• 분석과학
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• 제10권5호
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• pp.1087-1104
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• 1997

• 한국진공학회:학술대회논문집
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• 한국진공학회 1996년도 제10회 학술발표회 논문개요집
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• pp.168-168
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• 1996

• Bulletin of the Korean Chemical Society
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• 제20권7호
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• pp.853-856
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• 1999

• 한국운동역학회지
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• 제27권3호
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• pp.171-179
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• 2017

Objective: The purpose of this study was to perform a kinematic and kinetic analysis of double-under jump rope technique according to skill level and sex. Method: Participants comprised a skilled group of 16 (9 males, 7 females), and an unskilled group of 16 with 6 months or less of experience (9 males, 7 females). Five consecutive double-under successes were regarded as 1 trial, and all participants were asked to complete 3 successful trials. The data for these 3 trials were averaged and analyzed after collecting the stable third jump in each trial. The variables used in the analysis included phase duration, total duration, flight time, vertical toe height, stance width, vertical center of mass displacement, and right lower limb ankle, knee, and hip joint angles in the sagittal plane during all events. Results: The skilled group had a shorter phase and total duration and a shorter flight time than the unskilled group. The vertical center of mass displacement and ankle dorsiflexion angle were significantly smaller in the skilled group. The male group had a shorter phase duration than the female group. The vertical toe height was greater, the stance width was smaller, and the ankle and hip flexion angles were smaller in the male group. Conclusion: Variables that can be used to distinguish between skill levels are phase and total duration, flight time, vertical center of mass displacement, and ankle dorsiflexion angle. Differences between sexes in double-under jump rope technique may be related to lower limb flexion angle control.

• 분석과학
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• 제28권2호
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• pp.132-138
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• 2015

Rosiglitazone metabolites in rat plasma were analyzed after intraperitoneal and oral administration to rats. Seven metabolites (M1-M7) were detected in rat plasma (IP and PO), and the structures were confirmed using liquid chromatography-triple time of flight (TOF) mass spectrometry; as a result, the most abundant metabolite was M5, a de-methylated rosiglitazone. Other minor in vivo metabolites were driven from monooxygenation and demethylation (M2), thiazolidinedione ring-opening (M1, M3), mono-oxygenation (M4, M7), and mono-oxygenation followed by sulfation (M6). Among them, M1 was found to be a 3-{p-[2-(N-methyl-N-2-pyridylamino)ethoxy]phenyl}-2-(methylsulfinyl)propionamide, which is a novel metabolite of rosiglitazone. There was no significant difference in the metabolic profiles resulting from the two administrations. The findings of this study provide the first comparison of circulating metabolite profiles of rosiglitazone in rat after IP and PO administration and a novel metabolite of rosiglitazone in rat plasma.

• 한국추진공학회:학술대회논문집
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• 한국추진공학회 2008년도 제31회 추계학술대회논문집
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• pp.203-206
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• 2008

KSLV-I 2단 추진기관에 적용될 킥모터는 고고도용 고체 추진기관으로 인공위성을 궤도에 진입시킬 때 반드시 필요한 하드웨어이다. 킥모터는 연소 시 내부에 내열재가 삭마되고 추진제가 소진되며 반면에 슬래그 적층으로 인해 무게가 변하게 된다. 본 문서는 지상연소시험 시 케이스, 추진제, 노즐, 점화기, 슬래그 등으로 구성된 킥모터의 무게 변화량을 분석하여 실제 비행시간에 따른 무게 변화량을 예측하였다. 킥모터의 비행 시 무게 변화 예측은 KSLV-I 2단의 무게 및 무게중심 변화를 계산하는데 활용될 수 있다.

• Bulletin of the Korean Chemical Society
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• 제19권8호
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• pp.830-835
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• 1998

The characteristics of the ablation plume generated by 532 nm Nd: YAG laser irradiation of a Pb(Zr0.52Ti0.48)O3 (PZT) target have been investigated using a pulsed-field time-of-flight mass spectrometer (TOFMS). The relative abundance of O+, Ti+, Zr+, Pb+, TiO+, and ZrO+ ions has been measured and discussed. TiO+ and ZrO+ ions were also found to be particularly stable within the laser ablation plasma with respect to PbO+ species. The behavior of the temporal distributions of each ionic species was studied as a function of the delay time between the laser shot and the ion extraction pulse. The most probable velocity of each ablated ion is estimated to be Vmp=1.1-1.6x 105 cm/s at a laser fluence of 1.2 J/cm2, which is typically employed for the thin film deposition of PZT. The TOF distribution of Ti+ and Zr+ ions shows a trimodal distribution with one fast and two slow velocity components. The fast velocity component (6.8x 10' cm/s) appears to consist of directly ablated species via nonthermal process. The second component, originated from the thermal evaporation process, has a characteristic velocity of 1.4-1.6 x 105 cm/s. The slowest component (1.2 x 105 cm/s) is composed of a dissociation product formed from the corresponding oxide ion.

• Bulletin of the Korean Chemical Society
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• 제34권1호
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• pp.275-278
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• 2013

• 한국결정성장학회지
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• 제7권3호
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• pp.465-472
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• 1997

본 연구는 전기 장에서 광여기 탈착과 이온화에 근거한 표면연구의 새로운 장치를 개발하고 시험한 결과를 보고한다. 실험장치의 분해능을 테스트 하기 위해 텡스텐(110)면에서 흡착기체 $H_2$ 와 He 가스를 조사하였으며, 팁의 온도는 80 K이었다. 장세기가 10 V/nm에서 50 V/nm사이에서 사용한 파장은 193 nm이였으며, 텡스텐(110)면에 가스가 흡착되었을때 레이저빔의 전자적인 여기로 부터 흡착가스와 팁에서 여러종류의 이온들이 형성되었다($H_2^+, CO^+, H_2O^+, He^+, W^{3+}$ 그리고 $W^{2+}$). 전체 mass spectrum의 기록은 Transient recorder가 가능하게 한다.

• Mass Spectrometry Letters
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• 제2권2호
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• pp.53-56
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• 2011

[ $C_8$ ]functionalized magnetic nanoparticles were synthesized by coating magnetic $Fe_3O_4$ nanoparticles with silicaamine groups using 3-aminopropyltriethoxysilane and by subsequently modifying the amine groups with chloro(dimethyl)octylsilane to produce octyl groups on the surface of the MNPs. The $C_8$-functionalized MNPs were used to enrich peptides from tryptic protein digests of myoglobin and ${\alpha}$-casein. The enriched peptides were analyzed by matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF-MS). MALDI-MS was also used to investigate desalting of the $C_8$-functionalized MNPs. Sample solutions were prepared in 1.0 M NaCl, and the successful removal of salt was observed. Enrichment with $C_8$-functionalized MNPs was very effective for separating and concentrating tryptic peptides.