분말의 소결특성 -치밀화와 결정립 성장 및 파괴인성-)

  • Son, G.S.;Suh, J.;Baik, S.K.;Kim, K.T.
    • Journal of the Korean Ceramic Society
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    • v.30 no.1
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    • pp.62-68
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    • 1993
  • Densification of alumina powder, grain size and fracture toughness of sintered body by hot pressing after cold compaction were investigated and compared to traditional hot pressing process (without cold cyclic compaction). To achieve a higher densification and to reduce the hot pressing time, hot pressing after cold cyclic compaction was more efficient compared to traditional hot pressing. This phenomenon resulted from the increment of packing densityby the acceleration fo rearrangement of powders under cold cyclic compaction. The grain size of sintered body was only dependent on relative density, and densification during hot pressing was governed by thelattice diffusion. Comprisons of grain size, densification mechanism and fracture toughness resulted from hot pressing after/without cold cyclic compaction showed that a low cyclic pressure may not effect on the fragmentation of alumina powders.

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HIGH STRENGTH ALUMINIUM ALLOYS PROCESSED BY SPRAY/CODEPOSITION

  • Juarez-Islas, Julio Alberto
    • Proceedings of the Materials Research Society of Korea Conference
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    • 1992.05a
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    • pp.14-14
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    • 1992
  • During the past five years a very successful effort has been made to improve existing and develop new aluminium alloys. The progress achieved has been possible because of the development of new production methods, such as powder metallurgy and spray/deposition. These methods make use of rapid solidification process which alloys compositions other than those achieved by conventional ingot metallurgy. The ingot metallurgy of the 2000 and 7000 series used thus far, as well as the age hardening Al-Li alloys, show several disadvantages caused by the production process. Such problems are primarily coarse intermetallic constituent phases, coarse grains and macrosegregation, resulting in low fracture toughness. The present contribution reports results of an experimental investigation performed on a modern high strength spay deposited aluminium alloy of the Al-Zn-Mg-Cu (7075 and the modified 7150X) type. Results are given in terms of its microstructural characterization by using X-ray diffractomertry and transmission electron microscopic. The mechanical propierties of those alloys in the as-extruded and extruded+aged condition were evaluated by using microhardness Vickers, tensile test and fracture toughness measurements.

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Sintering Characterization of Hot-Pressed SiC Prepared by SHS Microwave Method (SHS Microwave 법으로 합성한 SiC 분말의 고온가압 소결특성)

  • 김도경;안주삼;김익진;이형복
    • Journal of the Korean Ceramic Society
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    • v.32 no.8
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    • pp.865-872
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    • 1995
  • Ultra-fine $\beta$-SiC powders were fabricated by self-propagating high temperature synthesis process (SHS) using microwave oven. The flexural strength, fracture toughness, and hardness of hot pressed sample at 200$0^{\circ}C$ for 60 min using synthesized SiC powders, which had 2 wt% of Al2O3 and 2.5 wt% of B4C content, showed 438 MPa, 4.15MPa.m1/2 and 28 GPa, respectively. The highest strength, fracture toughness, and hardness of composites containing 4wt% of Al2O3, which had highest relative density of 99.9%, showed 458 MPa, 4.6MPa.m1/2 and 36.2 GPa, respectively.

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Microstructure characterization of glass fiber-doped cordierite (그라스 화이버 첨가 코디에라이트의 미세구조특성)

  • Choi, H.S.;Kim, M.K.;Choi, S.H.;Han, T.H.;Park, S.J.;Hwang, J.S.;Han, B.S.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1992.11a
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    • pp.97-101
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    • 1992
  • Cordierite glass ceramic has become an electronic substrate material for electronic circuits and the use of whiskers for improving strength and toughness is evident. Green sheets of mixtures containing 15% silicon nitride were sintered to greater than 99 % density. The microstructure was analysed using optical microscopy, scanning electron microscopy (SEM), and X-ray diffraction (XRD). The toughness and hardness were improved with increasing the whisker vol. % and sintering temperature. Especially, it is assumed that toughening increasing at the more high sintering temperature relevants to the glass phase increasing, as showned in the roughness of the fracture surfaces. It was directionally dependent of whisker direction during processing.

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A Study on the Low Temperature Fracture Toughness of Ion-nitrided Ni-Cr-Mo Steel (이온 실화처리한 Ni-Cr-Mo강의 저온파괴인성에 관한 연구)

  • 오세욱;윤한기;문인철
    • Journal of Ocean Engineering and Technology
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    • v.1 no.2
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    • pp.101-112
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    • 1987
  • Fracture toughness characterization in the transition region is examined for heat-treated and ionnitrided Ni-Cr-Mo steel. After heat treatment for the specimens of Ni-Cr-Mo steel, organizations of specimens-specimens which are heat-treated and ion-nitrided for 4 hours at 500 .deg. C and 5 torr in 25%N/dub 2/-75%H/sub 2/mixed gas-, hardness variety, and X-ray diffraction pattern of the ion-nitriding compound layer are observed. Fracture toughenss test of unloading compliance method were conducted over the regions from room trmperature to -70.deg. C. The compound layer was consisted of r'=Fe/sub 4/N phase and ion-nitrided layer's depth was 200mm from surface. The transition regions of heat-treated and ion-nitrided specimens were about -30.deg. C and -50.deg. C, respectively. The transition region of ion-nitrided specimens is estimated less than that of heat-treated one, and this is the effect of ion-nitriding.

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Effects of Composition and Additives on the Mechanical Characteristics of 3Y-TZP (3Y-TZP의 기계적 특성에 미치는 산화물 조성 및 첨가제의 영향)

  • Park, Mi-Jung;Yang, Seong-Koo;Kang, Jong-Bong
    • Journal of the Korean Ceramic Society
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    • v.43 no.10 s.293
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    • pp.640-645
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    • 2006
  • Monoclinic zirconia and yttria were mixed with a stoichiometric composition of 3Y-TZP (3 mol% Yttria-stabilized Tetragonal Zirconia Polycrystal). The specimen was sintered at 1350$\sim$1450$^{\circ}C$ and mechanical characterization and microstructure analysis were conducted. Microhardness and fracture toughness were shown as 1357.4 Hv and 8.56 MPa $m^{1/2}$. respectively. Without alumina, they were 1311 Hv and 10.02 MPa $m^{1/2}$ respectively. By mixing two different oxides, it was possible to obtain high values of microhardness and fracture toughness. It was possible that was turned out nano-scale particle using the co-milling of high mechanical energy.

The Effects of Physical Aging of PSF/AS4 Laminate on Fatigue (PSF/AS4 복합재료의 가속노화가 피로강도에 미치는 영향)

  • Kim, Hyung-Won
    • Composites Research
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    • v.19 no.4
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    • pp.1-6
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    • 2006
  • The effects of aging on fatigue of PSF/AS4 laminates tvas studied using the new energy release rate analysis. The analysis by the variational mechanics has been useful in providing fracture mechanics interpretation of matrix microcracking in cross-ply laminates. This paper describes the changes of the critical energy release rate ${\Delta}Gmc$(microcracking toughness) about the variation of the aging period during fatigue loading. The master plot by modified Pans-law gives a characterization of a material system's resistance to microcrack formation. PSF/AS4 $[0/902]_s$ laminates were aged at four different temperatures based on the glass transition temperature for 60 days. At all temperatures, the toughness decreased with aging time. The decrease of the toughness at higher temperature was faster than at lower temperature. To assess the effects of aging on fatigue, the unaged laminates were compared with the laminates which were aged for 60 days at $170^{\circ}C$ near $180^{\circ}C\;T_g$. The slope of dD/dN versus A 6u, of the aged laminates was lower than that of the unaged laminates. There was a significant shift of the aged data to formation of microcracks at the lower values of ${\Delta}G_m$.

Fabrication and Characterization of Alumina Matrix Composites Reinforced with SiC whiskers

  • Han, Byung-Dong;Park, Dong-Soo
    • The Korean Journal of Ceramics
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    • v.5 no.1
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    • pp.12-18
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    • 1999
  • Alumina matrix composites reinforced with up to 20vol% of aligned SiC whiskers were fabricated by tape casting and hot pressing. Alumina composited with randomly distribution SiC whiskers were also fabricated in order to investigate the effect of whisker alignment on properties of the composites. XRD and optical microscopy were used to examine the whisker orientation. The fracture toughness increased with increasing whisker content, and it was higher in the direction normal to the tape casting direction.

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