• 제목/요약/키워드: sublimation method

검색결과 159건 처리시간 0.025초

환형 캐스케이드 내 고정된 터빈 블레이드 및 슈라우드에서의 열/물질전달 특성 (I) - 블레이드 끝단 인접 표면 - (Heat/Mass Transfer Characteristics on Stationary Turbine Blade and Shroud in a Low Speed Annular Cascade (I) - Near-tip Blade Surface -)

  • 이동호;조형희
    • 대한기계학회논문집B
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    • 제29권4호
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    • pp.485-494
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    • 2005
  • For the extensive investigation of local heat/mass transfer on the near-tip surface of turbine blade, experiments were conducted in a low speed stationary annular cascade. The turbine test section has a single stage composed of sixteen guide vanes and blades. The chord length and the height of the tested blade are 150 mm and about 125 mm, respectively. The blade has flat tip geometry and the mean tip clearance is about $2.5{\%}$ of the blade chord. Detailed mass transfer coefficient on the blade near-tip surface was obtained using a naphthalene sublimation technique. The inlet flow Reynolds number based on chord length and incoming flow velocity is changed from $1.0{\times}10^{5}\;to\;2.3{\times}10^{5}.$ Extremely complex heat transfer characteristics are observed on the blade surface due, to complicated flow patterns, such as flow acceleration, laminarization, transition, separation bubble and tip leakage flow. Especially, the suction side surface of the blade has higher heat/mass transfer coefficients and more complex distribution than the pressure side surface, which is related to the leakage flow. For all the tested Reynolds numbers, the heat/mass transfer characteristics on the turbine blade are the similar. The overall averaged $Sh_{c}$ values are proportional to $Re_{c}^{0.5}$ on the stagnation region and the laminar flow region such as the pressure side surface. However, since the flow is fully turbulent in the near-tip region, the heat/mass transfer coefficients are proportional to $Re_{c}^{0.8}.$

승화법에 의한 $CdS_{0.67}Se_{0.33}$ 단결정 성장과 광전도 특성 (Growth of $CdS_{0.67}Se_{0.33}$ single crystal by sublimation method and their photoconductive characteristics)

  • 홍광준;이상열
    • 센서학회지
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    • 제7권2호
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    • pp.131-139
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    • 1998
  • $CdS_{0.67}Se_{0.33}$ 단결정을 승화법으로 성장시켜 Laue 배면 반사법 (back refection Laue method)으로 결정성과 면의 방향이 (0001)임을 알아보았고, EDS(Energy Dispersive X-ray Spectrometer)를 이용하여 소성비가 $CdS_{0.67}Se_{0.33}$ 임을 확인하였다. Van der Pauw 법으로 Hall 효과를 측정하여 운반자 농도(carrier density)와 이동도(mobility)의 온도의존성을 연구하였으며, 이동도는 30 K에서 150 K까지는 불순물에 의한 산란 (impurity scattering)에 기인하고 있으며, 150 K에서 293 K까지는 격자 산란 (lattice scattering)에 따라 감소하였다. 또한 운반자 농도의 In n 대 (1/T)에서 구한 활성화 에너지는 0.21 eV였다. 광전도 셀(cell)의 특성으로 spectral response, 최대 허용 소비전력(maximum allowable power dissipation: MAPD), 광전류와 암전류(photocurrent/darkcurrent: pc/dc) 및 응답시간을 측정하였다. Cu 증기분위기에서 열처리한 광전도 셀의 경우 ${\gamma}$ = 0.99, pc/dc = $1.84{\times}10^{7}$, MAPD : 323mW, rise time : 9.3ms, decay time : 9.7ms로 가장 좋은 특성을 얻었다.

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승화법에 의한 CdS 단결정 성장 (Growth of CdS Single Crystal by Sublimation Method)

  • 정태수;김현숙;유평렬;신영진;신현길;김택성;정철훈;이훈;신영신;강신국;정경수;홍광준
    • 한국결정성장학회지
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    • 제3권2호
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    • pp.125-130
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    • 1993
  • 수직 2단 전기로를 제작하고 결정성장관에 꼬리관을 연결하여 seed 결정없이 승화 방법으로 CdS 결정을 성장하였다. 이때 시료부분과 성장부분의 온도차 ${\Delta}T$가 이론적인 값 $14.7^{\circ}C$와 비교해서 실험적으로 얻은 값이 $15^{\circ}C$ 로 아주 일치하는 값을 나타내었다. 이때 꼬리관의 온도를 $110^{\circ}C$로 시간당 0.38mm 정도로 빨리 결정성장관을 끌어 올려 결정을 성장하였다. 분말법의 X-선 회절무늬와 Laue 배면 반사법의 Laue 무늬로부터 성장된 결정이 육방정이고 결정성장관의 길이 방향으로 c축을 갖는 단결정임을 확인하였다. 또한 CdS 단결정은 상온에서 전자 이동도와 운반자 밀도는 각각 $316cm^2/V{\cdot}sec$$2.90{\times}10^{16}cm^{-3}$정도이였다.

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오프셋인쇄 및 교정인쇄용 색료의 색재현 특성에 대한 측색적 평가 (Colorimetric Evaluation on Color Reproduction Properties of the Colorants for Offset Printing and Proofing)

  • 강상훈
    • 한국인쇄학회지
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    • 제21권2호
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    • pp.31-42
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    • 2003
  • The optimum color proofing system with the similar colorants to the printing system has to be used in high quality offset color printing. And so, the evaluation on color reproduction properties of the colorants for proofer and press are very important. In this paper, the optimum color proofing method is recommended by means of colorimeric comparative evaluation on the color reproduction properties such as color gamut, color difference, hue error of the colorants for the proofing system of CRT monitor, inkjet printer, dye sublimation type digital proofer, and the actual printing system of offset press.

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성막조건에 따른 $\alpha$-Sexithienyl 박막의 물리적 특성 및 전기전도도에 관한 연구 (A study on the physical characteristics and conductivities of $\alpha$ -Sexithienyl thin films with various deposition conditions)

  • 박용인;권오관;오세운;최종선;김영관;신동명;강도열
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1997년도 춘계학술대회 논문집
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    • pp.91-94
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    • 1997
  • $\alpha$-sexithienyl($\alpha$-6T) thin films were deposited by Organic Molecular Beam Deposition(OMBD) technique, where the $\alpha$-6T was synthesized and purified by the sublimation method. The thin films of the $\alpha$-6T were deposited under various deposition conditions. The effects of deposition rate, substrate temperature. and vacuum pressure an the formation of these films have been studied. The molecular orientations of $\alpha$-6T films were investigated with the polarized electronic absorption spectroscopy. The molecules in the $\alpha$-6T film deposited at a low deposition rate under a high vacuum were aligned almost perpendicular to the substrate. The film deposited at an elevated substrate temperature (~9 $O^{\circ}C$) showed higher conductivity than the film deposited at room temperature.

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의용소자로 응용하기 위해 제작한 BSCCO 박막의 부착계수 해석 (Analysis of Sticking Coefficient in BSCCO Thin Film Fabricatied for apply to Biomedical device)

  • 양승호;박용필
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2006년도 추계학술대회 논문집 Vol.19
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    • pp.351-352
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    • 2006
  • BSCCO thin films are fabricated by an ion beam sputtering method, and sticking coefficients of the respective elements are evaluated. The sticking coefficient of Bi element in BSCCO film formation was observed to show a unique temperature dependence; it was almost a constant value of 0.49 below about $730^{\circ}C$ and decreased linearly over about $730^{\circ}C$. In contrast, Sr and Ca, displayed no such remarkable temperature dependence. This behavior of the sticking coefficient was explained consistently on the basis of the evaporation and sublimation processes of $Bi_2O_3$. It was concluded that Bi(2212) thin film constructs from the partial melted Bi(2201) phase with the aid of the liquid phase of $Bi_2O_3$.

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Bi 초전도 박막의 부착계수 해석 (Analysis of Sticking Coefficient in Bi-Superconducting Thin film)

  • 천민우;박용필;이성일
    • 한국전기전자재료학회논문지
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    • 제15권11호
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    • pp.997-1002
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    • 2002
  • BSCCO thin films are fabricated by an ion beam sputtering method, and sticking coefficients of the respective elements are evaluated. The sticking coefficient of Bi element in BSCCO film formation was observed to show a unique temperature dependence; it was almost a constant value of 0.49 below about 730$^{\circ}C$ and decreased linearly over about 730$^{\circ}C$ In contrast, Sr and Ca, displayed no such remarkable temperature dependence. This behavior of the sticking coefficient was explained consistently on the basis of the evaporation and sublimation processes of Bi$\sub$2/O$\sub$3/. It was concluded that Bi(2212) thin film constructs from the partial melted Bi(2201) phase with the aid of the liquid phase of Bi$\sub$2/O$\sub$3/.

핵연료 집합체에서의 열유동 특성에 관한 연구 (A Study on Thermal-hydraulic Characteristics for Nuclear Fuel Rod Bundle)

  • 유성연;정민호;김만웅;최영준;김현군
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2001년도 추계학술대회논문집B
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    • pp.3-8
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    • 2001
  • For the successful design of nuclear reactor, it is very important to investigate thermal-hydraulic characteristics of fuel rod bundle. Fluid flow and heat transfer in the non-circular cross-section of nuclear fuel rod bundle are different from those found in common circular tube. And complex three dimensional flow including secondary and vortex flow, is formed around the bundles. The purpose of this research is to examine how geometries and flow conditions affect heat transfer in fuel rod bundle. Design data for nuclear fuel rod bundle and structure are surveyed, and $3{\times}3$ sub-channel model is adopted in this study. Computational results are compared with the heat transfer data measured by naphthalene sublimation method, and numerical analysis and evaluation are performed at various design conditions and flow conditions.

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막냉각되는 원봉 표면에의 물질전달에 관한 실험적 연구 (Experimental Study of Mass Transfer on a Film Cooled Cirular Cylinder Surface)

  • 이준식;이택식;이상우
    • 대한기계학회논문집
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    • 제15권5호
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    • pp.1756-1762
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    • 1991
  • 본 연구에서는 막냉각되는 터빈블레이드에서의 열전달 계수를 측정하기 위하 여 열전달과 물질전달의 상사관계를 이용하였다.터빈블레이드의 선단을 다른 연구 에서와 마찬가지로 원봉으로 모사하였고, 원봉의 표면에 위치하고 있는 1열의 분사홀 로부터 제트가 분사될 때 분사홀 근처 및 그 하류에서의 물질 전달계수를 측정하기 위 해 나프탈렌승화법을 이용하였다. 분사홀 열의 위치를 정체점에서 하류방향으로 이 동시키면서, 물질전달계수의 변화를 연구하였고, 분사율(M=.rho.$_{j}$ U$_{j}$ /.rho.$_{\infty}$ U$_{\infty}$)의 영향도 고찰하였다.

평판 후류가 원통 표면의 물질전달에 미치는 영향에 대한 실험적 연구 (Experimental study on the effect of flat-plate wake on mass transfer about a cylinder in crossflow)

  • 맹두진;김형수;이준식
    • 대한기계학회논문집
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    • 제18권10호
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    • pp.2779-2786
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    • 1994
  • This study presents an experimental investigation of the effect of the wake on mass transfer about a circular cylinder in crossflow. The flat-plate wake was generated by merging two mirror images of turbulent boundary layers that were well developed along the both sides of flat plate with a sharp trailing edge. The velocity field was measured by a hot-wire system and the mass transfer rate by a naphthalene sublimation method. The mixing and developing stages of the wake were addressed to identify flow conditions. The mass transfer effects of different developing stages of the wake was discussed in detail. It is noted that a local maximum appears not at the front stagnation point but at a point a little downstream when the cylinder is located in the nearwake region and much more elevated mass transfer rate is obtained compared to effect of free-stream turbulence.