• 제목/요약/키워드: superconducting material growth

검색결과 52건 처리시간 0.031초

초 저속 순차증착으로 제작한 Bi계 초전도 박막의 생성막 평가 (Analysis of the Hi-system Superconducting Thin Films Fabricated by Layer-by-Layer Deposition Method at an Ultra low growth rate)

  • 양승호;김영표;박용필
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
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    • pp.503-504
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    • 2007
  • $Bi_2Sr_2Ca_{n-1}Cu_nO_x$(n=0, 1, 2)superconducting thin films have been fabricated by atomic layer-by-layer deposition at an ultra low growth rate using IBS(Ion Beam Sputtering) method. During the deposition, 90 mol% ozone gas of typical pressure of $1{\sim}9{\times}10^{-5}$ Torr are supplied with ultraviolet light irradiation for oxidation. XRD and RHEED investigations reveal out that a buffer layer with some different compositions is formed at the early deposition stage of less than 10 units cell and then Bi-2201 oriented along the c-axis is grown.

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Flux Pinning Enhancement in Melt- Processed $(Y_{0.5}Nd_{0.25}Sm_{0.25})_{1.8}Ba_{2.4}Cu_{3.4}O_y$ Superconductors

  • Kim, So-Jung;Cheon, Nam-Young;Park, Jong-Kuk;Lee, Sang-Kyo;Shim, Sang-Heung
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2005년도 하계학술대회 논문집 Vol.6
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    • pp.280-281
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    • 2005
  • We have studied the superconducting properties and flux pinning enhancement of $(Y_{0.5}Nd_{0.25}Sm_{0.25})_{1.8}Ba_{2.4}Cu_{3.4}O_y$ [(YNS)-1.8] composite oxides by melt growth process in air. A sample prepared by this method showed well-textured microstructure, and $(Y_{0.5}Nd_{0.25}Sm_{0.25})_2BaCuO_5$ [(YNS)211] nonsuperconducting particles were uniformly dispersed in large (YNS)123 superconducting matrix. The sample showed a sharp superconducting transition at 91 K. The magnetization measurements of the (YSN)-1.8 sample exhibited the enhanced flux pinning, compared with $YBa_2Cu_3O_y$ (Y-123) sample without Sm and Nd.

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동시증착법에 의해 성장된 붕화마그네슘 박막의 증착속도에 따른 효과 (Effect of Deposition Rate on $MgB_2$ Thin Films Growth by Co-deposition Method)

  • 박성창;강성구;정대길;정준기;임영진;김찬중;김철진
    • Progress in Superconductivity
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    • 제10권1호
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    • pp.29-34
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    • 2008
  • Magnesium diboride ($MgB_2$) is an inexpensive and simple superconductor. This material was first synthesized and its structure confirmed in 1953 but its superconducting properties were not discovered until 2001 when they caused great excitement. In this study, superconducting $MgB_2$ thin films on the r-$Al_{2}O_3$ substrates have been grown by the combination of radio frequency magnetron sputtering of B and thermal evaporation of Mg. The deposition conditions were varied by changing deposition rate. Before the co-deposition of Mg and B, the deposition rates of each element have been measured separately. The $MgB_2$ layers had 400nm in thickness and superconducting transition temperatures have been measured around $\sim$38.6K. Superconducting properties have been measured by PPMS, XRD, and SEM.

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Fabrication of High Tc Superconducting Films by CVD Process

  • Lee, Sang-Heon
    • Transactions on Electrical and Electronic Materials
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    • 제5권3호
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    • pp.120-121
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    • 2004
  • YBaCuO thick films were fabricated by plasma enhanced chemical vapor deposition, and the crystallinity and the superconducting properties were investigated. The growth temperature to obtain the thick films was decreased by around 150$^{\circ}C$ due to plasma enhancement. The zero resistivity temperatures for films grown at 590$^{\circ}C$ and 620$^{\circ}C$ were 55 and 80 K, respectively.

Characterizing Pb-based superconducting thin films

  • Park, Sang-Il;Kim, Hong-Seok;Lee, Joon Sung;Doh, Yong-Joo
    • 한국초전도ㆍ저온공학회논문지
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    • 제16권4호
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    • pp.36-39
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    • 2014
  • We report on the superconducting and structural characteristics of Pb-based alloy ($Pb_{0.9}In_{0.1}$, $Pb_{0.8}In_{0.2}$ and $Pb_{0.85}Bi_{0.15}$) thin films, depending on the film deposition rate. The maximum critical magnetic field strength of $Pb_{0.85}Bi_{0.15}$ is almost six times larger than that of $Pb_{0.9}In_{0.1}$, and more rapid growth of the film enhances the critical magnetic field strength even for the same alloy material. Scanning electron microscopy inspection indicates that lower deposition rate condition is vulnerable to the formation of void structure in the film. Topographic images using atomic force microscopy are useful to optimize the deposition condition for the growth of smooth superconducting film. Our work can be utilized for future studies on hybrid superconducting devices using low-dimensional nanostructures.

국부용융성장법으로 제조한 (Sm/Y)-Ba-Cu-0계 고온복합초전도체의 CeO2첨가에 따른 초전도특성 (Superconducting Properties of (Sm/Y)-Ba-Cu-0 High Tc Composite Superconductors with CeO2 Additive by Zone-Melt Textured Growth)

  • 김소정
    • 한국전기전자재료학회논문지
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    • 제15권3호
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    • pp.269-274
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    • 2002
  • (Sm/Y)-Ba-Cu-O system high Tc composite superconductors with/without $CeO_2$ additive were directionally grown by zone-melting process, haying large temperature gradient, In air atmosphere. Cylindrical green rods of $({Sm/y})_{1.8}Ba_{2.4}Cu_{3.4}O_x$ [(Sm/Y)1.8] composite oxides by cold isostatic pressing(CIP) method using rubber mold were fabricated. The microstructure and superconducting properties were investigated by XRD, SEM, TEM and SQUID magnetometer. The size of nonsuperconducting $({Sm/y})_2BaCuO_5$ inclusions of the melt-textured (Sm/Y)1.8 sample with CeO$_2$ additive were remarkably reduced and uniformly distributed within the superconducting (Sm/Y)1.8 matrix. Both samples, with/without $CeO_2$ additive, showed an onset Tc $\geq$ 90 K and sharp superconducting transition. The critical current density Jc value of the $CeO_2$ addictive were $1{\times}10^5A/\textrm{cm}^2$ in 77 K, 0 Tesla.

용융법에 의한 YBa2Cu3O7-y 초전도체 제작 (Preparation of YBa2Cu3O7-y Superconductor Using Melt Method)

  • 이상헌
    • 한국전기전자재료학회논문지
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    • 제35권6호
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    • pp.622-625
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    • 2022
  • YBa2Cu3O7-y bulk as a high temperature oxide superconducting conductor has the high critical temperature of 92 K. YBa2Cu3O7-y bulk superconductors have been fabricated by a seeded melting growth. Magnetic properties were studied by using superconductor of melted YBa2Cu3O7-y oxides. It was demonstrated that Y2BaCuO5 particles acts as a pinning center which plays an important role on the magnetic properties. The thickness of the upper and lower pellets of the YBa2Cu3O7-y bulk was formed at 40 mm with 55 g of the composition, and the YBa2Cu3O7-y superconductor was manufactured through a heat treatment process. Manufacturing the superconducting bulk, it is possible to improve the pore density of the superconducting bulk by providing a path through which oxygen could be emitted.

철심과 권선을 이용한 전류제한기에 적용시킨 안정화층이 다른 YBCO Coated Conductor의 전류제한 특성에 관한 연구 (The Study on the Current Limiting Characteristics of YBCO Coated Conductor with Different kinds of Stabilization Layer Applied to SFCL Using Iron Core and Coil)

  • 이동혁;두호익;김용진;한병성;임성우;한상철;이정필
    • 한국전기전자재료학회논문지
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    • 제23권10호
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    • pp.788-792
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    • 2010
  • The yttrium-barium-copper-oxide (YBCO) coated conductor, which supplement the fault of the existing superconducting current-limit materials YBCO thin film, bismuth-strontium-calcium-copper-oxide(BSCCO) wire and bulk, has been improved its mechanical weakness and has high index; hence, after quench YBCO coated conductor could limit the fault current effectively because of fast resistance occurrence speed. Furthermore, it has wide applicable area as an current limit material because it shows different resistance occurrence tendency by the thickness and kind of stabilization material sputtered on the superconducting layer. Therefore, many researchers are carrying out the study of application of YBCO coated conductor to superconducting fault current limiter (SFCL) for making high quality current limit element, based on resistance type. On the other hand, the study for other type except resistance type has been rarely conducted for the application of YBCO coated conductor to SFCL as an current limit element. Consequently, in this study, YBCO coated conductor with different stabilization layer Cu and Stainless steel, is applied to SFCL using iron core and coil, and examine the many index points as an current limit element, such as current limit characteristic, the tendency of resistance occurrence, response time, the temperature trend for stability.

확산법에 의한 Bi-2223 초전도상의 제조 및 성장기구에 관한 연구 (Study on the fabrication and the growth mechanism of Bi-2223 superconducting phase by diffusion method)

  • 최성환;최효상;한태희;황종선;한병성
    • E2M - 전기 전자와 첨단 소재
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    • 제7권4호
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    • pp.281-288
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    • 1994
  • According to spread volume of B(BiPbCuO) layer, composition ratio and each stage of sintering process, we studied stability of high Tc superconductor phase and generation and growth movement of superconducting phase. The dual layer composed of SrCaCuO and BiPbCuO compound were prepared to develop the Bi-2223 superconductor[108K] through interaction and diffusion during sintering process. The dual layer samples were sintered at 830.deg. C for 0-210 hours. From the result, the optimum conditions were : spread volume(A:B=1:0.6), sintering time(210h) and composition ratio(A:S $r_{2}$C $a_{2}$C $u_{2}$- $O_{x}$, B:B $i_{1.9}$P $b_{0.5}$C $u_{3}$ $O_{y}$) at 830.deg. C.. C.C.C.

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Characterization and Electrical Properties in (YNS)BCO Oxides by Rod-type Seeded Melt Growth Process

  • Kim, So-Jung;Park, Jong-Kuk;Lee, Sang-Gyo
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
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    • pp.243-243
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    • 2007
  • We have studied the electrical properties and microstructure of $(Y_{0.5}Nd_{0.25}Sm_{0.25})Ba_2Cu_3O_y[(YNS)-123]$ Oxides by rod-type seeded melt growth process(RSMG) in air atmosphere. Rod-type $NdBa_2Cu_3O_y${Nd-123) seed crystals made a extrusion process method, were used for achieving the ab-plane alignment having large grains perpendicular to the center of (YNS)-123 samples. The observations using SEM and TEM micrographs of the melt-textured (YNS)-123 samples revealed that the nonsuperconducting $(Y_{0.5}Nd_{0.25}Sm_{0.25})Ba_2Cu_3O_y[(YNS)-211]$ inclusions are uniformly distributed in the superconducting matrix. The microstructure and electrical properties were investigated by XRD, SEM, TEM and DC SQUID magnetometer. The sample showed a sharp superconducting transition at 90 K. The magnetization values of the (YNS)-123 sample exhibited the enhanced electrical properties, compared with $YBa_2Cu_3O_y$(Y-123) sample.

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