• 한국터널지하공간학회 논문집
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• 제15권4호
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• pp.431-442
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• 2013

기존의 연구에서 삼각형 돌출부의 크기 즉 돌출부 길이 및 돌출부 경사각 변화에 따른 전단거동 및 파괴 형상 특성에 대한 광범위한 실험적 연구는 부족하였다. 본 연구에서는 직접전단시험기를 사용하여 삼각형 돌출부의 전단거동에 있어서 돌출부의 길이 및 경사각 특성이 표면 돌출부의 파괴 형상 특성에 미치는 영향을 규명하고자 한다. 이를 위하여 돌출부 길이는 4가지로 변환하였고, 수직응력은 3가지로, 그리고 돌출부 경사각은 3개의 각도로 변환하면서 총 36회의 시험을 수행하였다. 시험을 수행한 시편은 3차원 형상측정기를 사용하여 파괴 형상 특성을 정량적으로 분석하였다. 이러한 시험을 통하여, 수직응력 변화에 따른 돌출부의 파괴 형상 특성을 조사하였다. 또한 각각의 경사각에서 돌출부의 길이를 변화시켜 시험을 수행함으로써, 특정 수직응력 하에서 돌출부가 파괴되는 길이 및 높이를 정의하였다.

• Restorative Dentistry and Endodontics
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• 제20권1호
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• pp.193-213
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• 1995

The purpose of this study is to investigate a possible contribution of nonspecific esterases, which occur in the oral cavity, to the degradation of ester bonds in polymethacrylates. One of the problems connected with the use of composite resins for restorations is their inadequate resistance to wear. It has been shown that methacrylate hydrolysis can be catalyzed by enzymes and that a carboxylic hydrolase (porcine liver esterase) catalyzed the hydrolysis of several mono - and dimethacrylates. The softening effect on a BISGMA/TEGDMA polymer induced by hydrolase will accelerate the in vivo wear of the polymer. Porcine liver esterase (EC 3.1.1.1) 3.2 mol/L $(NH_4)_2$ $SO_4$ was obtained from Sigma Chemical Company. The esterase activity of one unit is defined as the amount of enzyme capable of hydrolyzing $l{\mu}mol$ ethyl butyrate per min at pH 8.0 AT $25^{\circ}C$. Phosphate buffer, 10mmol/L, pH 7.0, was made by adjustment of a solution of $Na_2HPO_4$ with $H_3PO_4$. Composite resins used in this study are Silux Plus, Z-100, Durafil VS, and Prisma APH. Cylindrical specimens, 14mm in diameter and 3mm thick, of Silux Plus, Z-100, Durafil VS, Prisma APH were polymerized under the celluloid strip. 60 specimens were divided into 2 groups. One group was emersed only in buffer solution, the other group was emersed in buffer and enzyme solution. Silux Plus and Z-100 were divided into 2 subgroups, one subgroup was cured only Visilux 2. And the other subgroup was cured Visilux 2 and Triaid II. Thereafter, specimens were polished to its best achievable surface according to manufacture's directions. The Vickers hardness of the specimens was measured after 1, 2, 4, 7, 9, 15, 50 days. The solutions were changed after each measurement. Composite resin surfaces were evaluated for the surface roughness with profilometer (${\alpha}$-step 200, Tencor instruments, USA) after 1 and 50 days. And then surfaces of specimens were pictured with stereosopy after 1 and 50 days. The results were as follows. 1. The surface hardness of Silux plus, durafil VS, and Prisma APH were decreased with time. But, the surface hardness of Z-100 was not decreased. 2. The surface hardness of all composite resins was decreased by esterase. 3. Composite resins, which were light-cured by Visilux 2 and concomitantly baked by oven, showed more hardened surface than light-cured by Visilux 2 only. 4. Significant surface changes were occured in Silux plus after esterase treatment.

• 한국광학회지
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• 제19권6호
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• pp.400-407
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• 2008

퓨리에 변환 적외선 분광기(FT-IR)를 이용한 물질의 적외선 분광 복사율 측정 장치를 구축하고 이 장치의 성능을 평가하였다. 본 장치는 기준 흑체, 시료 가열로, 광학계, FT-IR로 구성되어 있으며, 측정 온도 및 파장 영역은 $200^{\circ}C{\sim}500^{\circ}C$와 $3.5{\mu}m{\sim}20{\mu}m$ 이다. 기준 흑체의 유효 복사율은 0.9993 이상으로 거의 1에 가까운 값을 나타내고 있었으며, 흑체의 분광 복사율에 대한 합성 상대 불확도는 0.69% 이하이다. $300^{\circ}C$에서 불투명한 알루미나, 흑연, 양극 처리된 알루미늄 시료의 수직 분광 복사율과, 금속(IMS200)의 표면 거칠기에 따른 복사율을 측정하였다. 금속(IMS200)의 표면 거칠기에 따른 복사율 변화는 거칠기가 증가할수록 증가하였다.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2004년도 추계학술대회 논문집
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• pp.1066-1069
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• 2004

Recently the monitoring system of tool setup in high speed precision machining tool is required for manufacturing products that have highly complex and small shape, high precision and high function. It is very important to reduce time to setup tool in order to improve the machining precision and productivity and to protect the breakage of cutting tool as the shape of product is smaller and more complex. Generally, the combination of errors that geometrical clamping error of fixing tool at the spindle of machining center and the asynchronized error of driving mechanism causes that the run-out of tool reaches to 3∼20 times of the thickness of cutting chip. And also the run-out is occurred by the misalignment between axis of tool shank and axis of spindle and spindle bearing in high speed rotation. Generally, high speed machining is considered when the rotating speed is more than 8,000 rpm. At that time, the life time of tool is reduced to about 50％ and the roughness of machining surface is worse as the run-out is increased to 10 micron. The life time of tool could be increased by making monitoring of tool-setting easy, quick and precise in high speed machining center. This means the consumption of tool is much more reduced. And also it reduces the manufacturing cost and increases the productivity by reducing the tool-setup time of operator. In this study, in order to establish the concept of tool-setting monitoring the measuring method of the geometrical error of tool system is studied when the spindle is stopped. And also the measuring method of run-out, dynamic error of tool system, is studied when the spindle is rotated in 8,000 ∼ 60,000 rpm. The dynamic phenomena of tool-setup is analyzed by implementing the monitoring system of rotating tool system and the noncontact measuring system of micro displacement in high speed.

• 한국결정성장학회지
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• 제6권3호
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• pp.406-414
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• 1996

본 연구에서는 금속타겟을 이용한 반응성 스퍼터링법을 이용하여 PZT 박막 증착후 냉각시 산소분압에 따른 박막의 상형성 거동 및 전기적 특성에 미치는 영향을 고찰하였다. 냉각시 산소분압의 감소에 따라 박막 표면의 휘발에 기인하여 표면거칠기는 증가하였고 입성장은 거의 일어나지 않았다. 산소분압이 증가할수록 각형비가 보다 우수한 hysteresis 특성을 얻을 수 있었고 산소분압이 감소함에 따라 remanent polarization과 retained polarization이 감소하였으며, 항전계의 감소가 관찰되었다. 산소분압에 따른 유전율-전압 특성 측정에서 산소분입이 감소함에 따라 internal bias field의 증가가 관찰되었으며, 유전율도 조금씩 감소하였다. Field accelerated retention 시험결과 냉각시 산소분압이 감소함에 따라 nonswitched polarization의 증가가 관찰되었고 bias time이 증가함에 따라 nonswitched polarization이 감소하였다.

• 한국환경과학회지
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• 제24권4호
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• pp.371-381
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• 2015

In the mountain streams in Jeju Island, strong turbulence and roughness usually made it nearly impossible to utilize most of intrusive instrumentation for streamflow discharge measurements. Instead, a non-intrusive fixed electro-magnetic wave surface velocimetry (fixed EWSV: Kalesto) became alternatively popular in many representative streams to measure stream discharge seamlessly. Currently, Kalesto has shown noteworthy performance with little loss in flood discharge measurements and also has successfully provided discharge for every minute. However, Kalesto has been operated to regard its measured one-point velocity as the representative mean velocity for the given cross-section. Therefore, it could be highly possible to potentially encompass discharge measurements errors. In this study, we analyzed the difference between such Kalesto discharge measurements and other alternative concurrent discharge measurements such as Acoustic Doppler Current Profiler (ADCP) and mobile EWSV which were able to measure velocity in multi-points in the cross-section. Consequently, Kalesto discharge deviated from ADCP discharge in amount of 48% for relatively low flow, and more than 20% difference for high flow compared with mobile EWSV discharge measurements. These results indicated that the one-point velocity measured by Kalesto should be used as a cross-sectional mean velocity, rather it should be accounted for as an index-velocity in conjunction with directly measured cross-sectional mean velocity by using more reliable instrumentations. After inducing Kalesto Discharge Correction Coefficient (KDCC) that actually means relationship between index velocity and cross-sectional mean velocity, the corrected discharge from Kalesto was significantly improved. Therefore, we found that index velocity method should be applied to obtain better accuracy of discharge measurement in case of Kalesto operation.

• 보존과학회지
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• 제32권3호
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• pp.377-384
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• 2016

철불의 개금 시 표면에 남아 있는 옻칠 제거 방법에는 물리적인 방법과 화학적인 방법을 사용하고 있으나, 표면 손상 및 약품 사용으로 인한 환경오염, 보존과학자의 건강에도 매우 유해하다. 그래서 본 연구에서는 비접촉식이고 친환경적인 Nd:YAG 레이저를 이용하여 옻칠 제거 실험을 실시하였다. 시편은 크기가 $5{\times}5cm$인 철제(Fe 99.9%)시편 표면을 균일하게 연마한 후 생칠을 도포 횟수를 달리하여 각각 $10{\mu}m$, $20{\mu}m$, $30{\mu}m$의 두께 차이로 제작하였다. 본 실험에서 사용된 레이저기기는 Nd:YAG 레이저로, 적외선 영역의 1064 nm(160~800 mJ)와 가시광선 영역인 532nm(50~350 mJ)의 두 가지 파장 모드를 이용하였다. 실험은 레이저 파장 에너지 조사 횟수 등에 따른 시편 표면의 변화를 조사하였다. 레이저 조사 전 후 표면을 실체현미경과 SEM 관찰, 비접촉 표면 조도 측정기, FT-IR 등을 이용하여 옻칠의 제거 및 잔류 여부를 알아보았다. 분석 결과 1064 nm 파장을 이용하여 $1.0J/cm^2$ 밀도에서 표면 손상 없이 $10{\mu}m$, $20{\mu}m$ 두께의 옻칠이 제거됨을 확인할 수 있었다. 이와 같은 결과를 통해 철불 개금 시 잔류하고 있는 옻칠 제거 방법으로 Nd:YAG 레이저가 효율적임을 본 실험을 통해 알 수 있었다. 향후 금속뿐만 아니라 목칠 가구 등 다양한 재질의 연구가 이루어지면 표면 손상 없이 옻칠을 제거 하는데 효과적으로 활용 가능할 것으로 본다.

• 한국재료학회지
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• 제19권11호
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• pp.601-606
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• 2009

$BiFeO_3$ (BFO) thin films were prepared on $Pt/TiO_2/Si$ substrate by r.f. magnetron sputtering. The effects of deposition pressure on electrical properties were investigated using measurement of dielectric properties, leakage current and polarization. When BFO targets were prepared, Fe atoms were substituted with Mn 0.05% to increase electrical resistivity of films. (Fe+Mn)/Bi ratio of BFO thin films increases with increasing partial pressure of $O_2$ gas. The deposited films showed the only BFO phase at 10 mTorr, the coexistence of BFO and $Bi_2O_3$ phase at 30-50 mTorr, and the only $Bi_2O_3$ phase at 70 mTorr. The crystallinity of BFO films was reduced due to the higher Bi contents and the decrease of surface mobility of atoms at high temperature. The porosity and surface roughness of films increased with the increase of the deposition pressure. The films deposited at high pressure showed low dielectric constant and high leakage current. The dielectric constant of films deposited at various deposition pressures was 84${\sim}$153 at 1 kHz. The leakage current density of the films deposited at 10${\sim}$70 mTorr was about $7{\times}10.6{\sim}1.5{\times}10.2A/cm^2$ at 100 kV/cm. The leakage current was found to be closely related to the morphology and composition of the BFO films. BFO films showed poor P-E hysteresis loops due to high leakage current.

• 한국정밀공학회지
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• 제19권4호
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• pp.93-100
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• 2002

The current from the feed motor of a machine tool contains substantial information about the machining state. There have been many researches that investigated the current as a measure for the cutting farces. However it has been reported that this indirect measurement of the cutting farces from the feed motor current is only feasible in low frequency. In this research, it was presented that the bandwidth of the current monitoring can be expanded to 130 Hz. And the unusual behavior of the current was examined in this bandwidth. The cross-feed directional cutting force influences the machined surface of the workpiece, which makes it necessary to estimate this force to control the roughness of the machined sulfate. The current exists in the stationary feed motor, and it can give the useful information on the quality of the machined surface. But the unpredictable behavior of the current prevents applying the current to prediction of the cutting state. Empirical approach was conducted to resolve the problem. As a result, the current was shown to be related to the accumulation of the accumulation of the infinitesimal rotation of the motor. rotation of the motor. Subsequently the relationship between the current and the cutting force was identified.

• 한국재료학회지
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• 제23권6호
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• pp.334-338
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• 2013

In this study, $BaTiO_3$ thin films were grown by RF-magnetron sputtering, and the effects of the thin film thickness on the structural characteristics of $BaTiO_3$ thin films were systematically investigated. Instead of the oxide substrates generally used for the growth of $BaTiO_3$ thin films, p-Si substrates which are widely used in the current semiconductor processing, were used in this study in order to pursue high efficiency in device integration processing. For the crystallization of the grown thin films, annealing was carried out in air, and the annealing temperature was varied from $700^{\circ}C$. The changed thickness was within 200 nm~1200 nm. The XRD results showed that the best crystal quality was obtained for ample thicknesses 700 nm~1200 nm. The SEM analysis revealed that Si/$BaTiO_3$ are good quality interface characteristics within 300 nm when observed thickness. And surface roughness observed of $BaTiO_3$ thin films from AFM measurement are good quality surface characteristics within 300 nm. Depth-profiling analysis through GDS (glow discharge spectrometer) showed that the stoichiometric composition could be maintained. The results obtained in this study clearly revealed $BaTiO_3$ thin films grown on a p-Si substrate such as thin film thickness. The optimum thickness was 300 nm, the thin film was found to have the characteristics of thin film with good electrical properties.