• 제목/요약/키워드: time of extraction

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추출방법에 따른 인삼의 Polyacetylene 성분 회수율 비교 연구 (Studies on the Extraction Efficiency of Polyacetylene from Korean Ginseng)

  • 박찬엘;박창호
    • KSBB Journal
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    • 제16권3호
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    • pp.264-268
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    • 2001
  • The extraction efficiencies of panaxynol and panaxydol were optimal at 80$^{\circ}C$ with soxhlet method. The extraction efficiencies increased up to 45$^{\circ}C$ with shaking method. Amounts of panaxynol and panaxydol were determined by gas chromatography. Extracted quantities of panaxynol and panaxydol using the shaking method increased over a period of 14 hours. The efficiencies of panaxynol and panaxydol extraction by soxhlet and shaking methods were higher for smaller particle sizes. Upon water swelling treatment, extraction efficiencies of panaxynol and panaxydol decreased gradually with time for both methods.

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Optimization of Oil from Moringa oleifera seed using Soxhlet Extraction method

  • Ojewumi, M.E.;Oyekunle, D.T.;Emetere, M.E.;Olanipekun, O.O.
    • 식품보건융합연구
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    • 제5권5호
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    • pp.11-25
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    • 2019
  • Extraction of oil from Moringa oleifera seed using Response Surface Methodology (RSM) was investigated. Effects of three factors namely: sample mass, particle size and extraction time on the response, Moringa oleifera a volume extracted, were determined. The Box-Behnken design of RSM was employed which resulted in 15 experimental runs. Extraction was carried out in a 250 ml Soxhlet extractor with Hexane and Ethanol as solvent. The Moringa oleifera seed powder was packed inside a muslin cloth placed in a thimble of the Soxhlet extractor. The extraction was carried out at 60℃ using thermostatic heating mantle. The solvent in the extracted oil was evaporated and the resulting oil further dried to constant weight in the oven. This study demonstrates that Moringa oleifera oil can be extracted from its seed using ethanol and acetone as extraction solvent. The optimum process variables for both solvent (ethanol and acetone) was determined at sample weight of 40 g, particle size of 325 ㎛ and extraction time of 8 hours. It can be deduced that using acetone as solvent produces a higher yield of oil at the same optimum variable conditions compared to when ethanol was used.

열수추출 및 효소처리에 따른 감귤 과피 추출물의 기능성성분 수득에 대한 연구 (A Study on the Yield of Functional Components of Citrus Peel Extracts using Optimized Hot Water Extraction and Enzymatic Hydrolysis)

  • 노정은;윤성란;임애경;김혜정;허담;김대익
    • 한국식품조리과학회지
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    • 제28권1호
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    • pp.51-55
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    • 2012
  • This study was conducted to investigate the physicochemical properties of citrus peel extracts with different hot water extraction and enzymatic hydrolysis conditions. Enzymatic hydrolysis was also employed using Viscozyme L and results were compared with that of optimized hot water extract. Hot water extraction was performed under different parameters; the sample to solvent ratio(1:20, 1:15, 1:10), extraction time(2, 4 hrs), extraction temperature(85, $95^{\circ}C$) and enzymatic hydrolysis(0, 1%) and the subsequent extracts were used for determining their physicochemical properties, such as total yield, total phenolics, total flavonoids, and electron donating ability (EDA). With the increase in the sample to solvent ratio and extraction time, total yield, total phenolics, total flavonoids and EDA increased. But extraction temperature did not significantly affect the hot water extract. As hot water extract was hydrolyzed by the enzyme, total yield and active ingredients increased rapidly. In the result of total yield, total phenolics, total flavonoids and EDA, the activity of enzyme-treated extract was higher than those of enzyme-untreated extract. Based upon the overall hot water extraction efficiency, it was found that 20 times volume or 120 min at a time at $95^{\circ}C$ after enzyme treatment was optimal.

추출방법에 따른 홍삼추출액의 사포닌 조성과 품질특성 (Ginsenoside Composition and Quality Characteristics of Red Ginseng Extracts prepared with Different Extracting Methods)

  • 이강선;남기열;최재을
    • 한국약용작물학회지
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    • 제21권4호
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    • pp.276-281
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    • 2013
  • This study was conducted to compare the contents of ginsenoside according the water extract conditions of red ginseng. In method A, red ginseng extract was prepared at $75^{\circ}C$ for 18 hours by 1 time extraction, and method B, the preparation was done at $85^{\circ}C$ for 18 hours by 1 time extraction. In method C, the primary extract prepared at $75^{\circ}C$ for 9 hours was blended with the secondary extract prepared by re-extracting the red ginseng residue obtained after the primary extraction, at $85^{\circ}C$ for 9 hours. Method D was the same procedure as method C but the extraction temperature for the primary extraction was $85^{\circ}C$ and that for the secondary extraction was $95^{\circ}C$. The contents of total and $Rb_1$, $Rg_1$ and $Rg_3$ ginsenoside were highest in Method C. The content of prosapogenin (ginsenoside $Rg_2$, $Rg_3$, $Rb_1$ and $Rb_2$) was highest in Method B. There was no consistent tendency in Brix, pH, Hue value and absorbance among extraction methods.

마이크로웨이브 추출공정에 의한 홍고추 올레오레진의 함량 및 기능적 특성 (Oleoresin Content and Physiological Activities of Fresh Red pepper by microwave-Assiated Extraction)

  • 권영주;정승원;김현구;권중호
    • 한국식품저장유통학회지
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    • 제7권1호
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    • pp.74-79
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    • 2000
  • Water and ethanol extracts of fresh red peppers were obtained by two methods, conventional extraction (CE) and microwave-assiated extraction (MAE), under different extraction conditions. Red pepper oleoresins extracted by CE and MAE were examined in oleoresin yield and physiological activities. The proper extraction time of MAE was about 5 minutes, whereas that of CE was 2 hours. therefore extraction time was decreased drastically by MAE but there was no significance in oleolesin yields. the electron donating abilities also showed negligible difference between two extracts obtained by CE and MAE, and 80% level in all extracts . the nitrite scavenging effect was reduced by increased of ph , and showed a high elimination effect over 85% at ph 1.2. All extracts had a high tyrosinase inhibitory effects of 100%. The angiotensin I-conventing enzyme effect showed higher activity with over 80% in MAE than 70% level in CE. the capsanthin was extracted with ethanol and was 11.4 and 12.9 ${\mu}$moles per 1 g of fresh red pepper by CE and MAE, respectively.

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Optimization of Extraction of Cycloalliin from Garlic (Allium sativum L.) by Using Principal Components Analysis

  • Lee, Hyun Jung;Suh, Hyung Joo;Han, Sung Hee;Hong, Jungil;Choi, Hyeon-Son
    • Preventive Nutrition and Food Science
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    • 제21권2호
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    • pp.138-146
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    • 2016
  • In this study, we report the optimal extraction conditions for obtaining organosulfur compounds, such as cycloalliin, from garlic by using principal component analysis (PCA). Extraction variables including temperature ($40{\sim}80^{\circ}C$), time (0.5~12 h), and pH (4~12) were investigated for the highest cycloalliin yields. The cycloalliin yield (5.5 mmol/mL) at pH 10 was enhanced by ~40% relative to those (~3.9 mmol/mL) at pH 4 and pH 6. The cycloalliin level at $80^{\circ}C$ showed the highest yield among the tested temperatures (5.05 mmol/mL). Prolonged extraction times also increased cycloalliin yield; the yield after 12 h was enhanced ~2-fold (4 mmol/mL) compared to the control. Isoalliin and cycloalliin levels were inversely correlated, whereas a direct correlation between polyphenol and cycloalliin levels was observed. In storage for 30 days, garlic stored at $60^{\circ}C$ (11 mmol/mL) showed higher levels of cycloalliin and polyphenols than those at $40^{\circ}C$, with the maximum cycloalliin level (13 mmol/mL) on day 15. Based on the PCA analysis, the isoalliin level depended on the extraction time, while cycloalliin amounts were influenced not only by extraction time, but also by pH and temperature. Taken together, extraction of garlic at $80^{\circ}C$, with an incubation time of 12 h, at pH 10 afforded the maximum yield of cycloalliin.

Direct identification of aeroelastic force coefficients using forced vibration method

  • Herry, Irpanni;Hiroshi, Katsuchi;Hitoshi, Yamada
    • Wind and Structures
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    • 제35권5호
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    • pp.323-336
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    • 2022
  • This study investigates the applicability of the direct identification of flutter derivatives in the time domain using Rational Function Approximation (RFA), where the extraction procedure requires either a combination of at least two wind speeds or one wind speed. In the frequency domain, flutter derivatives are identified at every wind speed. The ease of identifying flutter derivatives in the time domain creates a paradox because flutter derivative patterns sometimes change in higher-order polynomials. The first step involves a numerical study of RFA extractions for different deck shapes from existing bridges to verify the accurate wind speed combination for the extraction. The second step involves validating numerical simulation results through a wind tunnel experiment using the forced vibration method in one degree of freedom. The findings of the RFA extraction are compared to those obtained using the analytical solution. The numerical study and the wind tunnel experiment results are in good agreement. The results show that the evolution pattern of flutter derivatives determines the accuracy of the direct identification of RFA.

Optimization and Bioassay Guided Comparative Techniques for Efficient Extraction of Lutein Esters from Tagetes erecta (Var. Pusa Narangi Genda) Flowers

  • Kawar Lal Dabodhia;Brijesh Tripathi;Narendra Pal Lamba;Manmohan Singh Chauhan;Rohit Bhatia;Vivek Mishra
    • Mass Spectrometry Letters
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    • 제15권1호
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    • pp.40-48
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    • 2024
  • Capacity of the analytical/quantitative evaluation techniques to satisfy both qualitative and quantitative considerations for effective extraction of marigold oleoresins/xanthophylls and their potential as anti-mycotic and antioxidant activity was assessed. Accelerated solvent extraction (ASE), Soxhlet extraction (SE), Supercritical fluid extraction (SCFE), Cold extraction (CE), and ultrasonically assisted extraction (USE) techniques were evaluated for extraction of oleoresin/xanthophyll content from Tagetes erecta (Var. Pusa Narangi Genda) with respect to solvent consumption, extraction time, reproducibility, and yield. Followed by the antifungal and antioxidant activity evaluation. The overall yield of Tagetes oleoresin was higher in ASE (64.5 g/kg) followed by SE (57.3 g/kg), USE (50.7 g/kg), SCFE (45.3 g/kg) and CE (31.6 g/kg). The lutein esters represented more than 80% of the constituents. Further, xanthophyll/ lutein content in oleoresin was found to be quite higher in HPLC (r2 = 0.996) analysis than in the AOAC recommended UV spectrophotometer analysis. The oleoresin exhibited moderate antioxidant activity (DPPH assay) and antifungal activity against three phytopathogenic fungi. Based on the various parameters, the reproducibility of ASE was better (0.3-8.0%) than that of SE (0.5-12.9%), SCFE (0.2-9.4%), USE (0.3-12.4%) and CE (0.8-15.3%). ASE with (RSD 1.6%) is preferred being faster, reproducible, uses less solvent, robust and automation allows sequential extraction of the sample in less time.

Agaricus blazei 자실체로부터 마이크로웨이브를 이용한 생리활성물질 추출공정 (Microwave Assisted Extraction of Physiologically Active Materials from Agaricus blazei Fruiting Bodies)

  • 최정우;류동열;홍억기;권명상;한진수;이원홍
    • KSBB Journal
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    • 제15권3호
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    • pp.307-312
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    • 2000
  • 버섯에서 추출되는 생리활성물질얀 ${\beta}$-glucan은 탁월한 항암 효과를 갖는 물질이다. 특히 Agaricus blazei에 $\beta$-glucan이 많이 포함되어 있는 것으로 보고되어져 있다. 본 연구의 목적은 마이 크로웨이브를 사용하여 아가리쿠스버섯으로부터 ${\beta}$-glucan을 추 출하는 공정의 추출효율을 극대화하는 것으로, 다양한 추출시간 과 마이크로웨이브 출력을 이용하여 최적 운전조건을 결정하였 다. 최적 마이크로웨이브의 최적 출력은 200, 500, 650 watt의 경우에서 실험하여 결정하였다. 추출물질의 구조와 농도 분석은 nuclear magnetic resonance spectroscopy와 infrared spectroscopy 를 이용하여 수행하였다 본 실험 결과로 마이크로웨이브를 이 용한 추출의 다당류 수율이 전통적 인 열수추출방법보다 향상됨을 확인하였고, 소량의 용매와 짧은 추출 시간으로 향상된 수율을 얻을 수 있음을 알 수 있었다.

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Design and Implementation of Web Crawler with Real-Time Keyword Extraction based on the RAKE Algorithm

  • Zhang, Fei;Jang, Sunggyun;Joe, Inwhee
    • 한국정보처리학회:학술대회논문집
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    • 한국정보처리학회 2017년도 추계학술발표대회
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    • pp.395-398
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    • 2017
  • We propose a web crawler system with keyword extraction function in this paper. Researches on the keyword extraction in existing text mining are mostly based on databases which have already been grabbed by documents or corpora, but the purpose of this paper is to establish a real-time keyword extraction system which can extract the keywords of the corresponding text and store them into the database together while grasping the text of the web page. In this paper, we design and implement a crawler combining RAKE keyword extraction algorithm. It can extract keywords from the corresponding content while grasping the content of web page. As a result, the performance of the RAKE algorithm is improved by increasing the weight of the important features (such as the noun appearing in the title). The experimental results show that this method is superior to the existing method and it can extract keywords satisfactorily.