• 한국세라믹학회지
• /
• 제31권11호
• /
• pp.1337-1345
• /
• 1994

Glasses in the system of 45CaO-25TiO2-30P2O5 containing 1 mole% of M2O(M=Li, Na, K) were melted and crystallized. And their crystal phases were Ca3(PO4)2, CaTi4(PO4)6, and TiO2. Porous glass-ceramics with skeleton of two crystal phase CaTi4(PO4)6 and TiO2 were prepared by selective leaching of Ca3(PO4)2 with 0.1 N-HCl. Glass transition temperature(Tg) and crystallization temperature(Tc) were decreased by addition of 1 mole% alkali metal oxide. Pore size of porous glass-ceramics was increased with increasing heat treatment temperature and its dependence on heat treatment temperature was decreased with addition of Na2O and K2O. It was found that porous glass-ceramics of parent glass and containing 1mole% M2O(M=Li, Na, K) composition had maximum specific surface area, porosity and maximum of crystallzed phase by heat treatment at 80$0^{\circ}C$, 76$0^{\circ}C$, 78$0^{\circ}C$, 80$0^{\circ}C$ respectively.

• Journal of Welding and Joining
• /
• 제25권3호
• /
• pp.28-36
• /
• 2007

A bulk amorphous NiTiZrSiSn powder produced using an inert gas atomization was sprayed by kinetic spraying process that is basically a solid-state deposition process onto a mild steel substrate. They were successfully overlaid onto the mild steel substrate. In order to evaluate the tribological behavior of the kinetic sprayed NiTiZrSiSn BMG (Bulk Metallic Glass) coatings, a partially crystallized coating and a fully crystallized coating were prepared by the isothermal heat treatments. Tribological behaviors were investigated in view of friction coefficient, hardness and amorphous phase fraction of coating layer. Surface morphologies and depth in the wear tracks were observed and measured by scanning electron microscope and alpha-step. From the examination of the scratch wear track microstructure, transition from the ductile like deformation (micro cutting) to the brittle deformation (micro fracturing) in the scratch groove was observed with the increase of the crystallinity.

• 한국세라믹학회지
• /
• 제55권5호
• /
• pp.498-503
• /
• 2018

Using the thermal ablation method, the oxidation behavior of $SiC_f/SiC$ composites was investigated in air and in the temperature range of $1,300^{\circ}C$ to $2,000^{\circ}C$. At the relatively low temperature of $1,300^{\circ}C$, passive oxidation, which formed amorphous phase, predominantly occurred in the thermal ablation test. When the oxidation temperature increased, SiO (g) and CO (g) were formed by active oxidation and the dense oxide layer changed to a porous one by vaporization of gas phases. In the higher temperature oxidation test, both active oxidation due to $SiO_2$ decomposition on the surface of the oxide layer and active/passive oxidation transition due to interfacial reaction between oxide and base materials such as SiC fiber and matrix phase simultaneously occurred. This was another cause of high temperature degradation of $SiC_f/SiC$ composites.

• 한국지반공학회지:지반
• /
• 제13권1호
• /
• pp.111-122
• /
• 1997

표면파를 이용하여 지반의 강성을 추정하는 기법인 SASW 시험에서 위상속도(phase volocity)를 결정하기 위해서는 위상각(phase angle)의 전개(unwrapping)가 필수적이다. 포장 구조에서처럼 깊이에 따라 강성의 차이가 현저한 경우는 기존의 위상각 전개방식으조는 정확한 위상속도를 결정하기가 용이하지 않다. 이는 기존의 위상각 전개방식은 주위상각(principal phase angle)에 2n의 정수배를 더하는 것인데, 위상각 스펙트럼(phase spectrum)에서 정수배를 결정하는 데에 어려움이 있기 때문이다. 본 연구에서는 이러한 문제점을 해결하기 위해서, 임펄스 응답 필터 기법(Impulse Response Filtration Technique), 또는 IRF기법이라고 하는 새로운 위상각 분석 기법을 제안하였다. IRF 기법의 원리는 임펄스 응답을 필터 처리함으로써 파군(wave group)을 분리하는 것인데,파군의 분리는 임펄스 응답에 대한 Gabor spectrogram을 분석한 정보를 근거로 한다. Gabor spectrogram은 전파되는 파의 에너지를 주파수-시간 공간에서 나타내는 contour 그림으로서, 파군의 전파 상황을 시각적으로 표현하는 수단이다. 이렇게 필터 처리된 임펄스 응답을 이용하면, 위상각 스펙트럼의 분석을 정확하게 할 수 있으며, 위상각의 전개에 있어서 난해함을 제거할 수 있다. 끝으로, 전쳔적인 포장 구조에 대하여 이론적으로 SASW 시험을 모사하였으며, 그 결과를 이용하여 IRF기법의 효용성을 입증하였다.

• 해양환경안전학회지
• /
• 제25권7호
• /
• pp.936-944
• /
• 2019

보이지 않는 힘으로도 불리는 잠수함은 수중에서 활동하는 은밀성을 장점으로 대함전, 대잠전 및 핵심표적 타격 등의 임무를 수행하는 전략 수중 무기 체계로 심해에서 높은 수압을 견디며 작전을 수행할 수 있어야 한다. 이러한 관점에서 잠수함 압력 선체는 잠항 깊이에 상응하는 외부 수압에 저항하는 가장 중요한 체계로서 누수, 화재, 충격 및 폭발과 같은 위험으로부터 안전성을 확보함으로써 생존성을 높임과 동시에, 작전 수행 능력을 유지할 수 있게 해주는 강도를 확보하고 있어야 한다. 이를 위해서는 잠수함 압력 선체의 구조형상 설계가 초기에 수행되는 것이 합리적이다. 특히, 함미 원추부 구조물과 압력선체 평형부 및 함미 비압력선체를 연결하는 함미 트랜지션 링의 경우, 설계된 잠수함에 따라 다양한 형상을 띄고 있다. 본 구조물 설계를 위해서는 응력 흐름과 연결성을 고려한 설계뿐만 아니라 복잡한 형상이 기인한 구조물 제작 투입 시수 증가로 인한 원가 상승 또한 검토해야 한다. 따라서, 본 연구에서는 4가지 서로 다른 형상을 갖는 함미 트랜지션 링에 대해서 비선형 유한요소해석을 통한 구조 강도 검토와 더불어 함미 트랜지션 링 형상 복잡도에 따른 작업 일수 및 자재비 검토를 통해 경제성 측면에서의 적정성 검토를 수행하였으며, 검토된 4가지 형상 중 가장 합리적인 잠수함 함미 트랜지션 링 형상을 제안하였다.

• 한국윤활학회:학술대회논문집
• /
• 한국윤활학회 2002년도 proceedings of the second asia international conference on tribology
• /
• pp.147-148
• /
• 2002

This study made use of four kinds of mating balls that were made with stainless steel but subjected to different annealing conditions in order to achieve different levels of hardness. In all load conditions, testing results demonstrated that the harder the mating materials, the lower the friction coefficient was. Conversely, the high friction coefficient found in soft martensite balls appeared to be caused by the larger contact area between the DLC film and the ball. Raman Spectra analysis showed that the transferred materials were a kind of graphite and that the contact surface of the DLC film seemed to undergo a phase transition from carbon to graphite during the high friction process.

• 한국세라믹학회지
• /
• 제36권6호
• /
• pp.604-610
• /
• 1999

Silicide layer structures and morphology degradation of the surface and interface of the silicide layers for he Co/refractory metal bilayer sputter-deposited on the P-doped polycrystalline Si substrate and subjected to rapid thermal annealing were investigated and compared with those on the single Si substrate. The CoSi-CoSi2 phase transition temperature is lower an morphology degradation of the silcide layer occurs more severely for the Co/refractorymetal bilayer on the P-doped polycrystalline Si substrate than on the single Si substrate. Also the final layer structure and the morphology of the films after silicidation annealing was found to depend strongly upon the interlayer metal. The layer structure after silicidation annealing of Co/Hf/doped-poly Si is Co-Hf alloy/polycrystalline CoSi2/poly Si substrate while that of Co/Nb is polycrystalline CoSi2/NbSi2/polycrystalline CoSi2/poly Si.

• 한국마린엔지니어링학회:학술대회논문집
• /
• 한국마린엔지니어링학회 2005년도 전기학술대회논문집
• /
• pp.331-338
• /
• 2005

The grain structure, dislocation density and second phase particles in various regions including the stir zone(SZ), thermo-mechanically affected zone(TMAZ), and heat affected zone(HAZ) of a friction stir weld 6.35mm thick aluminum 7075-T651 alloy were investigated and compared with the base metal. The microstruectures of nugget zone were compared according to tool rotation speeds and tool transition speeds. The hardness profiles of nugget zone were increased, while decreasing rotation speed and increasing welding speed. The optimal microstructure was gained at the low rotation speed 800rpm and th high welding speed 124mm/min. The nugget microstructures of fracture surface, transgranular dimple and quasicleavage type were showed different fracture type with the HAZ, shear fracture type.

• 한국윤활학회:학술대회논문집
• /
• 한국윤활학회 2003년도 학술대회지
• /
• pp.50-55
• /
• 2003

Tribological testing of DLC films was conducted using a rotating type ball on a disk friction tester in a dry chamber. This study made use of four kinds of mating balls that were made with stainless steel but subjected to diverse annealing conditions in order to achieve different levels of hardness. In all load conditions using martensite mating balls, the test results demonstrated that the friction coefficient was lower when the mating materials were harder. The high friction coefficient found in soft martensite balls appeared to be caused by the larger contact areas. The wear track on the mating balls indicated that a certain amount of material transfer occurs from the DLC film to the mating ball during the high friction process. Raman Spectra analysis showed that the transferred materials were a kind of graphite and that the contact surface of the DLC film seemed to undergo a phase transition from carbon to graphite during the high friction process.

• 천문학회지
• /
• 제29권2호
• /
• pp.83-91
• /
• 1996

We present a model that rotating primordial blackholes(PBHs) produced at the end of inflation generate the random, non-oriented primordial magnetic field. PBHs are copiously produced as the Universe completes the cosmic phase transition via bubble nucleation and tunneling processes in the extended inflation hypothesis. The PBHs produced acquire angular momentum through the mutual tidal gravitational interaction. For PBHs of mass less than 1013g, one can show that the evaporation (photon) luminosity of PBHs exceeds the Eddington limit. Thus throughout the lifetime of the rotating PBH, radiation flow from the central blackhole along the Kerr-geodesic exerts torque to ambient plasma. In the process similar to the Bierman's battery mechanism electron current reaching up to the horizon scale is induced. For PBHs of Grand Unified Theories extended inflation with the symmetry breaking temperature of $T_{GUT}\;\~\;10^{10}$ GeV, which evaporate near decoupling, we find that they generate random, non-oriented magnetic fields of $\~10^{-11}G$ on the last-scattering surface on (the present comoving) scales of $\~O(10)Mpc$.