• 대한화장품학회지
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• 제31권2호
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• pp.135-140
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• 2005

본 연구는 고형상 에멀젼의 표면에서 일어나는 물리적 특성을 레올로지를 이용해 관찰해 보았다. 고형상 에멀젼이 전단변형에 따라 고상에서 액상으로의 전이시 전단속도가 큰 고형상 에멀젼의 경우 낮은 전단변형과 높은 전단변형에서 두 번의 전이구간을 보여주는 반면에 전단속도가 작은 고형상 에멀젼의 경우 높은 전단변형에서 전이구간이 한 번만 나타내는 것을 볼 수 있었다. 이는 고형상 에멀젼의 전단변형에 따른 표면의 물리적 특성이 중요한 요소로서 고형상 에멀젼의 구성요소에 따라 변화하게 된다. 유상과 수상으로 구성되어진 고형상 에멀젼에서 수상의 함량이 증가하게 되면 표면전이(surface transition) 구간이 점점줄어들다가 사라지는 것을 볼 수 있었으며, 유상과 분체로 구성되어진 고형상 에멀젼에서는 분체의 함량이 증가함에 따라 표면전이 구간이 점점 증가하는 것을 볼 수 있었다. 그리고 유상, 수상 그리고 분체로 이루어진 고형상 에멀젼에서는 분체의 함량이 증가함에 따라 표면전이 구간이 점점 줄어들다가 사라지는 것을 볼 수 있었다.

• 한국표면공학회지
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• 제25권4호
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• pp.165-172
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• 1992

Filler, popularly used in the polymer materials, was dispersed randomly and irregularly. For the study of dispersed behavior, the specimen which have two particles in polystyrene was prepared. And the tensile strength, modulus and SEM picture were measured. When the distance between particles increased, the tensile strength and modulus increased, but particle size did not affect the values. And when the am-bient temperature increased, the tensile strength and modulus decreased, but the distance did not affect the tensile strength and modulus.

• 한국표면공학회지
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• 제50권5호
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• pp.392-397
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• 2017

The Young's modulus of a nanoscale titanium (Ti) thin-film was evaluated using a high-speed microcantilever resonating at the megahertz frequency in the present study. A 350 nm thick Ti film was deposited on the surface of a silicon microcantilever, and the morphology of the film was analyzed using the atomic force microscopy. The microcantilever was excited to resonate using an ultrasonic pulser that generates tone burst signals and the resonance frequency shift induced by the deposition of Ti was measured using a Michelson interferometer. The Young's modulus was determined through a modal analysis using the finite element method and the result was validated by the nanoindentation testing, showing good agreement within a relative error of 1.0%. The present study proposes a nanomechanical characterization technique with enhanced accuracy and sensitivity.

• 열처리공학회지
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• 제32권3호
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• pp.113-117
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• 2019

The effects of severe plastic deformation and heat treatment on the mechanical properties of Al 5052 and 6005 alloys were investigated using the metallurgical technique and nano-indentation technique in nano-surface region. Equal channel angular pressing (ECAP) was used to apply severe plastic deformation to the aluminum alloys in order to obtain fine grain sized materials. The elastic modulus was measured and interpreted in relation to the metallurgical observation. The elastic modulus increased after ECAP process due to evolution of the fine grains. However, the elastic modulus decreased after heat treatment due to generation of coarsened precipitates on the grain boundaries.

• 대한토목학회논문집
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• 제35권1호
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• pp.229-236
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• 2015

본 연구는 에폭시 아스팔트 포장 내부 상태 평가를 위해 이동 차량하중 모사가 가능한 회복탄성계수 실험과 LWD 실험을 수행하였다. 회복탄성계수 실험에서 측정된 변위는 일반 아스팔트와 달리 잔류변형이 매우 미소한 수준으로 탄성변형과 유사한 거동을 보여 정상 상태로 해석해도 무리가 없는 것으로 나타났다. 회복탄성계수에서 측정된 변위 결과를 처짐 탄성계수로 변환 후 1 SIGMA 단계를 적용하여 정상 처짐 탄성계수 범위를 산정하였다. $60^{\circ}C$에서의 파손 의심 처짐 범위와 하중-변위 선도 개형으로 포장 내부 상태를 예측하였다. 정상 표면처짐 구간인 $140{\mu}m$의 일부 구간에서 수분 침투 및 접착성능 저하가 관찰되었으나, 하중-변위 선도 개형에서 변곡점 발생 구간으로 확인되었다. 현장 확인 결과 제시된 기준은 높은 수준의 정확도를 보이는 것으로 나타났다.

• 한국기계가공학회지
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• 제16권2호
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• pp.102-107
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• 2017

This study focuses on the effect of the elasticity modulus of jig material on blade edge shape in the grinding process of a sapphire medical knife. The ELID grinding process was applied as the edge-grinding method for sapphire material. Carbon steel and copper have been selected as the hard and soft jig materials, respectively. The blade edge created by ELID grinding was measured by a surface roughness tester and optical microscope. The shape of the ground edge and surface roughness were compared using the measurement results. As a result, it was found that chipping in the blade edge of the sapphire knife occurred more than in the case of jig material with a high-elasticity modulus because of the high normal force in the grinding process. Moreover, the maximum height surface roughness, $R_{max}$,of the ground surface was higher in the case of the jig material with a high-elasticity modulus due to the difference in elasticelongation. It was considered to lead to chipping from the notch effect.

• Smart Structures and Systems
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• 제20권4호
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• pp.473-481
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• 2017

This study suggests a simple, convenient and non-destructive method for investigation of the Young's modulus detection in stepped shafts which only utilizes the first-order resonant frequency in flexural mode and dimensions of structures. The method is based on the impulse excitation technique (IET) to pick up the fundamental resonant frequencies. The standard Young's modulus detection formulas for rectangular and circular cross-sections are well investigated in literatures. However, the Young's modulus of stepped shafts can not be directly detected using the formula for a beam with rectangular or circular cross-section. A response surface method (RSM) is introduced to design numerical simulation experiments to build up experimental formula to detect Young's modulus of stepped shafts. The numerical simulation performed by finite element method (FEM) to obtain enough simulation data for RSM analysis. After analysis and calculation, the relationship of flexural resonant frequencies, dimensions of stepped shafts and Young's modulus is obtained. Numerical simulations and experimental investigations show that the IET method can be used to investigate Young's modulus in stepped shafts, and the FEM simulation and RSM based IET formula proposed in this paper is applicable to calculate the Young's modulus in stepped shaft. The method can be further developed to detect mechanical parameters of more complicated structures using the combination of FEM simulation and RSM.

• 한국재료학회지
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• 제13권9호
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• pp.606-612
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• 2003

Surface and mechanical properties of thin films with submicron thickness was characterized by nanoindentation with Berkovich and Vickers tips, and scanning probe microscopy. Nanoindention was made in a depth range of 15 to 200 nm from the surface by applying tiny force in a range from 150 to $9,000 \mu$N. Stiffness, contact area, hardness, and elastic modulus were determined from the force-displacement curve obtained. Reliability was first tested by using fused quartz, a standard sample. Elastic modulus and hardness values of fused quartz measured were the same as those reported in the literature within two percent of error. Mechanical properties of ITO thin film were characterized in a depth range of 15∼200nm. As indentation depth increased, elastic modulus and hardness decreased by substrate effect. Ion beam deposited DLC thin films were indented in a depth range of 40∼50 nm. The results showed that the DLC thin film using benzene and bias voltage 0∼-50 V has elastic modulus and hardness value of 132 and 18 GPa respectively. Pure DLC thin films showed roughnesses lower than 0.25 nm, but silicon-added DLC thin films showed much higher roughness values, and the wavy surface morphology.

• 한국표면공학회지
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• 제43권6호
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• pp.260-265
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• 2010

STD 61 steel has been widely used for tools, metallic mold and die for press working because of its favorable mechanical properties such as high toughness, and creep strength as well as excellent oxidation resistance. The STD 61 tool steel coated with TiN and ZrN by sputtering results in improvement of wear and corrosion resistance. In this study, surface characteristics of TiN and ZrN film coated STD 61 by sputtering were studied by using FE-SEM, EDS, XRD, and XRR and nanoindentation tests. From the results of surface characteristics of coated specimen, the ZrN coated surface showed finer granular than that of TiN coated surface. The coated layer structures of ZrN and TiN were grown to (111) and (200) preferred orientation. From the results of XRR test for surface roughness, density and growth rate of coating film, surface roughness and growth rate of ZrN coated film revealed lower values those of TiN coated film, whereas density of ZrN coated film showed higher values than that of TiN coated film. From the nanohardness and elastic modulus test, nanohardness value and elastic modulus of ZrN coated film became higher than those of TiN coated film.

• 동력기계공학회지
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• 제12권3호
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• pp.55-59
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• 2008

In this paper, we have investigated on collection efficiency of fine particle of glass fiber-filter bag according to the surface treatment. The solution consisted of polytetrafluoroethylene(teflon), graphite powder, silicon resin and water was used as a basic surface treatment agent. Tensile strength of glass filter-bag increased with up to 3hrs and then decreased with surface treatment time. Tensile strength and initial modulus of the glass fiber-filter bag treated by iodine after basic surface treatment for 3hrs were lower than those of basic surface treatment for 3hrs, however collection efficiency and fracture strain were higher than those of basic surface treatment for 3hrs. Glass fiber-filter bag with lower initial modulus and more strain will be extend the durable period and the one treated by iodine after basic surface treatment 3or 3hrs is expected high collection efficiency of fine particle. This method makes it possible to manufacture glass fiber-filter bag of the optimum condition.