• 제목/요약/키워드: surface inhomogeneity

검색결과 72건 처리시간 0.033초

Fourier Transform Infrared Spectrophotometric Direct on Filter 방법을 이용한 석영 분석의 기초 연구 - 필터재질, 비균일 침착 및 습도의 영향 - (The Preliminary Study on the Quantitative Analysis of Quarts by Fourier Transform Infrared Spectrophotometric Direct on Filter(FTIR-DOF) Method -Effects of filter materials, inhomogeneity of deposition, and humidity-)

  • 피영규;김현욱
    • 한국산업보건학회지
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    • 제15권1호
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    • pp.1-7
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    • 2005
  • Although the Fourier Transform Infra-Red spectrophotometric Direct on Filter(FTIR-DOF) method is a useful analytical technique for quantifying quartz content in respirable dust samples, a number of analytical problems must be taken into consideration such as, to name only a few, inhomogeneous deposition of particles, level of environmental humidity, uneven surface of the filter, and interfering minerals in the sample. This study was designed to select the most suitable wavelength and proper filter material for the method, and to investigate effects of humidity and inhomogeneous deposition of particles on the filter. Samples of respirable dust, created in a dust chamber containing standard material of quartz, were collected using a cyclone equipped with a 25mm filter as a collection medium. The results were as follows; 1. Among seven (7) commercially available filters tested for the FTIR-DOF method, the DM 800 filter showed the best analytical performance having the lowest background absorbance bands and no overlapping peaks at 799, 779, and $695cm^{-1}$. 2. The variations of absorbance due to humidity ranged from 1.0% to 3.3% for $799cm^{-1}$, 1.0% to 3.3% for $779cm^{-1}$, and 8.9%~20.9% for $695cm^{-1}$ peaks, respectively. The $699cm^{-1}$ peak was proved to be most vulnerble to environmental humidity for quantitative analysis of quartz. 3. As for effects of inhomogeneous deposition of samples, the highest variation of absorbance of 10.9% ($13.5{\mu}g$) was observed when using the 695cm-1. The variations of absorbance from the other two peaks, 799 and $779cm^{-1}$, ranged from 1.2 to 3.2%, and 1.4 to 4.1%, respectively. Therefore, the $799cm^{-1}$ peak was considered to be most reliable for quantitative analysis of quartz. The results of this study suggest that, for quantitative analysis of quartz in the respirable dust samples, use of the $799cm^{-1}$ peak can minimize the influence of environmental humidity and inhomogeneous deposition of particles on the filter. The FTIR-DOF method, if adopted for routine analysis of quartz in the respirable dust samples, could save sample preparation time and efforts substantially and also could increase analytical throughputs. Since use of the $799cm^{-1}$ peak is prone to be affected by interferences in the sample, further research on minimizing the effects is needed.

안경 렌즈의 국소적 투과율 균일도 비교 연구 (A Comparative Study on the Local Transmittance Homogeneity of the Ocular Lens)

  • 박상국;이형철;장윤석;성덕용;강성수
    • 한국안광학회지
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    • 제20권4호
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    • pp.471-476
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    • 2015
  • 목적: 다양한 안경렌즈의 투과율 분포를 국소 투과율 현미경을 이용하여 분석함으로써 렌즈의 광학적 균일성을 연구하고자 한다. 방법: 안경렌즈 표면에 집광된 레이저의 국소적 투과율을 광검출기, 락인앰프 그리고 전동이송장치로 측정하였다. 5종 25장의 멀티코팅된 무착색렌즈와 9종 45장의 멀티코팅된 착색렌즈가 시료로서 분석되었다. 결과: 굴절률과 코팅 종류에 따른 무착색렌즈의 투과율과 렌즈별 투과율 편차는 거의 균일하게 측정되었다. 하지만 착색렌즈의 경우 렌즈별 투과율 편차가 무착색렌즈에 비해 약 3.7배 크게 측정되었다. 또한 렌즈의 국소적 투과율 불균일도도 무착색렌즈에 비해 착색렌즈가 평균 약 3.1배 큰 것으로 분석되었다. 결론: 무착색렌즈에 비해 착색렌즈가 렌즈별 투과율의 편차와 투과율 불균일도가 모두 큰 것을 국소 투과율 현미경을 이용하여 분석할 수 있었다. 국소 투과율 현미경을 통한 이러한 분석은 렌즈의 성능 평가와 광학적 균일성 향상에 적용될 수 있다.

Intra-Rater and Inter-Rater Reliability of Brain Surface Intensity Model (BSIM)-Based Cortical Thickness Analysis Using 3T MRI

  • Jeon, Ji Young;Moon, Won-Jin;Moon, Yeon-Sil;Han, Seol-Heui
    • Investigative Magnetic Resonance Imaging
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    • 제19권3호
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    • pp.168-177
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    • 2015
  • Purpose: Brain surface intensity model (BSIM)-based cortical thickness analysis does not require complicated 3D segmentation of brain gray/white matters. Instead, this technique uses the local intensity profile to compute cortical thickness. The aim of the present study was to evaluate intra-rater and inter-rater reliability of BSIM-based cortical thickness analysis using images from elderly participants. Materials and Methods: Fifteen healthy elderly participants (ages, 55-84 years) were included in this study. High-resolution 3D T1-spoiled gradient recalled-echo (SPGR) images were obtained using 3T MRI. BSIM-based processing steps included an inhomogeneity correction, intensity normalization, skull stripping, atlas registration, extraction of intensity profiles, and calculation of cortical thickness. Processing steps were automatic, with the exception of semiautomatic skull stripping. Individual cortical thicknesses were compared to a database indicating mean cortical thickness of healthy adults, in order to produce Z-score thinning maps. Intra-class correlation coefficients (ICCs) were calculated in order to evaluate inter-rater and intra-rater reliabilities. Results: ICCs for intra-rater reliability were excellent, ranging from 0.751-0.940 in brain regions except the right occipital, left anterior cingulate, and left and right cerebellum (ICCs = 0.65-0.741). Although ICCs for inter-rater reliability were fair to excellent in most regions, poor inter-rater correlations were observed for the cingulate and occipital regions. Processing time, including manual skull stripping, was $17.07{\pm}3.43min$. Z-score maps for all participants indicated that cortical thicknesses were not significantly different from those in the comparison databases of healthy adults. Conclusion: BSIM-based cortical thickness measurements provide acceptable intra-rater and inter-rater reliability. We therefore suggest BSIM-based cortical thickness analysis as an adjunct clinical tool to detect cortical atrophy.

Clinical Implementation of 3D Printing in the Construction of Patient Specific Bolus for Photon Beam Radiotherapy for Mycosis Fungoides

  • Kim, Sung-woo;Kwak, Jungwon;Cho, Byungchul;Song, Si Yeol;Lee, Sang-wook;Jeong, Chiyoung
    • 한국의학물리학회지:의학물리
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    • 제28권1호
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    • pp.33-38
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    • 2017
  • Creating individualized build-up material for superficial photon beam radiation therapy at irregular surface is complex with rice or commonly used flat shape bolus. In this study, we implemented a workflow using 3D printed patient specific bolus and describe our clinical experience. To provide better fitted build-up to irregular surface, the 3D printing technique was used. The PolyLactic Acid (PLA) which processed with nontoxic plant component was used for 3D printer filament material for clinical usage. The 3D printed bolus was designed using virtual bolus structure delineated on patient CT images. Dose distributions were generated from treatment plan for bolus assigned uniform relative electron density and bolus using relative electron density from CT image and compared to evaluate the inhomogeneity effect of bolus material. Pretreatment QA is performed to verify the relative electron density applied to bolus structure by gamma analysis. As an in-vivo dosimetry, Optically Stimulated Luminescent Dosimeters (OSLD) are used to measure the skin dose. The plan comparison result shows that discrepancies between the virtual bolus plan and printed bolus plan are negligible. (0.3% maximum dose difference and 0.2% mean dose difference). The dose distribution is evaluated with gamma method (2%, 2 mm) at the center of GTV and the passing rate was 99.6%. The OSLD measurement shows 0.3% to 2.1% higher than expected dose at patient treatment lesion. In this study, we treated Mycosis fungoides patient with patient specific bolus using 3D printing technique. The accuracy of treatment plan was verified by pretreatment QA and in-vivo dosimetry. The QA results and 4 month follow up result shows the radiation treatment using 3D printing bolus is feasible to treat irregular patient skin.

EBSD측정에 의한 반복겹침접합압연된 무산소동의 두께방향으로의 미세조직 변화 분석 (Microstructural Evolution Analysis in Thickness Direction of An Oxygen Free Copper Processed by Accumulative Roll-Bonding Using EBSD Measurement)

  • 이성희;임차용
    • 한국재료학회지
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    • 제24권11호
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    • pp.585-590
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    • 2014
  • Microstructural evolution in the thickness direction of an oxygen free copper processed by accumulative rollbonding (ARB) is investigated by electron back scatter diffraction (EBSD) measurement. For the ARB, two copper alloy sheets 1 mm thick, 30 mm wide and 300 mm long are first degreased and wire-brushed for sound bonding. The sheets are then stacked and roll-bonded by about 50% reduction rolling without lubrication at an ambient temperature. The bonded sheet is then cut to the two pieces of the same dimensions and the same procedure was repeated on the sheets up to eight cycles. The specimen after 1 cycle showed inhomogeneous microstructure in the thickness direction so that the grains near the surface were finer than those near the center. This inhomogeneity decreased with an increasing number of ARB cycles, and the grain sizes of the specimens after 3 cycles were almost identical. In addition, the aspect ratio of the grains decreased with an increasing number of ARB cycles due to the subdivision of the grains by shear deformation. The fraction of grains with high angle grain boundaries also increased with continuing process of the ARB so that it was higher than that of the low angle grain boundaries in specimens after 3 cycles. A discontinuous dynamic recrystallization occurred partially in specimens after 5 cycles.

원료분체 $Nb_20_5$의 응집상태가 $Pb(MG_{1/3}Nb_{2/3})O_3$소결, 유전특성에 미치는 영향 (Effect of Agglomeration of $Nb_20_5$ on Formation Reaction, Sintering and Dielectric Properties in$Pb(MG_{1/3}Nb_{2/3})O_3$)

  • 조영국;김진호;박병옥;조상희
    • 한국결정성장학회지
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    • 제2권1호
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    • pp.51-59
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    • 1992
  • 일차입경이 동일한 $Nb_20_5$분체의 응집 상태가 $Pb(Mg_{1/3}Nb_{2/3})O_3$의 생성 반응 및 소결에 미치는 영향을 조사하였다. 합성 방법으로는 고체 반응법과 용융염법으로 나누어 각각 실험하였다. 고체 반응법의 경우에는 perovskite 상의 생성 반응이 $Nb_20_5$의 응집도가 낮을수록 크게 영향을 받았으나, 용융법시에는 거의 영향을 받지 않았다. 그 이유는 고상 반응법시에는 perovskite 상의 생성이 중간생성물인 perovskite 상의 분포의 균일성, 즉 $Nb_20_5$의 응집도에 지배를 받게되나, 용해, 석출 과정에 의해 진행되는 용융염법에서는 반응물의 비표면적에 의존하므로, 응집도에는 그다지 영향을 받지않는 것으로 사료된다.

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희박 예혼합 가스터빈 연소기 3 차원 전산 해석 및 화학반응기 네트워크에 의한 NOx 예측 (3D RANS Simulation and the Prediction by CRN Regarding NOx in a Lean Premixed Combustion in a Gas Turbine Combustor)

  • 이재복;정대로;허강열;진재민;박정규;이민철
    • 대한기계학회논문집B
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    • 제35권12호
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    • pp.1257-1264
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    • 2011
  • 희박예혼합 가스터빈 연소기에 대한 3 차원 RANS 해석을 수행하였으며 PCFM(Partially Premixed Coherent Flame Model) 화염면적밀도 생성항 상수의 보정을 통하여 희박연소조건을 모사하였다. PCFM 에서 계산된 화염면적밀도에 의해 층류 예혼합 화염의 전파를 예측하고 불균일하게 분포한 기연 가스의 물성을 평형 가정에 따라 예측하였다. 복사와 대류 열전달을 모사하기 위해 냉각 조건으로서 실험과의 비교를 통해 결정된 열유속을 적용하였다. 이러한 3 차원 해석 결과를 바탕으로 파일럿 노즐과 메인 노즐에 분배되는 연료량 비에 대한 민감도 조사를 수행하였으며 CRN(Chemical Reactor Network)을 구성하여 NOx 배출량을 예측하고 측정값과 비교 분석하였다.

1975년에 발생한 중국 해성지진이 한반도에 미친 영향 (Effects of the 1975 Haicheng Earthquake on the Korean Peninsula)

  • 추교승
    • 한국지진공학회:학술대회논문집
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    • 한국지진공학회 1998년도 추계 학술발표회 논문집 Proceedings of EESK Conference-Spring 1998
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    • pp.210-221
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    • 1998
  • In the period from the year 1500 to 1980. at least 14 large earthquake with epicenters in the northeastern China and Yellow Sea were felt or destructive in the Korean Peninsula. The most sigmificant events among them were the 1668 July 25 Tancheng earthquake of mamnitude 8.5, and the 1975 Feb. 4 Haicheng earthquake of magnitude 7.3. The Haicheng earthquake of the year 1975 in am extraordinary one among those occurred in the northeastern China in the 20th century in the sense the Shake of the event affected all over the Korean Peninsula. The tremor was felt even at the southeastern tip of the Korea and northern part of Kyushu 700km far away from the epicenter. In order to see the variation and trend of the effect of the Haicheng earthquake on the Korean Peninsula, the two data sets of the northern and southern parts of the peninsula were merged into one combined data set. The spatial variation of intensity shows smooth decrease from the value 4 of the northwestern region near the source to the value 1 of the Cheju Island and Kjushu. However, there are four regions of locally high intensity value. They are the region along downstream of Abrok(Yalu) River with intensity 5, the region around Shinpo of intensity 4, the area comprising Seoul and Chuncheon Cities of intensity 4, and Pohang-Pusan area of intensity 3. We suppose that there might be three types of possible mechanisms. The first one is concerned with the lateral inhomogeneity of velocity in the crust caused by wide distribution of relatively fractured rock. The second one is related with reflections of surface waves caused by the crestal thinning effect at border regions of the Peninsular in contact with the Ulleung Basin and the Japan Basin. The third possibility is local site effect caused by thick Tertiary or Quaternary rocks and soil layers.

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ECAP 가공에 의해 제조된 초미세립 OFHC Cu 봉재의 미세조직 및 기계적 특성의 균질성 (Homogeneity of Microstructure and Mechanical Properties of Ultrafine Grained OFHC Cu Bars Processed by ECAP)

  • 지정훈;박이주;김형원;황시우;이종수;박경태
    • 대한금속재료학회지
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    • 제49권6호
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    • pp.474-487
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    • 2011
  • Bars of OFHC Cu with the diameter of 45 mm were processed by equal channel angular pressing up to 16 passes via route $B_c$, and homogeneity of their microstructures and mechanical properties was examined at every four passes which develop the equiaxed ultrafine grains. In general, overall hardness, yield strength and tensile strength increased by 3, 7, and 2 times respectively compared with those of unECAPed sample. Cross-sectional hardness exhibited a concentric distribution. Hardness was the highest at the center of bar and it decreased gradually from center to surface. After 16 passes, overall hardness decreased due to recovery and partial recrystallization. Regardless of the number of passage, yield strength and tensile strength were quite uniform at all positions, but elongation showed some degree of scattering. At 4 passes, coarse and ultrafine grains coexisted at all positions. After 4 passes, uniform equiaxed ultrafine grains were obtained at the center, while uniform elongated ultrafine grains were manifested at the upper half position. At the lower half position, grains were equiaxed but its size were inhomogeneous. It was found that inhomogeneity of grain morphology and grain size distribution at different positions are to be attributed to scattering in elongation but they did not affect strength. The present results reveal the high potential of practical application of equal channel angular pressing on fabrication of large-sized ultrafine grained bars with quite homogeneous mechanical properties.

연약 점성토 지반에 시공되는 원형 수직구의 히빙 안정성에 대한 수치해석적 연구 (Numerical study on basal heave stability of a circular vertical shaft constructed in clay)

  • 강석준;조계춘
    • 한국터널지하공간학회 논문집
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    • 제24권3호
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    • pp.231-245
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    • 2022
  • 지반강도가 낮은 연약 점성토 지반을 대상으로 수직구가 시공되는 경우, 굴착면에서의 토압 불균형에 대한 지반의 지지력이 낮아 굴착면이 융기하는 히빙이 발생할 위험이 존재한다. 히빙에 대한 안정성을 평가하기 위해 안전율을 계산하는 방법들이 제안되어왔으나, 이론적인 유도 과정에서 많은 가정사항들이 포함되어 정확한 히빙 안정성 평가가 어렵다는 한계를 가진다. 본 연구에서는 선행 연구를 보완하기 위해 원형 수직구가 연약 점성토 지반에 시공되는 경우를 상정하여 굴착 형상에 따른 지반 지지력의 변화, 지반 점성토의 비균질성, 그리고 관내토의 효과에 대한 이론적 접근을 통해 기존 안전율 제안식을 보완하였다. 보완된 식의 검증과 다양한 사례 연구를 통한 히빙 안정성 검토를 위해 원형 수직구 굴착 시 발생하는 굴착면의 히빙을 3차원 수치해석으로 모사하여 안전율을 도출하였다. 수치해석 및 히빙 안전율 제안식들을 이용하여 다양한 인자의 변화에 따른 히빙 안전율의 변화를 검토한 결과, 본 연구에서 추가적으로 보완된 특성이 3차원 안전율 식 내에 적절하게 반영되었음을 확인하였다. 다양한 사례를 모사하여 수행된 수치해석 결과를 이용하여 수식을 구성하는 인자들이 히빙 안전율에 미치는 영향을 도출하였으며, 깊이에 따른 비배수 전단강도 증가의 고려 여부가 안전율 값 산정에 지배적인 영향을 미치는 것을 확인하였다.