• Title/Summary/Keyword: temperature-sensitive

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A Study on Synthesis of Acrylic Pressure Sensitive Adhesive for Polarizer Film by Solution Polymerization (용액중합에 의한 편광필름용 아크릴 점착제의 합성에 관한 연구)

  • Lim, Chang-Hyuk;Jung, Young-Jae;Cho, Ur-Ryong
    • Elastomers and Composites
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    • v.44 no.2
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    • pp.175-181
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    • 2009
  • The solution polymerization was conducted to synthesize pressure sensitive adhesive for polarizer film using acrylic monomers. 2-Ethylhexyl acrylate, butyl acrylate, acrylic acid were used as acrylic monomers, benzoyl peroxide as initiator, ethyl acetate as solvent. The ratio of monomers was 2-ethylhexyl acrylate: butyl acrylate: acrylic acid = 25:50:3.6 reflecting $-40^{\circ}C$ of glass transition temperature in the pressure sensitive adhesive. The amount of initiator was determined as 0.09% to monomer considering wetting power and initial tackiness. The ratio of monomer to solvent was determined as 1:1.7 considering wetting power and transmissivity. The transmissivity of pressure sensitive adhesive increased with decreasing both viscosity and molecular weight due to reducing of refractive index by low entanglement between molecules. In the measurement of pot life, it was found that the storage stability was good at 1:1.7 of monomer: solvent without large change of viscosity during 200 min.

Rapid and Sensitive Detection of Salmonella in Chickens Using Loop-Mediated Isothermal Amplification Combined with a Lateral Flow Dipstick

  • Liu, Zhi-Ke;Zhang, Qiu-Yu;Yang, Ning-Ning;Xu, Ming-Guo;Xu, Jin-Feng;Jing, Ming-Long;Wu, Wen-Xing;Lu, Ya-Dong;Shi, Feng;Chen, Chuang-Fu
    • Journal of Microbiology and Biotechnology
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    • v.29 no.3
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    • pp.454-464
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    • 2019
  • Salmonellosis is a highly contagious bacterial disease that threatens both human and poultry health. Tests that can detect Salmonella in the field are urgently required to facilitate disease control and for epidemiological investigations. Here, we combined loop-mediated isothermal amplification (LAMP) with a chromatographic lateral flow dipstick (LFD) to rapidly and accurately detect Salmonella. LAMP primers were designed to target the Salmonella invA gene. LAMP conditions were optimized by adjusting the ratio of inner to outer primers, $MgSO_4$ concentration, dNTP mix concentration, amplification temperature, and amplification time. We evaluated the specificity of our novel LAMP-LFD method using six Salmonella species and six related non-Salmonella strains. All six of the Salmonella strains, but none of the non-Salmonella strains, were amplified. LAMP-LFD was sensitive enough to detect concentrations of Salmonella enterica subsp. enterica serovar Pullorum genomic DNA as low as $89fg/{\mu}l$, which is 1,000 times more sensitive than conventional PCR. When artificially contaminated feed samples were analyzed, LAMP-LFD was also more sensitive than PCR. Finally, LAMP-LFD gave no false positives across 350 chicken anal swabs. Therefore, our novel LAMP-LFD assay was highly sensitive, specific, convenient, and fast, making it a valuable tool for the early diagnosis and monitoring of Salmonella infection in chickens.

Humidity-Sensitive Characteristics and Reliabilities of Polymeric Humidity Sensors Using 2-Methacryloxyethyl dimethyl 2-hydroxyethyl ammonium brornide (2-Methacryloxyethyl dimethyl 2-hydroxyethyl ammonium bromide를 이용한 고분자 습도센서의 감습 특성 및 신뢰성)

  • Lee, Chil-Won;Gong, Myoung-Seon
    • Applied Chemistry for Engineering
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    • v.10 no.3
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    • pp.461-466
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    • 1999
  • The humidity sensor containing ammonium salt was prepared from the copolymer of 2-methacryloxyethyl dimethyl 2-hydroxyethyl ammonium bromide (MDHAB)/MMA/DAEMA = 6/3/1. The humid membrane was fabricated on the gold/alumina electrode by dipping. The impedances were $298k{\Omega},\;11k{\Omega}$, and $2.3k{\Omega}$ at 40%RH, 70%RH and 90%RH, respectively, at $5^{\circ}C$ and the humidity-sensitive characteristics were suitable for low temperature humidity sensor. The temperature-dependent coefficient between $5^{\circ}C$ and $20^{\circ}C$ was found to be $-0.80%RH/^{\circ}C$ and the hysteresis falled in the ${\pm}2%RH$ range. The response time was found to be 38 sec for the relative humidity ranging from 34%RH to 88%RH at $20^{\circ}C$. The reliabilities such as temperature cycle, humidity cycle, high temperature and humidity resistance, electrical load stability, stability of long-term storage and water durability were measured and evaluated for the application as a humidity sensor.

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Hydrothermal Synthetic Study of Zeolites from Siliceous Mudstone (규질 이암으로부터 제올라이트의 수열 합성에 관한 연구)

  • 노진환
    • Journal of the Mineralogical Society of Korea
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    • v.13 no.4
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    • pp.171-185
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    • 2000
  • Siliceous mudstones are embedded on a large scale in the Tertiary formations of Pohang area. Some useful zeolites such as NsP, (Na, TMA)P, analcime and hydroxysodalite were synthesized from the siliceous mudstones by treating with the variety of solution, i.e ., NaOH, NaOH+NaCl, NaOH, NaOH+$NaAlO_2$and NaOH+TMAOH at the low-temperature hydrothermal system ranging 60~12$0^{\circ}C$. Major precursor of zeolites is found as opal-CT in the zeolite-forming reaction. Smectite, which is included in considerable amounts in the mudstone, appears to play a major role of Al-source in the zeolite synthesis. In comparison, chalcedonic quartz and mica are rather insoluble in alkaline solution, and thus, these are observed as major impurities in the reaction products. An addition of $NaAlO_2$to NaOH solution is effective for eliminating these impurities in the reaction procedure, through these are partly dissolved when elevating the reaction temperature, concentration, and time. Phase change from NaP to hydroxysodalite takes place at the NaOH concentrations of 3.0~4.0 M, and the reaction is not sensitive to the temperature shift. NaP is more stable at lower NaOH concentration and higher activity of $Na_{+}$ whereas analcime is sensitive to the temperature change and stable at higher than $100^{\circ}C$ and 2.0~4.0 M in NaOH concentration. For the pure NaP synthesis without any other products, the treatment of mudstones with 1:1 solution of NaOH and $NaAlO _2$ turns out to be quite effective. NaP was successfully synthesized together with analcime at $100^{\circ}C$ as well as lower concentrations of NaOH+NaCl solution. In addition, the organic type, (Na, TMA)P was formed together with smectite in the 1:1 solution of NaOH and TMAOH.

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Partial Characterization of Bacillus thuringiensis var. kurstaki Temperature-sensitive Mutants (Bacillus thringiensis var. kurstaki 감온성 돌연변이주의 일부특성)

  • 김영권;유관희;이형환;이호원
    • Korean Journal of Microbiology
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    • v.23 no.3
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    • pp.203-208
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    • 1985
  • Partial characterization of B. thuringiensis var. kurstaki 3ab temperature-sensitive mutants was carried out through biochemical analyses, utilization tests of carbohydrate sources, antobiotic resistant test, hemolytic reaction test, growth measurement of Fructus gardenia sxtrant medium and toxicity test against mice. Six ts mutants, ts-U154, ts-U601, ts-U602, ts-U603, tsU-604, and ts-U788 could not produce urease, ts-U603 lost its motility, ts-U154 could not use salicin and cellobiose and ts-U603 not ribose. All ts mutants except ts-U154 and wild type strain were resistant to cephalothin, ampicillin, and penicillin. but ts-U154 was sensitive to the three. Four mutants, ts-U21, ts-U74, ts0U131 and ts-U154 did not form pigment colonies on the F. gardenia medium. All the mutants and wild type strain showed hemolysis reaction on the blood agar. The B. thuringiensis and mutants were not toxic to mice.

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Synthesis and Characterization of Biodegradable Thermo- and pH-Sensitive Hydrogels Based on Pluronic F127/Poly($\varepsilon$-caprolactone) Macromer and Acrylic Acid

  • Zhao, Sanping;Cao, Mengjie;Wu, Jun;Xu, Weilin
    • Macromolecular Research
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    • v.17 no.12
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    • pp.1025-1031
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    • 2009
  • Several kinds of biodegradable hydrogels were prepared via in situ photopolymerization of Pluronic F127/poly($\varepsilon$-caprolactone) macromer and acrylic acid (AA) comonomer in aqueous medium. The swelling kinetics measurements showed that the resultant hydrogels exhibited both thermo- and pH-sensitive behaviors, and that this stimuli-responsiveness underwent a fast reversible process. With increasing pH of the local buffer solutions, the pH sensitivity of the hydrogels was increased, while the temperature sensitivity was decreased. In vitro hydrolytic degradation in the buffer solution (pH 7.4, $37^{\circ}C$), the degradation rate of the hydrogels was greatly improved due to the introduction of the AA comonomer. The in vitro release profiles of bovine serum albumin (BSA) in-situ embedded into the hydrogels were also investigated: the release mechanism of BSA based on the Peppas equation was followed Case II diffusion. Such biodegradable dual-sensitive hydrogel materials may have more advantages as a potentially interesting platform for smart drug delivery carriers and tissue engineering scaffolds.

A Survey on the Aged Consumers' Needs for an Elderly Friendly and Sensitive Bathtub Alternative (노인 친화적 감성용 욕조 대안에 대한 노인 소비자의 요구 및 평가)

  • Choi, Byungsook;Kwon, Tae-Kyu
    • Journal of the Korean housing association
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    • v.24 no.6
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    • pp.41-49
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    • 2013
  • This study finds out the aged consumers' needs on the developing elderly friendly and sensitive bathtub. This bathtub focuses on enhancement of multi-senses and enhancement of health, safety & convenience during bath. The enhancing multi-senses would have four functions; therapy with color and aroma, the massage with micro water bubbles, the visual and auditory with TV & cinema, and the auditory with music and radio. Also, enhancing others of bathtub would have seven functions; emergency bell, blood-pressure check system for health condition, water temperature indicator, keeping water warm, reading a book in that, and controlling of house entrance door and a getting the phone during bath. The aged consumers' needs find throughout a questionnaire survey, and 497 data was analyzed. The main results are as follow. They consider a full bath behavior as a healthcare. They have an intention to purchase or use the elderly and friendly bathtub, and they prefer using it in common facilities to using it at home. They highly need health related function of bathtub, which are massage (64.4%), blood-pressure check system (55.1%) and aroma therapy (45.7%). The emergency bell (67.0%), keeping water warm (62.2%), and water temperature indicator (49.7%), related to safety & information function of bathtub, are needed. Also, they think tolerance for error and low physical effort in bathtub design alternative, opening door and inside sitting support, to be important.