• Title/Summary/Keyword: temperature cycles

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Endurance Life and Deformation Behavior under Thermo-mechanical Fatigue of Nb-added Heat Resistant Austenitic Stainless Steel (Nb 첨가 오스테나이트계 내열 스테인리스강의 열기계적 피로 수명 및 변형 거동)

  • Oh, Yong Jun;Park, Joong-Cheul;Yang, Won Jon
    • Korean Journal of Metals and Materials
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    • v.49 no.7
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    • pp.541-548
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    • 2011
  • Thermomechanical fatigue (TMF) behavior of heat resistant austenitic stainless steel was evaluated in the temperature range from 100$^{\circ}C$ to peak temperatures of 600 to 800$^{\circ}C$; The fatigue lives under TMF conditions were plotted against the plastic strain range and the dissipated energy per cycle. In the expression of the inelastic strain range versus fatigue life, the TMF data obtained at different temperature ranges were located close to a single line with a small deviation; however, when the dissipated energy per cycle, calculated from the area of the stress-strain hysteresis loops at the half of the fatigue life, was plotted against the fatigue life, the data showed greater scattering than the TMF life against the inelastic strain range. A noticeable stress relaxation in the stress-strain hysteresis curve took place at the peak temperatures higher than 700$^{\circ}C$, but all specimens in this study exhibited cyclic hardening behavior with TMF cycles. Recrystallization occurred during the TMF cycle concurrent with the formation of fine subgrains in the recrystallized region, which is considered to cause the cyclic hardening of the steel.

Regeneration of Zeolite 5A in the Adsorption Process for Isoprene Purification (이소프렌 정제를 위한 제올라이트 5A 흡착제 재생)

  • Jeon, Kyung-Jin;Yoo, Kye-Sang;Lee, Chang-Ha;Ahn, Byoung-Sung
    • Clean Technology
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    • v.16 no.4
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    • pp.272-276
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    • 2010
  • Adsorption process for the removal of acetylene, especially 2-butyne, from isoprene was studied with zeolite as an adsorbent. In this work, zeolite 5A was selected to investigate the effects of various regeneration conditions by repeated adsorption experiments. The effect of regeneration temperature and desorption pressure was investigated to identity the optimum regeneration conditions. Repeated adsorption and desorption experiments were carried out for 10 cycles to confirm the efficiency of regeneration process under temperature of 423 K and desorption time of 16 h.

A study on the temperature guidelines for weapon system test and evaluation in the Korean peninsula (무기체계의 환경시험을 위한 한반도의 온도기준 설정에 관한 연구)

  • Moon, Jayoung;Kim, DongGil;Sung, InChul;Hong, YeonWoong
    • Journal of the Korean Data and Information Science Society
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    • v.27 no.6
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    • pp.1593-1600
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    • 2016
  • This paper suggests a temperature guidance for requirements which must be addressed in the preparation of specifications for military equipment used in land applications in the Korean peninsula. In general, the equipment should be designed to operate during all but a certain small percentage of the time. Daegu and Yangpyeong are the hottest and coldest regions by month, respectively, based on surface weather observations over 132 regions from 1904 to 2014. The 1-percent high and low temperatures for land environment in the South Korea are $38.7^{\circ}C$, and -$29.0^{\circ}C$, respectively. This paper also presents the temperature values occurring for specified frequencies of occurrence during the most severe month. Diurnal cycles associated with the hottest and coldest top one-percent temperatures, including associated solar radiation, relative humidity, and wind-speed are provided.

A Study on Growth Behavior of Small Fatigue Crack in 304 Stainless Steel at Elevated Temperatures (고온하 304 스테인레스강의 작은 표면구열의 성장거동에 관한 연구)

  • 서창민;김영호
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.14 no.1
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    • pp.87-95
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    • 1990
  • Rotating bending fatigue tests of an authentic steel 304 were performed at various temperatures such as room temperature, $538^{\circ}$ and $593^{\circ}C$. The plastic replica method was also applied in order to estimate the fatigue life on the basis of serial observation of small fatigue crack initiation and growth on the pit specimen surface. The fatigue crack growth behavior of 304 stainless steel was investigated within the frame work of elastic-plastic fracture mechanics within a narrow scatterband in spite of different stress levels at elevated temperature as at room temperature. The growth law of small surface crack is determined uniquely by the term. $\DELTA\sigma^{n}a$ where $\DELTA\sigma$ is the stress amplitude, a is the crack length, and n is a constant. It is found that the small crack growth behavior is basically equivalent to the S-$N_{f}$ relationship, where S and $N_{f}$ are stress and number of cycles to failure, and the fatigue life prediction is in good agreement with the experimental results.

Stable Oxygen and Carbon Isotope Profiles of the Bivalve Shells collected from Coastal Regions of Korea: Comparison of the Coastal Water Properties

  • Khim, Boo-Keun
    • Journal of the korean society of oceanography
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    • v.32 no.1
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    • pp.28-37
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    • 1997
  • Two marine bivalve shells were collected from the eastern and western coastal regions of Korea, respectively. Stable oxygen and carbon isotope profiles are constructed using the incremental sampling along the axis of maximum growth to provide the continuous ${\delta}^{18}$O and ${\delta}^{13}$C records, which register the physical, biological and chemical properties of seawater where the organisms live. Cycles in the ${\delta}^{18}$O profiles are interpreted as annual along with the identification of annual growth bands; the maximum ${\delta}^{18}$O values correspond with the coldest temperature of seawater whereas the minimum ${\delta}^{18}$O values with the warmest temperature. The primary control on the amplitude of the ${\delta}^{18}$O profiles is seasonal variation of seawater temperature. The offset of the baseline between ${\delta}^{18}$O values of the two specimens is attributed to differences in both temperature and seawater ${\delta}^{18}$O values between two localities. The ${\delta}^{13}$C profiles show the similar seasonality of carbon cycling associated with phytoplankton productivity. The offset in the ${\delta}^{13}$C profiles between two specimens may be, as in the case of oxygen isotope profile, attributed to the different ${\delta}^{13}$C value of the seawater DIC (dissolved inorganic carbon) between the western coast and the eastern coast. Relationships between the shell isotopic composition and the coastal water properties of shell growth are readily interpreted from the ${\delta}^{18}$O-${\delta}^{13}$C pair diagram of the shell isotope data, similar to the use of salinity-${\delta}^{18}$O diagram for identifying water masses. The preliminary stable isotope results of this study suggest that mollusk shell isotope geochemistry may be useful to monitor the properties of water masses in the coastal and inner shelf setting around Korea and improve the interpretation of paleoceanography, provided the fossil mollusks are well preserved.

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A Numerical Analysis on Transient Fuel temperatures in a Military Aircraft under Non-operating Ground Static Condition (지상 정적 상태에서의 항공기내 연료온도변화에 대한 수치해석)

  • 김영준;김창녕
    • Journal of Energy Engineering
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    • v.12 no.1
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    • pp.11-16
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    • 2003
  • A numerical study was performed on the transient fuel temperatures of a military aircraft stationed under non-operating static condition. Numerical calculation was peformed by an explicit method using modified Dufort-Frankel scheme. It was assumed that the non-operating aircraft is subjected to repeated daily cycles of air temperature with the solar radiation and wind speed corresponding to the 1 % hot day ambient condition. And, the aircraft was assumed to be in turbulent flow. The convective heat transfer coefficient for turbulent flow on the flat plate suggested by Eckert was employed to calculate heat transfer between the aircraft surface and the ambience. The energy conservation equation on fuel was used as governing equation for this analysis. As a result of this analysis, the wing tank temperature showed the highest temperature and the largest rate of temperature changes among fuel tanks. The results of this analysis could be used as initial foe] temperatures for analysis of the transient fuel temperatures in various flight missions. Also, this analysis method could be used to analysis and design of an aircraft thermal energy management system.

Immobilization of Laccase on $SiO_2$ Nanocarriers Improves Its Stability and Reusability

  • Patel, Sanjay K.S.;Kalia, Vipin C.;Choi, Joon-Ho;Haw, Jung-Rim;Kim, In-Won;Lee, Jung Kul
    • Journal of Microbiology and Biotechnology
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    • v.24 no.5
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    • pp.639-647
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    • 2014
  • Laccases have a broad range of industrial applications. In this study, we immobilized laccase on $SiO_2$ nanoparticles to overcome problems associated with stability and reusability of the free enzyme. Among different reagents used to functionally activate the nanoparticles, glutaraldehyde was found to be the most effective for immobilization. Optimization of the immobilization pH, temperature, enzyme loading, and incubation period led to a maximum immobilization yield of 75.8% and an immobilization efficiency of 92.9%. The optimum pH and temperature for immobilized laccase were 3.5 and $45^{\circ}C$, respectively, which differed from the values of pH 3.0 and $40^{\circ}C$ obtained for the free enzyme. Immobilized laccase retained high residual activities over a broad range of pH and temperature. The kinetic parameter $V_{max}$ was slightly reduced from 1,890 to 1,630 ${\mu}mol/min/mg$ protein, and $K_m$ was increased from 29.3 to 45.6. The thermal stability of immobilized laccase was significantly higher than that of the free enzyme, with a half-life 11- and 18-fold higher at temperatures of $50^{\circ}C$ and $60^{\circ}C$, respectively. In addition, residual activity was 82.6% after 10 cycles of use. Thus, laccase immobilized on $SiO_2$ nanoparticles functionally activated with glutaraldehyde has broad pH and temperature ranges, thermostability, and high reusability compared with the free enzyme. It constitutes a notably efficient system for biotechnological applications.

A Design Process for Reduction of Pressure Drop of Air-cooled Condenser for Waste Heat Recovery System (폐열 회수 시스템용 공랭식 응축기의 압력 손실 저감 설계)

  • Bae, Sukjung;Heo, Hyungseok;Park, Jeongsang;Lee, Hongyeol;Kim, Charnjung
    • Transactions of the Korean Society of Automotive Engineers
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    • v.21 no.6
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    • pp.81-91
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    • 2013
  • A novel design process of a parallel multi-flow type air-cooled condenser of a dual-loop waste heat recovery system with Rankine steam cycles for improving the fuel efficiency of gasoline automobiles has been investigated focusing on reduction of the pressure drop inside the micro-tubes. The low temperature condenser plays a role to dissipate heat from the system by condensing the low temperature loop working fluid sufficiently. However, the refrigerant has low evaporation temperature enough to recover the waste from engine coolant of about $100^{\circ}C$ but has small saturation enthalpy so that excessive mass flow rate of the LT working fluid, e.g., over 150 g/s, causes enormously large pressure drop of the working fluid to maintain the heat dissipation performance of more than 20 kW. This paper has dealt with the scheme to design the low temperature condenser that has reduced pressure drop while ensuring the required thermal performance. The number of pass, the arrangement of the tubes of each pass, and the positions of the inlet and outlet ports on the header are most critical parameters affecting the flow uniformity through all the tubes of the condenser. For the purpose of the performance predictions and the parametric study for the LT condenser, we have developed a 1-dimensional user-friendly performance prediction program that calculates feasibly the phase change of the working fluid in the tubes. An example is presented through the proposed design process and compared with an experiment.

Practical Application of Sn-3.0Ag-0.5Cu Lead Free Solder in Electronic Production

  • Chae Kyu-Sang;Min Jae-Sang;Kim Ik-Joo;Cho Il-Je
    • Journal of the Microelectronics and Packaging Society
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    • v.12 no.1 s.34
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    • pp.65-71
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    • 2005
  • At present, Electronic industries push ahead to eliminate the Pb(Lead) -a hazardous material-from all products. Especially, we have performed to select the optimum standard composition of lead free alloy for the application to products for about 3 years from 2000. These days, we have the chance for applying to the mass-production. This project constructed the system for applying the lead free solders on consumer electronic products, which is one of the major products of the LG Electronics. To select the lead free solders with corresponding to the product features, we have passed through the test and applied with Sn-3.0Ag-0.5Cu alloy system to our products, and for the application to the high melting temperature composition, we secured the thermal resistance of the many parts and substrate and optimized the processing conditions. We have operated the temperature cycling test and the high temperature storage test under the standards to confirm the reliability of the products. On these samples, we considered the consequence of our decision by the operating test. For the long life time of the product, we have operated the temperature cycling test at $-45^{\circ}C\;-\;+125^{\circ}C$, 1 cycle/hour, 1000 cycles. Also we have tested the tin whisker growth about lead free plating on lead finish. We have analyzed with the SEM, EDS and any other equipment for confirming the failure mode at the joint and the tin whisker growth on lead free finish.

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Enhanced electrocapacitive performance and high power density of polypyrrole/graphene oxide nanocomposites prepared at reduced temperature

  • Mudila, Harish;Joshi, Varsha;Rana, Sweta;Zaidi, Mohmd. Ghulam Haider;Alam, Sarfaraz
    • Carbon letters
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    • v.15 no.3
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    • pp.171-179
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    • 2014
  • An attempt was made to investigate the effect of the preparation temperature on the electrocapacitive performance of polypyrrole (PPY)/graphene oxide (GO) nanocomposites (PNCs). For this purpose, a series of PNCs were prepared at various temperatures by the cetyltrimethylammonium bromide-assisted dilute-solution polymerization of pyrrole in presence of GO (wt%) ranging from 1.0 to 4.0 with ferric chloride as an oxidant. The formation of the PNCs was ascertained through Fourier-transform infrared spectrometry, X-ray diffraction spectra, scanning electron microscopy and simultaneous thermogravimetric-differential scanning calorimetry. The electrocapacitive performance of the electrodes derived from sulphonated polysulphone-bound PNCs was evaluated through cyclic voltammetry with reference to Ag/AgCl at a scan rate (V/s) ranging from 0.2 and 0.001 in potassium hydroxide (1.0 M). The incorporation of GO into the PPY matrix at a reduced temperature has a pronounced effect on the electrocapacitive performance of PNCs. Under identical scan rates (0.001 V/s), PNCs prepared at $10{\pm}1^{\circ}C$ render improved specific conductivity (526.33 F/g) and power density (731.19 W/Kg) values compared to those prepared at $30{\pm}1^{\circ}C$ (217.69 F/g, 279.43 W/Kg). PNCs prepared at $10{\pm}1^{\circ}C$ rendered a capacitive retention rate of ~96% during the first 500 cycles. This indicates the excellent cyclic stability of the PNCs prepared at reduced temperatures for supercapacitor applications.