• 한국산업융합학회 논문집
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• 제26권4_2호
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• pp.629-637
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• 2023

This study aimed to evaluate the effect of post-curing equipment and time on the flexural strength of 3D printing resins produced by a liquid crystal display(LCD) printer. The three 3D printing resins(DENTCA Denture Teeth, DT; C&B 5.0 hybrid, CH; C&B Permanent A2, CP) were divided into four groups according to post-curing time(10 min and 30 min) and equipment with or without vacuum treatment. For the three-point flexural strength test and biaxial strength test were prepared by method according to ISO 10477, ISO 6872, respectively. Flexural strength was measured with universal testing machine. Comparison between post-curing time of each post-curing equipment was analyzed by independent sample t-test and Mann-Whitney U test(α=.05), and comparison between groups according to each 3D printing resin was performed by Kruskal-Wallis test and post-hoc by Bonferroni-Dunn test(α=.05). The flexural strength of the resin post-curing under vacuum was higher than that of the resin post-curing in air. In the comparison according to the post-curing time, in the case of the post-curing equipment without vacuum, the 30 minute curing time showed significantly higher flexural strength than the 10 minute curing time, except for the biaxial flexural strength of CH(P<.05). In the post-curing equipment with vacuum, the three-point flexural strength of all 3D printing resins(DT, CH, and CP) showed a higher value at 30 minute curing time than at 10 minute curing time.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2007년도 춘계학술대회A
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• pp.321-325
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• 2007

Recently, demands on thin multi-layer printed circuit boards(PCB) have been rapidly increased with broad spread of personal portable digital appliances such as multi-media. In case of mobile phone, however, the fact that PCBs have low flexural strength might cause defects. The purpose of this study is to improve the flexural strength by substituting the well-known GFRP(glass fiber reinforced plastic) for CFRP(carbon fiber reinforced plastic). Firstly, finite element simulation was carried out using ABAQUS to find out a unique CFRP layer that has a role to sustain the applied forces mainly in PCB. Secondly, three point bending tests were conducted with the newly designed CFRP PCB model to verify the improvement of the flexural strength. Consequently, it is shown that PCB layered with the CFRP on both outer sides of the board can be used to improve the flexural strength effectively.

• 대한치과기공학회지
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• 제43권2호
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• pp.35-41
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• 2021

Purpose: This study aimed to investigate the flexural strength and surface microstructure of the zirconia crown according to the number of glazing zirconia prostheses. Methods: The specimens were made as follows. A specimen without glazing: 1ea, first glazed specimens (group B): 10ea, second glazed specimens (group C): 10ea, third glazed specimens (group D): 10ea. Three-point measuring strength equipment and electron microscopes were used for strength measurement and microstructure observation. As for statistical analysis, one-way ANOVA and t-test (level of significance level=5%) were used to determine the difference in the change in flexural strength according to the number of glazing zirconia prostheses. Results: ANOVA analysis of groups B (1st glazing), C (2nd glazing), and D (3rd glazing) revealed that the change in strength between the groups is statistically significant (p=0.023). The Mann-Whitney test for each group revealed that the difference in flexural strength between groups B and C was not statistically significant (z=-0.302, p=0.762) while that between groups C and D was statistically significant (z=-0.257, p=0.01). Microstructure observation revealed 3 changes in the microstructure of the surface of the glaze powder were observed. Conclusion: According to the number of glazing zirconia prostheses, it was found that the difference in strength between groups was statistically significant, and changes in the microstructure were observed.

• 대한치과기공학회지
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• 제42권2호
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• pp.73-79
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• 2020

Purpose: The aim of this study was to investigate the influence of short and long duration sintering on microstructure and flexural strength of zirconia. Methods: To conduct three-point bending test, Zirconia specimens are milled according to ISO 6872 guidelines(N=18, n=9 per group). Two specimens group(n=8) is sintered for 10 hours(Standard schedule) and 3 hours(Speed schedule) at the peak temperature of 1550℃ with silicon carbide sintering furnace. Flexural strength of specimens are measured by instron. After coating each specimen(n=1), microstructure of specimens is observed using Scanning Electron Microscope(SEM). T-test was utilized to statistically assess the data. Results: The mean and standard deviation value of the flexural strength for standard schedule group are 578.15±57.48Mpa, that of speed schedule are 465.9±62.34Mpa. T-test showed significant differences in flexural strength between two zirconia specimen group which applied standard schedule and speed schedule respectively(p<0.05). Conclusion: The result of this study showed that the increase in sintering time led to increased grain size, and also to a positive effect on the flexural strength.

• The Journal of Advanced Prosthodontics
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• 제3권3호
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• pp.136-139
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• 2011

PURPOSE. A new light curing urethane dimethacrylate and a cold curing resin with simpler and faster laboratory procedures may have even improved flexural properties. This study investigated the 3-point flexural strengths and flexural moduli of two alternate base materials. MATERIALS AND METHODS. A cold curing resin (Weropress) and a light curing urethane dimethacrylate base material (Eclipse). Along with Eclipse and Weropress, a high impact resin (Lucitone199) and three conventional base materials (QC 20, Meliodent and Paladent 20) were tested. A 3-point bending test was used to determine the flexural strengths and flexural moduli. The mean displacement, maximum load, flexural modulus and flexural strength values and standard deviations for each group were analyzed by means of one-way analysis of variance (ANOVA) (with mean difference significant at the 0.05 level). Post hoc analyses (Scheffe test) were carried out to determine the differences between the groups at a confidence level of 95%. RESULTS. Flexural strength, displacement and force maximum load values of Eclipse were significantly different from other base materials. Displacement values of QC 20 were significantly different from Lucitone 199 and Weropress. CONCLUSION. The flexural properties and simpler processing technique of Eclipse system presents an advantageous alternative to conventional base resins and Weropress offers another simple laboratory technique.

• The Journal of Advanced Prosthodontics
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• 제16권1호
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• pp.25-37
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• 2024

PURPOSE. To investigate the effect of sintering programs and surface treatments on surface properties, phase transformation and flexural strength of monolithic zirconia. MATERIALS AND METHODS. Zirconia specimens were sintered using three distinct sintering programs [classic (C), speed (S), and superspeed (SS)] (n = 56, each). One sample from each group underwent scanning electron microscopy (SEM) and grain size analysis following sintering. Remaining samples were divided into five subgroups (n = 11) based on the surface treatments: control (CL), polish (P), glaze (G), grind + polish (GP), and grind + glaze (GG). One sample from each subgroup underwent SEM analysis. Remaining samples were thermally aged. Monoclinic phase volume, surface roughness, and three-point flexural strength were measured. Monoclinic phase volume and surface roughness were analyzed by Kruskal-Wallis and Dunn tests. Flexural strength was analyzed by two-way ANOVA and Weibull analysis. The relationships among the groups were analyzed using Spearman's correlation analysis. RESULTS. Sintering program, surface treatment, and sintering × surface treatment (P ≤ .010) affected the monoclinic phase volume, whereas the type of surface treatment and sintering × surface treatment affected the surface roughness (P < .001). Type of sintering program or surface treatment did not affect the flexural strength. Weibull analysis revealed no significant differences between the m and σ_o values. Monoclinic phase volume was positively correlated with surface roughness in the SGG and SSP groups. CONCLUSION. After sintering monolithic zirconia in each of the three sintering programs, each of the surface treatments can be used. However, for surface quality and aging resistance, G or GG can be recommended as a surface finishing method.

• 대한치과기공학회지
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• 제39권1호
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• pp.9-16
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• 2017

Purpose: The purpose of this study was to evaluate flexural strength, composite surface and fractured surface of three different indirect composite resins. Methods: Fifteen bar-shaped specimens ($25mm{\times}2mm{\times}2mm$) were fabricated for each FL group (Flow type and Light curing) and PLP group (Putty type and Light, Pressure curing) and PL group (Putty type and Light curing) according to manufacturer's instructions and ISO 10477. Fabricated specimens were stored in the distilled water for 24 hours at the temperature of $37^{\circ}C$. Three-point bending strength test was performed to measure flexural strength using universal testing machine at a crosshead speed of 1mm/min (ISO 10477). Surface and fractured surface of specimens were observed by digital microscope. Results were analyzed with Kruskal-wallis tests (${\alpha}=0.05$). Results: Mean (SD) of three different indirect composite resins were 83.38 (6.67) MPa for FL group, 139.90(16.53) MPa for PLP group and 171.72(16.74) MPa for PL group. Flexural strength were statistically significant (p<0.05). Differences were not observed at fractured surface among three groups. However, many pores over $100{\mu}m$ were observed at PL group in observing surface of specimen. Conclusion: Flexural strength of composite resins was affected by second polymerization method and content of inorganic filler.

• 대한치과기공학회지
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• 제33권4호
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• pp.283-289
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• 2011

Purpose: The purpose of this study was to evaluate flexural strength of full zirconia crown using block after clinical work. Methods: The three point bending test was used to measure the flexural strength of zirconia block. Statistical analysis was done using the Statistical Package for Social Sciences version 19.0 for Windows. As for the analysis methods, the study used analysis of variance, Tukey's test. Results: The ave Rage value of flexural strengths of WIELAND, Zirkonzahn, Hass, D-MAX were 516.2 MPa, 612.6MPa, 566.2MPa, 744.6MPa. The ave Rage value of Surface Roughness of WIELAND, Zirkonzahn, Hass, D-MAX were 0.39Ra, 0.33Ra, 0.33Ra, 0.47Ra. Conclusion: Flexural strength of zirconia block decreased after clinical work. Flexural strength of zirconia block is equal to or higher than flexural strength of dental metal, so zirconia block can be used as dental material.

• The Journal of Advanced Prosthodontics
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• 제11권4호
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• pp.202-208
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• 2019

PURPOSE. Fabrication of zirconia restorations with ideal mechanical properties in a short period is a great challenge for clinicians. The purpose of the study was to investigate the effect of heating rate on the mechanical and microstructural properties of monolithic zirconia. MATERIALS AND METHODS. Forty monolithic zirconia specimens were prepared from presintered monolithic zirconia blanks. All specimens were then assigned to 4 groups according to heating rate as Control, Group $15^{\circ}C$, Group $20^{\circ}C$, and Group $40^{\circ}C$. All groups were sintered according to heating rates with the sintering temperature of $1500^{\circ}C$, a holding time of 90 minutes and natural cooling. The phase composition was examined by XRD analysis, three-point bending test was conducted to examine the flexural strength, and Weibull analysis was conducted to determine weibull modulus and characteristic strength. Average grain sizes were determined by SEM analysis. One-way ANOVA test was performed at a significance level of 0.05. RESULTS. Only tetragonal phase characteristic peaks were determined on the surface of analyzed specimens. Differences among the average grain sizes of the groups were not statistically significant. The results of the three-point bending test revealed no significant differences among the flexural strength of the groups (P>.05). Weibull modulus of groups was ranging from 3.50 to 4.74. The highest and the lowest characteristic strength values were obtained in Group $20^{\circ}C$ and Control Group, respectively. CONCLUSION. Heating rate has no significant effect on the flexural strength of monolithic zirconia. Monolithic zirconia restorations can be produced in shorter sintering periods without affecting the flexural strength by modifying the heating rate.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 1990년도 가을 학술발표회 논문집
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• pp.169-174
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• 1990

Fracture tests were carried out in order to investigate the flexural behavior of SFRC (Steel Fiber Reinforced Concrete) structures. Sixty three SFRC beams were used in the tests, the fracture mode, the relationships between loading and strains, and the relationships between loading and mid-span deflections of the beams were observed under the three point bending loading. From the test results, the effects of steel fiber contents and a/h ratio on the concrete flexural behavior were studied, and the stress intensity factors and the flexural strength of SFRC beams were calculated. According to the results of regression analysis, predicting formulas for the flexural strength of SFRC beams are also suggested.