• Title/Summary/Keyword: the standard of reference

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Quantitative Determination of $UO2^{2+}$ with Modified $[Ru(v-bpy)_3]^{2+}$ Polymer Film Electrode (수식된 $[Ru(v-bpy)_3]^{2+}$ 고분자 피막전극을 이용한 U(VI)의 정량)

  • Cha, Seong-Keuck
    • Journal of the Korean Chemical Society
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    • v.44 no.1
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    • pp.17-23
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    • 2000
  • Electrodes of the polycationic film with electropolymerized $[Ru(v-bpy)_3]^{2+}$ having about 1:1 ratio of $PF6^-/ClO_4^-$as the doped counter ions, were modified with xylenol orange and diethylditbiocarbamate by ion exchange which had stability constant as 38.6 and 17.5 respectively. These electrodes were employed in the quantitative multiple determination of U(W) in solution. The working electrode of electrochemical cell for the analytical signal was Pt/p-$[Ru(v-bpy)_3]^{2+}$, ligand, U(VI) with Ag/AgCl reference elecrode. In the stripping voltammetry. electrode process was electron transfer controlled one and calibration curves at the ranges of $1.0{\times}10^{-3}{\sim}1.0{\times}10^{-7}$ M had excellent relationship as 0.99 and relative standard deviation as 5${\sim}$8%.

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The role of matrix modifier for the determination of Lead (Pb) in blood by graphite furnace atomic absorption spectrometry (흑연로 원자흡수분광법에 의한 혈중 납분석시 매트릭스 변형제의 역할)

  • Yoo, Kwang-Sik;Kwon, Jin-Kee
    • Analytical Science and Technology
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    • v.5 no.4
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    • pp.349-358
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    • 1992
  • The direct determination of lead in the whole-blood by graphite furnace atomic absorption spectrometric analysis was carried out by using the sample which was diluted five-fold with 1% Triton X-100. Matrix modification was tried to remove the interferences of blood matrix and also to get the optimum analytical condition. Good agreement with certificated values in reference materials(bovine blood) supplied by comparison program in Japan was obstained when 1% $(NH_4)_2HPO_4$ as matrix modifier and ashing temperature, $700^{\circ}C$ were used or 1% $(NH_4)_2HPO_4$ and 0.1% $PdCl_2$ as matrix modifier and ashed at $700^{\circ}C$. Standard deviations were appeared as 2.2~6.3% for 1% $(NH_4)_2HPO_4$ and 3.1~9.1% for 1% $(NH_4)_2HPO_4$ and 0.1% $PdCl_2$ in the range of $31{\sim}624{\mu}gPb/l$.

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Making of sRGB image through digital camera colorimetric characterization (디지털 카메라 색 특성분석을 통한 sRGB 이미지 생성)

  • 유종우;김홍석;박승옥;박철호;박진희
    • Korean Journal of Optics and Photonics
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    • v.15 no.2
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    • pp.183-189
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    • 2004
  • As high quality digital cameras become readily available, digital cameras are being used not only for simple picture recording but also as information storing media in various fields. However, due to the fact that the spectral responses of the camera sensors are different from color matching functions of the CIE standard observer, the color can not be measured using these cameras. This study shows a method for converting camera image to sRGB image, in which color information is preserved. The transfer matrix between camera output signals and CIE stimulus values was determined using a multiple regression method with Macbeth ColorChecker as target colors. The CIE stimulus values for camera output signals can be mapped with a transfer matrix, and these values are converted to sRGB signals. As the result of testing a Kodak DC220 digital camera, the average color difference of Macbeth ColorChecker between true and displayed colors was 2.1 $\Delta$ $E_{ab}$ $^{*}$.$^{*}$.

A Study on the Documentation Styles of Online Resources and the Documentation Styles Suggested by Graduate Schools and Scholarly Journals in Korea (온라인 자료의 인용 및 참고문헌 수록 양식과 국내 대학 및 학술잡지에서 사용하고 있는 인용 및 참고문헌 수록 양식 조사연구)

  • 박온자
    • Journal of the Korean Society for information Management
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    • v.16 no.2
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    • pp.81-104
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    • 1999
  • Researchers commonly begin a project by studying past works in the area and deriving relevant information and ideas from their predecessors. In presenting their works researchers acknowledge their debts to preflecessors by carefully documenting each source to indicate what they borrowed. The obvious form of plagiarism is to cokx without crediting the sources. Students have to learn how to quote and how to make reference lists or works cited at the end of their reports which allow readers to locate and use the sources they used for their reports. Nowadays online information sources through the internet increase day by day, but there is no standard documentation style for citing these sources. In this paper up-to-date documentation styles recommened by APA(American Psychological Association) and MLA(Modern Language Association) are introduced. It was found that the graduate schools and the academic societies in Korea do not keep a certain documentation style consistently by checking the school catalogs and the policy statements on manuscript submisssion to the journals.

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Priority Polling and Dual Token Bucket based HCCA Algorithm for IEEE 802.11e WLAN (IEEE 802.11e WLAN을 위한 우선순위 폴링 및 이중 토큰 버킷 기반의 HCCA 알고리즘)

  • Lee, Dong-Yul;Lee, Chae-Woo
    • Journal of the Institute of Electronics Engineers of Korea CI
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    • v.46 no.4
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    • pp.31-41
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    • 2009
  • IEEE 802.11e proposed by IEEE 802.11 working group to guarantee QoS has contention based EDCA and contention free based HCCA. HCCA, a centralized polling based mechanism of 802.11e, needs a scheduling algorithm to allocate the network resource efficiently. The existing standard scheduler, however, is inefficient to support for QoS guarantee for real-time service having VBR traffic. To improve these limit, in this paper, we First, we propose priority polling algorithm which additionally considers the size of MSI and TXOP based on EDD algorithm to increase number of QSTAs. We also propose a dual token bucket TXOP allocation algorithm to reduce congestion caused by stations which enters network with considerable delay variance. TSPEC parameters, Maximum Burst Size (MBS) and Peak Data Rate (PR), are applied to design depth and token generation rate of two buckets. Simulation results show that the proposed algorithm has much higher performance compared with reference and SETT-EDD scheduler in terms of throughput and delay.

Development of Materials Strength Database (재료강도특성(材料强度特性) 데이터베이스 구축(構築))

  • Kim, Ik-Cheol
    • Journal of Information Management
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    • v.23 no.1
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    • pp.1-21
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    • 1992
  • The importance of factual database is becoming larger and larger as the application of computer in design and processing is increasing. To follow up and support this demand and tendency, construction of factual database is necessary. The goal of this research project is to construct a factual database about the creep properties of high temperature materials. A factual database on the creep properties of 25 kinds of high temperature materials was constructed. Domestically produced data which were appeared in journals, theses, reports, etc., were collected and used as a input data source. Evaluation on these collected data will be done during the 2nd year of this project. In addition to this database construction, an experimental facility to produce creep crack propagation data was set up.

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A Comparative Study on the Determination of the Selenium in Biological Samples using 75Se and 77mSe Nuclides (75Se과 77mSe 핵종을 이용한 생물시료 중의 셀렌 분석에 대한 비교 연구)

  • Moon, Jong-Hwa;Kang, Sang-Hoon;Kim, Sun-Ha;Chung, Yong-Sam;Kim, Young-Jin
    • Analytical Science and Technology
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    • v.18 no.1
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    • pp.23-26
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    • 2005
  • Se is well known as an anti-oxidant trace element and many customers are interested in an analysis and contents of Se in the various foodstuff samples. This study was aimed at establishig and comparing an analytical method for the determination of the Se in biological samples by neutron activation analysis using two nuclides, $^{75}Se$ and $^{77m}Se$. Keeping this objective, three NIST biological standard reference materials were chosen and the concentrations of the Se were determined under the prefixed analytical conditions such as the irradiation, decay and measurement time. The measured values by both analytical methods were evaluated with certified values. In addition, the detection limits and measurement uncertainty for the analytical results using $^{75}Se$ and $^{77m}Se$ were compared with each other.

Estimation of De-jitter Buffering Time for MPEG-2 TS Based Progressive Streaming over IP Networks (IP 망을 통한 MPEG-2 TS 기반의 프로그레시브 스트리밍을 위한 de-jitter 버퍼링 시간 추정 기법)

  • Seo, Kwang-Deok;Kim, Hyun-Jung;Kim, Jin-Soo;Jung, Soon-Heung;Yoo, Jeong-Ju;Jeong, Young-Ho
    • Journal of Broadcast Engineering
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    • v.16 no.5
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    • pp.722-737
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    • 2011
  • In this paper, we propose an estimation of network jitter that occurs when transmitting TCP packets containing MPEG-2 TS in progressive streaming service over wired or wireless Internet networks. Based on the estimated network jitter size, we can calculate required de-jitter buffering time to absorb the network jitter at the receiver side. For this purpose, by exploiting the PCR timestamp existing in the TS packet header, we create a new timestamp information that is marked in the optional field of TCP packet header to estimate the network jitter. By using the proposed de-jitter buffering scheme, it is possible to employ the conventional T-STD buffer model without any modification in the progressive streaming service over IP networks. The proposed method can be applicable to the recently developed international standard, MPEG DASH (dynamic adaptive streaming over HTTP) technology.

GIS Interoperability Issues for ITS Services : Map Datum and Location Referencing

  • Choi, Kee-Choo
    • Journal of Korea Spatial Information System Society
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    • v.1 no.1 s.1
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    • pp.57-67
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    • 1999
  • Two GIS and/or OGIS issues for ITS interoperability have been proposed and reviewed with some implications to Korean setting. They are location referencing and ITS map datum. The former must support ITS communication and data sharing. Therefore, an introduction of location referencing and other related issues have been addressed along with the Oak Ridge National Lab.'s (ORNL) location referencing scheme. The latter, proposed by ORNL, is a planned network of anchor points across the nation, that could potentially serve as a positional reference for ITS application (Gottsegen, 1997). It is composed of a set of nodes and links in a standard non-plannar network at a coarse scale for the entire nation for referencing purposes. To provide case of real time traffic information and to guarantee the seamless interoperability, we do need to develop the core ITS map datum as a national infrastructure, and the location referencing scheme should also be either developed or borrowed and localized to meet the domestic needs. Some institutional issues are also addressed along with the future research agenda.

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A Comparison of Sonication and Microwave-assisted Extraction Method for Speciation of Arsenic in Fish Tissue, DORM-2 (어류중 비소의 종분화 분석을 위한 초음파 추출법과 마이크로파 추출법의 비교)

  • Yoon, Cheol-Ho;Park, Yong-Chul;Hong, Jong-Ki
    • Analytical Science and Technology
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    • v.16 no.2
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    • pp.134-142
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    • 2003
  • Comparison of a microwave-assisted extraction with sonication extraction was performed for arsenic speciation in fish tissue with chromatographic separation and inductively coupled plasma mass spectrometry detection. The detection limits of arsenicals with ultrasonic nebulizerand cross-flow nebulizer were shown to be similar. The arsenicals investigated were arsenobetaine (AsB), arsenite [As(III)], dimethylarsine acid (DMA), monomethylarsonic acid (MMA), arsenate [As(v)], and phenylarsonic acid (PAA). Quantitative extraction of arsenicals from dogfish muscle, DORM-2, standard reference material of NRCC (National Research Council of Canada) was achieved using 50% (v/v) methanol-water in both extraction methods. Extraction efficiency of arsenobetaine in both methods is greater than 82% with RSDs on replicates of less than 5%. The concentrations of AsB determined in extract of microwave assisted extraction and sonication methods were $14.18{\pm}0.42mg\;kg^{-1}$ and $13.54 {\pm}0.84mg\;kg^{-1}$, respectively. And the concentrations of DMA were $0.45{\pm}0.06mg\;kg^{-1}$ and $0.44{\pm}0.06mg\;kg^{-1}$, respectively.