• Title/Summary/Keyword: the thermal treatment time

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A Study on the Treatment of Paper Mill Wastewater with the Addition of High Thermal Microbial Inoculants (고온성 종균제를 이용한 제지폐수 처리)

  • 이성호;임택준;조준형
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.34 no.2
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    • pp.54-60
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    • 2002
  • The Wastewater of toilet paper mill recycling recovered milk carton was used as a raw material for this study. According to the actual mill conditions, hydraulic retention time was adjusted to 12 hours and F/M (Food/Micro-organism) ratio was adjusted to 0.23. Temperature of aeration basin was varied from 2$0^{\circ}C$ to 5$0^{\circ}C$. The change of Micro-organisms and removal efficiency of pollutant were investigated at the varied temperature of basin. Aeration basin using high thermal microbial inoculants showed more removal efficiency of SS, COD than aeration basin using conventional microbial inoculants at high temperature. Floc consolidation of aeration basin using high thermal microbial inoculants added sludge was better than that of sludge from aeration basin using conventional microbial inoculants.

Rapid Thermal Annealing of GaN EpiLayer grown by Molecular Beam Epitaxy (MBE로 성장한 GaN 에피층의 급속 열처리)

  • Choi, Sung-Jai;Lee, Won-Sik
    • The Journal of the Institute of Internet, Broadcasting and Communication
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    • v.10 no.1
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    • pp.7-13
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    • 2010
  • We have investigated effects of the rapid thermal annealing of GaN epilayers by molecular beam epitaxy in nitrogen atmosphere. The improvement of structural properties of the samples was observed after rapid thermal annealing under optimum conditions. This improvement in crystal quality is due to a reduction of the spread in the lattice parameter in epilayers. The annealing has been performed in a rapid thermal annealing furnace at $950^{\circ}C$. The effect of rapid thermal annealing on the structural properties of GaN was studied by x-ray diffraction. The Bragg peak shifts toward larger angle as the annealing time increases. As the thermal treatment time increases, FWHM(full width at half maximum) of the peak slightly increase with its decreases followed and it increases again. Results demonstrate that rapid thermal annealing did not always promote qualities of GaN epilayers. However, rapid thermal annealing under optimum conditions improve structural properties of the samples, elevating their crystal quality with a reduction of inaccuracy in the lattice parameter of the epilayers.

Effect of Sealing Treatment on Solid Particle Impingement Erosion of Al-Zn-Zr Thermal Spray Coating Layer (Al-Zn-Zr 용사코팅층의 고체입자 충돌 침식특성에 미치는 봉공처리의 영향)

  • Heo, Ho-Seong;Kim, Seong-Jong
    • Corrosion Science and Technology
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    • v.21 no.1
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    • pp.68-76
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    • 2022
  • Several technologies are employed to protect substrates from corrosion and erosion damage. In particular, arc thermal spray coating technology is widely used as anti-corrosive technology for steel and concrete structures and is applied to offshore plants and petrochemical and drilling facilities. In this investigation, solid particle impingement erosion experiments were performed on an arc thermal spraying-coated specimen using 85% Al-14% Zn-1% Zr wire rod in KR-RA steel. This study investigated the effect of fluorosilicone sealing on the erosion resistance characteristics of the thermal spray coating layer. The erosion rates of the thermal spray-coated and sealed specimens were 4.1×10-4 and 8.5×10-4, respectively. At the beginning of the experiment, the fluorosilicone sealant was almost destroyed by the impact of the solid particles. The destruction time for the coating layer was 10 minutes for the thermal spray-coated specimen and 13 minutes for the sealed specimens, indicating that the sealed specimens had better erosion resistance characteristics to solid particle impingement.

Characteristics of Sucrose Thermal Degradation with High Temperature and High Pressure Treatment

  • Woo, Koan-Sik;Hwang, In-Guk;Lee, Youn-Ri;Lee, Jun-Soo;Jeong, Heon-Sang
    • Food Science and Biotechnology
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    • v.18 no.3
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    • pp.717-723
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    • 2009
  • Thermal degradation characteristics of sucrose was investigated. A 20% sucrose solution was heated to temperatures of $110-150^{\circ}C$ for 1-5 hr. Chromaticity, pH, organic acids, 5-hydroxymethylfurfural (HMF), free sugars, electron donating ability (EDA), and ascorbic acid equivalent antioxidant capacity (AEAC) of the heated sucrose solutions were evaluated. With increasing temperatures and times, the L-, a-, and b-values decreased; however, total color difference (${\Delta}E_{ab}$) increased. The pH and sucrose contents decreased, and fructose and glucose contents increased with increasing heating temperature and time. Organic acids, such as formic acid, lactic acid, and levulinic acid, and HMF contents increased with increasing heating temperatures and times. EDA (%) and the AEAC of the heated sucrose solutions increased with increasing heating temperature and time. The heated sucrose solution was more effective than unheated sucrose solution, having higher EDA (90 fold), and AEAC (13 fold).

A New Technology for Strengthening Surface of Forging Die

  • Xin Lu;Zhongde Liu
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2003.10b
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    • pp.189-192
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    • 2003
  • The Electro-thermal Explosion Coating (EEC) technique is a new surface treatment technology emerged in recent years. It uses an electrical discharge (with very high voltage from 5 to 30 kV or more) to produce a pulse current with large density inside the material to be deposited, the metal wire undergo the heating, melting, vaporization, ionization and explosion processes in a very short time (from tens ns to several hundreds ${\mu}s$), and the melted droplets shoot at the substrate with a very high velocity (3000 - 4500 m/s), so that the coating materials can be deposited on the surface of the substrate. Coatings with nano-size grains or ultra- fine grains can be formed because of rapid solidification (cooling rate up to $10^6-10^9\;k/s$). Surface of the substrate (about $1-5{\mu}m$ in depth) can be melted rapidly and coatings with very high bonding strength can be obtained.

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Selective Growth of Multi-walled Carbon Nanotubes by Thermal Chemical Vapor Deposition and Their Field Emission Characteristics

  • Jeong, Se-Jeong;Lee, Seung-Hwan;Lee, Nae-Sung;Han, In-Taek;Kim, Ha-Jin;Kim, Jong-Min
    • 한국정보디스플레이학회:학술대회논문집
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    • 2005.07b
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    • pp.1096-1099
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    • 2005
  • Multi-walled carbon nanotubes (CNTs) grown on catalyst dots by thermal chemical vapor deposition were vertically aligned with a high population density. Such densely populated CNTs showed poor field emission characteristics due to the electrical screening effect. We reduced the number density of CNTs using an adhesive tape treatment. For dotpatterned CNTs, the tape treatment decreased the CNT density by three orders of magnitude, drastically improved the turn-on electric field from 4.8 to $1.8V/{\mu}m$, and changed the emission image from spotty to uniform luminescence. We also report long-term emission stability of dot-patterned CNTs by measuring the emission currents with time at different duty ratios.

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A study of DSC using Ultrasonic and Thermal treatment on Photo-Electrode (염료감응형 태양전지 광전극 초음파 열처리에 관한 연구)

  • Hong, Ji-Tae;Kim, Mi-Jeong;Sim, Ji-Yong;Seo, Hyun-Woong;Kim, Hee-Je
    • Proceedings of the KIEE Conference
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    • 2007.07a
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    • pp.1291-1292
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    • 2007
  • Recently, there were many researches for efficiency improvement of DSC. Among of these works, research of surface treatment is still a prerequisite for electron diffusion, light-harvesting and surface state of DSC.[1] Using of the surface treatment, it can be raise up porosity of $TiO_2$ nano-crystalline structure on photo-electrode. There are chemical, physical, electrical and optical methods which raise up its porosity. In this paper, we have designed and manufactured MOPA-type ultrasonic circuit (100W, frequency and duty variable). Manufactured ultrasonic circuit to use to force cavity density and power into $TiO_2$ paste. Then, we have optimized forcing time, frequency and duty of ultrasonic irradiation for surface treatment of photo-electrode of DSC. In I-V characteristic test of DSC, ultrasonic and thermal treated DSC shows 19% improved its efficiency against monolithic DSC. And it shows stability of light-harvesting from drastically change of light irradiation test.

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Evaluation of Photocatalysis-Fixed Using Titanium for Advanced Wastewater Treatment (고도처리를 위한 금속티타늄 고정화광촉매기술평가)

  • Jang, Jun-Won;Min, Jee-Eun;Park, Jae-Woo
    • 한국방재학회:학술대회논문집
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    • 2008.02a
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    • pp.815-818
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    • 2008
  • Titanium was oxidized with oxygen plasma and calcinated with rapid thermal annealing for degradation of humic acid dissolved in water. Titania photocatalytic plate was produced by titanium surface oxidized with oxygen plasma by Plasma Enhanced Chemical Vapor Deposition(PECVD). RF-power and deposition condition is controlled under 100 W, 150 W, 300 W and 500 W. Treatment time was controlled by 5 min and 10 min. The film properties were evaluated by the X-ray Photoelectron Spectroscopy (XPS) and X-Ray Diffraction (XRD). From the experimental results, we found the optimal condition of titania film which exhibited good performance. Moreover photocatalytic capacity was about twice better than thermal spray titania film, and also as good as titania powder.

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On prediction temperature and microstructure change in large cast-forged product (대형 주.단조품의 온도 및 조직변화 예측에 관한 연구)

  • Lee, M.W.;Lee, Y.S.;Lee, S.W.;Kim, S.S.;Moon, Y.H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.10a
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    • pp.414-419
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    • 2009
  • Good control of thermal energy helps to increase characteristics and eliminate defects of large cast-forged part, such as large sized forged shell. Thermal energy control is a important factor. We have studied about forging process and after heat treatment process by FEM simulation. There are three ways of process. Changes of temperature and microstructure for forged shell were predicted according to temperature declination in large cast-forged product. So we will be able to choose the proper time from heat treatment conditions by FEM simulation.

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Thermal Assisted UV-Ozone Treatment to Improve Reliability of Ag Nanoparticle Thin Films

  • Lee, Inhwa;Kim, Taek-Soo
    • Journal of the Microelectronics and Packaging Society
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    • v.21 no.1
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    • pp.41-44
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    • 2014
  • We employed UV-Ozone treatment method for the fabrication of dense and highly conductive nanoparticle thin films. We demonstrated the UV-Ozone treatment effect on the silver nanoparticle thin films as a function of time and temperature. The capping layers of nanoparticles were decomposed after UV-Ozone treatment and dense nanoparticle thin films were obtained. Moreover, electrical and mechanical properties of the thin films after UV-Ozone treatment were measured by using resistance measurements under tension in an in-situ tensile tester. The initial resistance of nanoparticle thin films was decreased by 82.6% with optimized UV-Ozone treatment condition of $150^{\circ}C$ for 20 minutes.