• The Journal of Korean Academy of Prosthodontics
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• v.40 no.2
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• pp.201-212
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• 2002

This study investigated the shear bond strengths between abrasion-resistant denture teeth and composite resins according to surface treatments. Denture teeth for this study were Trubyte IPN teeth(Dentsply Inc., USA) with interpenetrating polymer network and Endura Posterio (Shofu Inc. Japan) of composite resin teeth, and restorative composite resins were Clearfil FII (Kuraray, Japan) of the self-cured composite resin and Z100(3M Dental Product, USA) of the light-cured composite resin. Five different surface treatments were evaluated: (1) $50{\mu}m\;A1_2O_3$ sandblasting: (2) #100 carbide paper; (3) chloroform; (4) retentive holes; and (5) no treatment. After surface treatments, denture teeth were examined by scanning electron microscopy(SEM), and the maximum shear bond strengths between abrasion-resistant denture teeth and composite resins were measured using Instron. The results were as follows; 1. IPN teeth treated with sandblasting had the highest shear bond strength, and Endura treated with sandblasting and carbide paper had significantly greater shear bond strength than with any other surface treatment. 2. Regardless or composite resins, the shear bond strength on Endura was greater than on IPN teeth. 3. Regardless of denture teeth, the shear bond strength of Clearfil FII was greater han of Z100. 4. In appearance of SEM, IPN teeth treated with sandblasting showed generalized roughness on the all of surface, however, carbide paper treatment resulted in partly rough. Endura treated with sandblasting and carbide paper showed similar surface characteristics. Wetting denture teeth surface with chloroform removed the debris and created a particle-free and smooth surface.

• Journal of Korean Academy of Dental Administration
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• v.11 no.1
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• pp.38-46
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• 2023

Composite resins, commonly used in clinical practice, have been developed to improve aesthetics to obtain smooth surfaces. Although the restored composite resin has a smooth surface, it gradually becomes rough over time. Therefore, this study measured glossiness to evaluate the surface of various composite resins and attempted to evaluate the maintenance of glossiness of composite resins by observing surfaces that change to roughness. Specimens were produced using resin used in clinical practice: Gradia direct anterior (GA), Tetric N-Ceram (TN), Ceram.X Sphere TEC one (CX), Filtek Z350XT (FT), Estelite sigma quick (ES). After creating a smooth surface with slide glass, five locations were randomly selected to measure surface gloss, and the average was the representative value of the specimen. Roughness was applied to the specimen under water pouring at the same speed and pressure using SiC paper #2400, 1200, and 400. The gloss unit of different SiC papers was measured. To evaluate the gloss unit and gloss retention between composite resins, one-way analysis of variance and Tukey multiple comparisons test were used. As a result of the study, there was a difference in gloss unit of specimens produced under the same conditions. Although the degree differed depending on the composite resin, there was also a difference in gloss retention. Based on the findings, composite resins show differences in gloss due to their different characteristics. Ceram.X Sphere TEC one (CX) showing the lowest gloss retention and Estelite sigma quick (ES) showing the highest.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.26 no.3
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• pp.292-298
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• 2017

Numerical analysis for various design parameters should be preceded by optimal design of composite materials. Numerous studies have been conducted on the bolting of interconnecting beams. In this study, the response surface method was applied to optimize the design of bolted joints connected by laminated wood composite beams. The response surface was created by combining the FEA code for composite analysis and the algorithm for forming the response surface. Optimization on this response surface was performed with a genetic algorithm to derive the results. The determination of the optimum bolt-hole position for the connection of composite beams is an optimization problem. Tsai-Wu composite failure index, maximum deflection, and simple von Mises stress are set as the objective functions. It has been proved that the design results of the optimized bolt-hole are superior to the design performance of the existing conventional bolt-hole position.

• Restorative Dentistry and Endodontics
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• v.14 no.1
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• pp.179-188
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• 1989

The purpose of this study was to measure Micro vicker's hardness of 4 kinds of anterior Composite resins (Pyrofil light bond anterior, Lite-fil anterior, Photo clear fil anterior, Silux) and 6 kinds of posterior Composite resin (Pyrofil light bond posterior. Lite-fil posterior, Photo clear fil posterior, Occlusin posterior, Palfique light posterior, P-30, posterior) according to deference of depth and distance of light tip from surface of composite resin. Each composite resin was filled into Teflon tube of 5mm in diameter and 5mm in depth, celluloid matrix was covered and the light in accordance with each composite resin was irradiated in distance of zero millimeter and 1 cm from light tip to surface of composite resin for 30 seconds. Specimens were sectioned longitudinally with cutting device. Microvicker's hardness measurements ware made at the depth of surface, 1mm, 2mm, 3mm, 4mm and 5mm from the surface to deep portion. Vicker's hardness numbers were taken on each depth under 200gm load for 30 seconds with MVK-E. The following results were: 1. The highest hardness value was measured at 1 mm depth. Then the deeper the depth, the lesser the hardness was observed. 2. The hardness value of anterior composite resins is lower than one of posterior composite resins. 3. Hardness number of composite resin irradiated in distance of zero millimeter from surface of composite resin was higher than one of 1 cm from surface of composite resin. 4. The pattern of hardness change at varying depth was similar to all the experimental material with no relation to distance of light from specimen.

• Restorative Dentistry and Endodontics
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• v.8 no.1
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• pp.107-113
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• 1982

The purpose of this study was to observe the tensile strength of composite resins to etched dentin surface with the various methods of placing bonding agent before composite resin or placing composite resin alone. Recently extracted 60 maxillary incisors were chosen. These were divided into 6 groups: Group I : Immediate Silar adaptation to the etched dentin surface with 37% phosphoric acid for 60 seconds without bonding agent. Group II : Immediate Silar adaptation to the etched dentin surface with 37% phosphoric acid for 60 seconds with bonding agent. Group III : Silar adaptation to the etched dentin surface with 37% phosphoric acid for 60 seconds after 5 minutes of bonding agent. Group IV : Immediate Enamelite adaptation to the etched dentin surfaces with 50% phosphoric acid for 120 seconds without bonding agent. Group V : Immediate Enamelite adaptation to the etched dentin surface with 50% phosphoric acid for 120 second s with bonding again. Group VI : Enamelite adaptation to the etched dentin surface with 50% phosphoric acid for 120 seconds after 5 minutes of bonding agent. All specimens were immersed in water at $37^{\circ}C$ for 24 hours before testing. The results were as follows: 1. The tensile strength of powder/liquid composite resin system was higher than that of pastel paste composite resin system. 2. The tensile strength of the composite resin group II, III, V, & VI with bonding agent was higher than that of the composite resin group I & IV without bonding agent. 3. The tensile strength of the composite resin group III & VI after 5 minutes added to bonding agent was higher than that of the composite resin group II & V immediately added to bonding agent.

• Restorative Dentistry and Endodontics
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• v.26 no.4
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• pp.316-325
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• 2001

The purpose of this study was to evaluate the effect of adhesive curing timing on the direction of polymerization shrinkage of light-curing composite resin. In this study, the curing times of adhesive and composite resin were measured by differential scanning calorimeter(DSC). 28 extracted human molars were embedded in clear resin and box-type cavities were prepared. Based on DSC data, the experimental teeth were divided into 4 groups. Group 1: no bond; Group 2: late curing; Group 3: Intermediate curing; Group 4: Early curing. After treating with adhesive, the buccal cavities were filled with Z-100 hybrid composite resin and the lingual ones were filled with AEliteflo flowable composite resin. The depressions at the surface were measured by surface profilometer, then the specimens were embedded in clear resin and sectioned. Impressions were obtained and used to get epoxy resin replicas. The epoxy replicas were gold-coated and observed under SEM. Average Maximum Gap(AMG), Gap Proportion(GP), Average Marginal Index(AMI) were used to compare the shrinkage gap of each group. The results were statistically analyzed using the Kruskal-Wallis One Way ANOVA, Student-Newman-Keuls method. The results of this study were as follows. 1. Average Maximum Gap, Gap Proportion, Average Marginal Index and depression at the surface or Z-100 hybride composite resin were smaller than those of AEliteflo flowable composite resin(P<0.05). 2. When the bonding between composite resin and tooth structure was strong, the shrinkage gap was small, and depression at the surface was deep(P<0.05). 3. In the well-bonded group, light-curing composite resin shrank toward bonded cavity wall, not toward light source. The result suggested that the direction of polymerization shrinkage was affected by the quality of bonding in the dentin-resin interface. The strong was the bonding between composite resin and tooth structure, the smaller was the gap and the deeper was the depression at the surface. Then the flow to compensate the polymerization shrinkage proceeded from surface to bonded cavity wall.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1998.06a
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• pp.195-198
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• 1998

In this paper, we study on the surface breakdown of Epoxy composite in silicon oil. Breakdown field strengths were simulated by using FEM with the experience data of surface breakdown of Epoxy composite. The surface endurance and field distribution (kV/mm) of Epoxy composite were calculated by FEM.

• Transactions of the Korean Society of Mechanical Engineers
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• v.14 no.2
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• pp.269-275
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• 1990

Nonaxisymmetric bifurcation behaviours of composite tubes two different materials subjected to uniform radial shrinkage at the external surface have been investigated and compared with those of single tube. The effect of material parameters normalized with respect to those of outer tube upon the bifurcation point and corresponding mode has been clarified. The parameters substantially affect the bifurcation mode with long-wavelength so that the composite tube with low hardening exponent or with high yield stress of inner tube destabilizes the overall deformation of the tube. However surface type bifurcation, short-wavelength mode, shown on the traction-free inner surface is hardly affected by the material parameters. The surface type bifurcation completely depends on the material characteristics of inner tube and the bifurcation point of composite tube almost coincides with the of single tube.

• Restorative Dentistry and Endodontics
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• v.42 no.1
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• pp.39-47
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• 2017

Objectives: Although the coating of surface sealants to dental composite resin may potentially reduce bacterial adhesion, there seems to be little information regarding this issue. This preliminary in vitro study investigated the adhesion of Streptococcus mutans (S. mutans) on the dental composite resins coated with three commercial surface sealants. Materials and Methods: Composite resin (Filtek Z250) discs (8 mm in diameter, 1 mm in thickness) were fabricated in a mold covered with a Mylar strip (control). In group PoGo, the surfaces were polished with PoGo. In groups PS, OG, and FP, the surfaces polished with PoGo were coated with the corresponding surface sealants (PermaSeal, PS; OptiGuard, OG; Fortify Plus, FP). The surfaces of the materials and S. mutans cells were characterized by various methods. S. mutans adhesion to the surfaces was quantitatively evaluated using flow cytometry (n = 9). Results: Group OG achieved the lowest water contact angle among all groups tested (p < 0.001). The cell surface of S. mutans tested showed hydrophobic characteristics. Group PoGo exhibited the greatest bacterial adhesion among all groups tested (p < 0.001). The sealant-coated groups showed statistically similar (groups PS and FP, p > 0.05) or significantly lower (group OG, p < 0.001) bacterial adhesion when compared with the control group. Conclusions: The application of the surface sealants significantly reduced S. mutans adhesion to the composite resin polished with the PoGo.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2002.10a
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• pp.15-19
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• 2002

In this work, the surface modification of carbon/epoxy composites was investigated using UV (ultraviolet ray) surface treatment to increase adhesion strength between the carbon/epoxy composites and adhesives. After UV surface treatment, XPS (X-ray photoelectron spectroscopy) tests were performed to analyze the surface characteristics of the carbon/epoxy composites. Comparing adhesion strengths with the surface characteristics, the effects of the surface modification of carbon/epoxy composites by UV surface treatments on the adhesion strengths were investigated.