• Title/Summary/Keyword: surface impregnation

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Effect of Impregnation Ratio and Carbonizing Temperature on Surface Temperature of Woodceramics Made from Thinned Logs of Pinus densiflora S. et. Z. (함침율 및 소성온도가 소나무 간벌재로 제조된 우드세라믹의 표면온도에 미치는 영향)

  • Oh, Seung-Won;Byeon, Hee-Seop
    • Journal of the Korean Wood Science and Technology
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    • v.32 no.4
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    • pp.1-7
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    • 2004
  • The change in surface temperature of woodceramics, made from thinned logs of Pinus densiflora, were investigated, by the impregnation ratio and carbonizing temperature. As the surface temperature of silicon rubber heater was going up, that of woodceramics also increase rapidly. In case of heaters surface temperature at 70℃, the surface temperature of woodceramics was 53.9℃ when a sample was the impregnation ratio of 80%, while it was 54.2℃ when a sample was at 1,000℃ in carbonizing temperature, showing the highest. Also, it was found that woodceramics maintained heat for a long time because the descending velocity of their surface temperature was lower than that of the heater.

Pd-doped $SnO_2$-based oxide semiconductor thick-film gas sensors prepared by three different catalyst-addition processes

  • Lee, Kyu-Chung;Hur, Chang-Wu
    • Journal of information and communication convergence engineering
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    • v.7 no.1
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    • pp.72-77
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    • 2009
  • Three different procedures for adding Pd compounds to $SnO_2$ particles have been investigated. These processes are: (1) coprecipitation; (2) dried powder impregnation; and (3) calcined powder impregnation. The microstructures of $SnO_2$ particles have been analyzed by X-ray diffraction (XRD), Brunauer-Emmett-Teller (BET), scanning electron microscope (SEM) and X-ray photoelectron spectroscopy (XPS). In the coprecipitaion method, the process does not restrain the growth of $SnO_2$ particles and it forms huge agglomerates. In the dried powder impregnation method, the process restrains the growth of $SnO_2$ particles and the surfaces of the agglomerates have many minute pores. In the calcined powder impregnation method, the process restrains the growth of $SnO_2$ particles further and the agglomerates have a lot more minute pores. The sensitivity ($S=R_{air}/R_{gas}$) of the $SnO_2$ gas sensor made by the calcined powder impregnation process shows the highest value (S = 21.5 at 5350 ppm of $C_3H_8$) and the sensor also indicates the lowest operating temperature of around $410^{\circ}C$. It is believed that the best result is caused by the plenty of minute pores at the surface of the microstructure and by the catalyst Pd that is dispersed at the surface rather than the inside of the agglomerate. Schematic models of Pd distribution in and on the three different $SnO_2$ particles are presented.

A Change in Surface Temperature of Ceramics Made from Board Mixed with Sawdust and Rice Husk - Effect of Resin Impregnation Rate and Carbonization Temperature - (톱밥과 왕겨 혼합보드로 제조된 세라믹의 표면 온도 변화 - 수지함침율 및 탄화온도의 영향 -)

  • Oh, Seung-Won;Park, Hee-Jun
    • Journal of the Korean Wood Science and Technology
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    • v.38 no.1
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    • pp.43-48
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    • 2010
  • This study was aimed at offering basic data to develop a new use of sawdust and rice husk. The results of this study were as follows: In surface temperature of ceramics by resin impregnation rate, the velocity was great in the early time of heat transfer because the temperature precipitously increased to 10 minutes elapsed. Also, the surface temperature of ceramics manufactured in resin impregnation rate of 60~70% indicated the highest. Heat transfer was fast in terms of the changes in surface temperature of ceramics according to the carbonization temperature, as because the density of ceramics made on condition of the carbonization temperature of $1000^{\circ}C$and $1200^{\circ}C$ was high. Moreover, ceramics maintained heat for a long time because the descent velocity of surface temperature of ceramics was slower than that of heater.

Change of Surface Temperature in Woodceramics Made from MDF(II) - Effect of Impregnation Rate and Burning Temperature - (MDF로 제조된 우드세라믹의 표면온도 변화(II) - 수지 함침율과 소성온도의 영향 -)

  • Oh, Seung Won;Byeon, Hee Seop
    • Journal of the Korean Wood Science and Technology
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    • v.31 no.1
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    • pp.41-45
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    • 2003
  • In this study, woodceramics were made from MDF with various resin impregnation rate. To investigate the change of surface temperature of woodceramics, the impregnated MDF was burned at the temp. 600, 800, 1,000, 1,200℃. Surface temperature of woodceramics was increased as impregnation rate and burning temperature was increased. The specimen burned at 800℃ was lower than others. Change of temperature under given temperature increased as time passed and it showed more increased in temperature at burning temperature of 1,200℃. Change of surface temperature increased when floor temperature increased and the temperature was 49.2℃ at 70℃ in floor temperature of 1,200℃ specimen. The decent in surface temperature of woodceramics was the fastest decrease at the burning temperature of 800℃ specimen.

Study on effect of chemical impregnation on the surface and porous characteristics of activated carbon fabric prepared from viscose rayon

  • Bhati, Surendra;Mahur, J.S.;Dixit, Savita;Chobey, O.N.
    • Carbon letters
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    • v.15 no.1
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    • pp.45-49
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    • 2014
  • In this study, synthetic viscose rayon fabric has been used for preparing activated carbon fabric (ACF), impregnated with different concentrations of $H_3PO_4$. The effect of $H_3PO_4$ impregnation on the weight yield, surface area, pore volume, chemical composition and morphology of ACF were studied. Experimental results revealed that both Brunauer-Emmett-Teller surface area and micropore volume increased with increasing $H_3PO_4$ concentration; however, the weight yield and microporosity (%) decreased. It was observed that samples impregnated at $70^{\circ}C$ (AC-70) give higher yield and higher microporosity as compared to $30^{\circ}C$ (AC-30). The average pore size of the ACF also gradually increases from 18.2 to 19 and 16.7 to $20.4{\AA}$ for $30^{\circ}C$ and $70^{\circ}C$, respectively. The pore size distribution of ACF was also studied. It is also concluded that the final ACF strength is dependent on the concentration of impregnant.

Characterization of CNT/TiO2 Electrode Prepared Through Impregnation with TNB and Their Photoelectrocatalytic Properties

  • Zhang, Feng-Jun;Chen, Ming-Liang;Oh, Won-Chun
    • Environmental Engineering Research
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    • v.14 no.1
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    • pp.32-40
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    • 2009
  • In this study, we have prepared three kinds of carbon nanometer tube $CNT/TiO_{2}$ electrodes through impregnation with different concentration titanium n-butoxide (TNB) solution. The prepared electrodes were characterized with surface properties, structural crystallinity, elemental identification and photoelectrocatalytic activity. The $N_2$ adsorption data showed that the composites had decreased surface area compared with the pristine CNT. This indicated the blocking of micropores on the surface of CNT, which was further supported by observation via SEM. XRD results showed patterns for the composites and a typical single and clear anatase crystal structure. The main elements such as C, O and Ti were existed for all samples from the EDX data. The catalytic efficiency of the developed electrode was evaluated by the photoelectrodegradation of methylene blue (MB). The positive potential applied in photoelectrocatalytic (PEC) oxidation was studied. It was found that photoelectrocatalytic (PEC) decomposition of MB solution could be attributed to combination effects between $TiO_2$ photocatalytic and CNT electro-assisted. Through the comparison between photocatalytic (PC) oxidation and photoelectrocatalytic (PEC) oxidation, it was found that the PEC oxidation efficiency for MB is higher than that of PC oxidation.

A Study on Characteristics of Concrete Impregnated with the Inorganic Surface Penetration Agents (무기계 표면침투제 용액으로 함침한 콘크리트의 특성 연구)

  • Bae, Ju-Seong;Kim, Hyeok-Jung;Park, Gook-Jun;Han, Jong-Won
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.14 no.1
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    • pp.71-77
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    • 2010
  • The concrete structure's durability and integrity is reduced owing to various deterioration phenomena. Therefore, it is important to prevent the deterioration phenomena. This study inquired into the various experimental results of specimens with different dilution concentration and impregnation time by the each solution to present the economic and efficient using method of the inorganic surface penetration agents. As a results, the reasonable dilution concentration and impregnation time of colloidal silica solutions are 15% and 5 minute and for the sodium alumina silicate solutions are 17% and 10 second.

A Study on the Evaluation of Carbonation Resistance of Fire Damaged Fiber-Reinforced High Strength Concrete with the Type of Surface Repair Materials (섬유혼입 고강도 콘크리트의 화재 후 표면보수재료의 종류에 따른 중성화 저항성 비교·평가에 관한 연구)

  • Sim, Sang-Rak;Ryu, Dong-Woo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2020.06a
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    • pp.81-82
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    • 2020
  • In this study, after applying a silicate-based impregnation and polymer-based coating to fire damaged high strength concrete, carbonation resistance was evaluated to compare and evaluate the carbonation depth according to the type of surface repair materials. As a result of the experiment, it was confirmed that the carbonation resistance was increased in the case of the concrete with the surface repair materials compared to the control specimen without the surface repair materials. In particular, in the case of the polymer-based coating agent, it was confirmed that the carbonation hardly progressed.

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Comparison of Resin Impregnation and Mechanical Properties of Composites Based on Fiber Plasma Treatment (섬유 플라즈마 처리에 따른 복합재료의 수지 함침성 및 기계적 특성 비교)

  • Seong Baek Yang;Donghyeon Lee;Yongseok Lee;Dong-Jun Kwon
    • Composites Research
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    • v.36 no.6
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    • pp.388-394
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    • 2023
  • In composites manufacturing, increasing resin impregnation is a key way to speed up the manufacturing process and improve product quality. While resin improvement is important, simple fiber surface treatments can also improve resin flowability. In this study, different plasma treatment times were applied to carbon fiber fabrics to improve the impregnation between resin and fiber. Electrical resistivity measurements were used to evaluate the dispersion of resin in the fibers, which changed with plasma treatment. The effect of fiber surface treatment on resin spreadability could be observed in real time. When inserting a carbon fiber tow into the resin, the amount of resin that soaked into the tow was measured to objectively compare resin impregnation. Five minutes of plasma treatment improved the tensile and compressive strength of the composite by more than 50%, while reducing the void content and increasing the fire point impregnation flow rate. Finally, a dynamic flexural fatigue test was conducted using a portion of the composite used as an architectural composite part, and the composite part did not fail after one million cycles of a 3 kN load.

Preparation and Properties of Disc Type CuO Catalyst Impregnated Ceramic Filters (디스크형 산화구리 촉매담지 세라믹필터의 제조와 물성)

  • Hong Min-Sun;Moon Su-Ho;Lee Jae-Chun;Lee Dong-Sub;Lim Woo Taik
    • Journal of Korean Society for Atmospheric Environment
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    • v.20 no.2
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    • pp.185-193
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    • 2004
  • A catalyst with CuO ceramic filter for simultaneous treatment of dust and HAP was prepared and characterized. Catalytic ceramic filter can not only potentially achieve the substantial savings in energy but provide with effective optimization and integration of process for simultaneous removal of SO$_2$, NO$_{x}$ and particulates from flue gases. Catalytic ceramic filters remove simultaneously particulates on exterior surface of filters and reduce NO to $N_2$ and $H_2O$ by SCR (Selective Catalytic Reduction) process. Preparation of catalyst impregnated ceramic filter with disk shape (Ψ 50) follow the processing of alumino-silicate ceramic filter, support impregnation and catalyst impregnation (copper oxide). Preparation routes of alumino-silicate catalyst carrier suitable for production of catalytic filters practically were studied and developed using the sol-gel and colloidal processing, homogeneous precipitation and impregnation method. Characterization of the catalyst, catalyst carrier catalytic filter materials have been performed the using various techniques such as BET, XRD, TGA, SEM. Combination of the sol-gel and colloidal processing and impregnation method is recommended to prepare catalyst carriers economically for catalytic filter applications.s.