• Proceedings of the KWS Conference
• /
• 2009.11a
• /
• pp.37-37
• /
• 2009

Due to their high corrosion resistance and improved mechanical properties super-duplex stainless steel (SDSS) are extensively used in petrochemical plants such as facilities in modern oil platform and off-shore process equipment. It is well known that the best mechanical and corrosion resistance properties of super-duplex stainless steel are obtained with a microstructure having approximately equal amounts of austenite and ferrite. And it is also known that sigma($\sigma$), chi($\chi$), secondary austenite(${\gamma}2$), chromium carbides and nitride affected adversely their properties. Therefore these phases must be avoided. However, effects of succeeding weld thermal cycle on the change of microstructure of weldment at multi-pass weld were not seldom experimentally researched. Therefore in the present work, the change of weldmetal microstructure and the effect of microstructure on pitting corrosion property at $40^{\circ}C$ by succeeding each weld thermal cycle were researched. The thermal history of root side was measured experimentally and the change of microstructure of root weld according to thermal cycle of each weld layer was evaluated. And the relationship between microstructure of root weld and pitting corrosion property at $40^{\circ}C$ was also investigated. Results of the present work are show as below. 1. The ferrite contents of root weld are gradually reduced by succeeding weld thermal cycle. 2. The 2nd phases such as sigma($\sigma$), chi($\chi$), secondary austenite(${\gamma}2$), chromium carbides and nitride are increased gradually by succeeding weld thermal cycle. 3. The pitting corrosion was detected in root weld part and weight loss by pitting corrosion is increased in proportional to the time exposed over $600^{\circ}C$ of the root weld. 4. The succeeding weld thermal cycles affect the microstructure of the former weldments and promote the formation of 2nd phases. That is, the more succeeding welds are added, the more 2nd phases are gradually increased. Consequently, it is thougth that this adversely affects pitting corrosion property.

• Applied Chemistry for Engineering
• /
• v.24 no.2
• /
• pp.144-147
• /
• 2013

Sweating, which is the excretion of oil on the surface of a solid product containing several kinds of pigments in oil and is also solidified with wax, is a unique phenomenon often observed on the surface of cover make-up or lipstick. The cause of sweating is an imbalanced formula. Many studies have been conducted to decrease the symptoms of sweating in the field of cosmetics. Differential scanning calorimetry (DSC) is a thermo-analytical technique that measures the amount of heat required to increase the temperature of a sample as a function of temperature or time under certain conditions. DSC has been used to determine the thermal properties of oil/wax structures. This study investigates how the thermal characteristics correlate with the sweating symptoms. An oil/wax formulation with an optimal melting point was studied in an attempt to make a stable product by considering the thermal properties that represent minimal structural changes with temperature variation. In addition, the sweating of the oil/wax formulation was observed over a various temperature range. As a result, it was found that sweating was minimized when the structure remained static or little bit changed over a variety of temperatures.

• Journal of Sensor Science and Technology
• /
• v.32 no.1
• /
• pp.39-43
• /
• 2023

Microscale thermophysical property measurements of liquids have been developed considering the increasing interest in the thermal management of cooling systems and energy storage/transportation systems. To accurately predict the heat transfer performance, information on the thermal conductivity, heat capacity, and density is required. However, a simultaneous analysis of the thermophysical properties of small-volume liquids has rarely been considered. Recently, we proposed a new methodology to simultaneously analyze the aforementioned three intrinsic properties using heater-integrated fluidic resonators (HFRs) in an atmospheric pressure environment comprising a microchannel, resistive heater/thermometer, and mechanical resonator. Typically, the thermal conductivity and volumetric heat capacity are measured based on a temperature response resulting from heating using a resistive thermometer, and the specific heat capacity can be obtained from the volumetric heat capacity by using a resonance densitometer. In this study, we analyze methods to improve the thermophysical property measurement performance using HFRs, focusing on the effect of the ambience around the sensor. The analytical method is validated using a numerical analysis, whose results agree well with preliminary experimental results. In a vacuum environment, the thermal conductivity measurement performance is enhanced, except for the thermal conductivity range of most gases, and the sensitivity of the specific heat capacity measurement is enhanced owing to an increase in the time constant.

• Journal of the Korean Applied Science and Technology
• /
• v.29 no.1
• /
• pp.141-148
• /
• 2012

In this study, the composite coating materials with improved thermal insulation property were prepared by incorporating the hydrophobic silica aerogel. The surface modification of silica aerogel was performed to obtain UV curable urethane acrylate hybrid coating sols with good compatibility by using surfactant(Brij 56). The polycarbonate substrates were coated by the prepared composites and cured under UV radiation. The incorporation of aerogel with only 10 vol% of content resulted in remarkable improvement by about 28% in the thermal insulation property of the coated film, as compared with substrate. In addition, increasing aerogel content was found to give minor effect on the variation of optical transparency, adhesion, and surface hardness of the coated film.

• Journal of Navigation and Port Research
• /
• v.39 no.6
• /
• pp.485-491
• /
• 2015

The technology review about risk of hypothermia of victim according to heat transfer characteristic of life raft and sea state can use accident correspondence of standing and sinking of ship. This study studied heat transfer characteristics required for the design of life raft and thermal insulation property analysis and evaluation methods. In addition, it is study for comprehend the risk of hypothermia and suggest analysis result that is experiment of thermal insulation property and body temperature property for decide of prediction the body temperature decline Thermal Analysis apply the finite element analysis method is comprehended the property of heat conductivity, convective effect of sea water and properties changes according to property of insulation material. it measure the heat flux with attach temperature sensor on body in order to comprehend the variation of body temperature with boarding a life raft experiment on a human body. This study validate results by comparing variation of temperature measured from experiment on a body with variation of temperature from finite element analysis model. Also, the criteria of hypothermia was discussed through result of finite element analysis.

• Proceedings of the KIEE Conference
• /
• 2001.07c
• /
• pp.1487-1489
• /
• 2001

The tantalum oxide($Ta_2O_5$) is an important material for present thin-film capacitor application owing to its high dielectric constant and thermal stability. We report dielectric property of Si(p type)/Pt/$Ta_2O_5$/Ag based MIM structure obtained by RF sputtering and annealed in vacuum environment. We have measured and researched the characteristics of C-F, C-V and EPMA. And we describe parameter dependence on sputtered condition and annealed temperature with dielectric property.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
• /
• 1999.10a
• /
• pp.185-189
• /
• 1999

There has been a considerable attention in Invar alloys because of its low thermal expansion property. A low thermal expansion property of Invar alloys, lower than 10-6 near the room temperature, is attractive for precision machine tools. However, the expansion property of Invar alloys is limited below about 520。K, and mechanical properties are relatively low to apply to machine tools. In order to improve mechanical properties in this alloy, Ti alloy element was added to an invar alloy. Microstructure changes and optimum heat-treatment conditions according to Ti addition were discussed in the Ni38-Mo2-Crl-Fe Invar alloy.

• Korean Journal of Materials Research
• /
• v.25 no.12
• /
• pp.678-682
• /
• 2015

The electrical property of polymer matrix composites with added carbon powder is studied based on the temperature dependency of the conduction mechanism. The temperature coefficient of the resistance of the polymer matrix composites below the percolation threshold (x) changed from negative to positive at 0.20 < x < 0.21; this trend decreased with increasing of the percolation threshold. The temperature dependence of the electrical property(resistivity) of the polymer matrix composites below the percolation threshold can be explained by using a tunneling conduction model that incorporates the effect of the thermal expansion of the polymer matrix composites into the tunneling gap. The temperature coefficient of the resistance of the polymer matrix composites above the percolation threshold has a positive value; its absolute value increased with increasing volume fraction of carbon powder. By assuming that the electrical conduction through the percolating paths is a thermally activated process and by incorporating the effect of thermal expansion into the volume fraction of the carbon power, the temperature dependency of the resistivity above the percolation threshold can be well explained without violating the universal law of conductivity.

• Nuclear Engineering and Technology
• /
• v.33 no.2
• /
• pp.184-191
• /
• 2001

The effects of ${\gamma}$-irradiation on the crosslinking of high density polyethylene (HDPE) was investigated for the purpose of obtaining a suitable formulation for heat shrinkable materials. In this study the HDPE specimens were prepared by blending with cross linking agents and pressed into a 0.2 mm sheet at 18$0^{\circ}C$. ${\gamma}$-irradiation was conducted at 40 to 100 kGy in nitrogen. The heat shrinkable property and thermal mechanical property of the HDPE sheets have been investigated. It was found that the degree of crosslinking of the irradiated HDPE samples were increased with irradiation dose. Compared with the HDPE containing triallylisocyanurate, the HDPE containing trimethylol propane triacrylate shows a slight increase in crosslinking density. The heat transformation and dimension change of HDPE decreased with increasing radiation dose. The heat shrinkage of the samples increased with increasing annealing temperatures. The thermal resistance of HDPE increased upon the crosslinking of HDPE.

• Journal of Powder Materials
• /
• v.26 no.6
• /
• pp.515-527
• /
• 2019

High-entropy alloys (HEAs) are generally defined as solid solutions containing at least 5 constituent elements with concentrations between 5 and 35 atomic percent without the formation of intermetallic compounds. Currently, HEAs receive great attention as promising candidate materials for extreme environments due to their potentially desirable properties that result from their unique structural properties. In this review paper, we aim to introduce HEAs and explain their properties and related research by classifying them into three main categories, namely, mechanical properties, thermal properties, and electrochemical properties. Due to the high demand for structural materials in extreme environments, the mechanical properties of HEAs including strength, hardness, ductility, fatigue, and wear resistance are mainly described. Thermal and electrochemical properties, essential for the application of these alloys as structural materials, are also described.