• 제목/요약/키워드: sublimation method

검색결과 159건 처리시간 0.024초

진공 동결에 의한 건조 화훼류의 품질특성 평가에 관한 연구 (The Evaluation for Quality Characteristics of Drying Flowering Plant by Vacuum-Freeze)

  • 김재돌
    • 동력기계공학회지
    • /
    • 제15권4호
    • /
    • pp.5-10
    • /
    • 2011
  • In case of using rapid vacuum-freeze drying for high quality dry flower of flowering plant, the morphological and physiological characteristics of dry rose showed as the following. The dry ratio of about 82% presented after 1 day in case of using rapid vacuum-freeze drying and it was reached that the optimum storage water content of general dry products was 18%. The dry ratio of about 89% presented after 4 days. This result indicates very short dry time comparing with natural dry time of 12 days. Also, the morphological characteristics of flowering plant in case of vacuum-freeze drying showed similar shape with real flower. The contraction decreased about 9% comparing with real flower under dry time of 72 hours. But the contraction in case of natural dry decreased 36% and showed noticeable difference. The brightness which affects physiological characteristics of dry flowering plant showed lower values according to the dry process and chromaticity was thick. After 4 days, natural dry was thick with about 2 times comparing with vacuum-freeze drying. In case of vacuum-freeze drying, the quantity of anthocyanin and chlorophyl which affect discoloration and bleaching of dry flowering plant showed the clear difference comparing with natural dry method due to the sublimation by vacuum after rapid freeze with short initial time.

원형가이드 설치에 따른 충돌제트/유출냉각에서 열/물질전달 특성 (Heat/Mass Transfer for Impingement/Effusion Cooling System with Circular Guide)

  • 홍성국;조형희
    • 대한기계학회논문집B
    • /
    • 제30권12호
    • /
    • pp.1147-1154
    • /
    • 2006
  • An experimental investigation was conducted to enhance the heat/mass transfer for impingement/effusion cooling system when the initial crossflow was formed. For the improvement of heat transfer, the circular guide is installed on the injection hole. At the fixed jet Reynolds number of 10,000, the measurements were carried out for blowing ratios ranging from 0.5 to 1.5. The local heat/mass transfer coefficients on the effusion plate are measured using a naphthalene sublimation method. The result presents that the circular guide protects the injected jet from the initial crossflow, increasing the heat/mass transfer. The heat transfer of stagnation region is hardly changed regardless of the blowing ratio. The secondary peak is obviously formed by flow transition to turbulent flow. At high blowing ratio of 1.5, the circular guide produces $26{\sim}30%$ augmentation on the averaged heat/mass transfer while the case without circular guide leads to the low and non-uniform heat/mass transfer. With the increased heat/mass transfer, the installation of circular guide is accompanied by the increase of pressure loss in the channel. However, the pressure drop caused by the circular guide is lower than that for other cooling technique with the circular pin fin.

CuO-Camphene 슬러리의 동결건조에 의한 Cu 다공체 제조 (Fabrication of Porous Cu by Freeze-Drying Method of CuO-Camphene Slurry)

  • 김민수;오승탁;장시영;석명진
    • 한국분말재료학회지
    • /
    • 제18권4호
    • /
    • pp.327-331
    • /
    • 2011
  • In order to fabricate the porous metal with controlled pore characteristics, unique processing by using metal oxide powder as the source and camphene as the sublimable material is introduced. CuO powder was selected as the source for the formation of Cu metal via hydrogen reduction. Camphene-based CuO slurry, prepared by milling at $47^{\circ}C$ with a small amount of dispersant, was frozen at $-25^{\circ}C$. Pores were generated subsequently by sublimation of the camphene. The green body was hydrogen-reduced at $200^{\circ}C$ for 30 min, and sintered at $500-700^{\circ}C$ for 1 h. Microstructural analysis revealed that the sintered Cu showed aligned large pore channels parallel to the camphene growth direction, and fine pores are formed around the large pore. Also, it showed that the pore size was controllable by the slurry concentration.

Growth of Nano- and Microstructured Indium Nitride Crystals by the Reaction of Indium Oxide with Ammonia

  • Jung, Woo-Sik;Ra, Choon-Sup;Min, Bong-Ki
    • Bulletin of the Korean Chemical Society
    • /
    • 제26권9호
    • /
    • pp.1354-1358
    • /
    • 2005
  • Nano- and microstructured indium nitride crystals were synthesized by the reaction of indium oxide ($In_2O_3$) powder and its pellet with ammonia in the temperature range 580-700 ${^{\circ}C}$. The degree of nitridation of $In_2O_3$ to InN was very sensitive to the nitridation temperature. The formation of zero- to three-dimensional structured InN crystals demonstrated that $In_2O_3$ is nitridated to InN via two dominant parallel routes (solid ($In_2O_3$)-to-solid (InN) and gas ($In_2O$)-to-solid (InN)). The growth of InN crystals with such various morphologies was explained by the vapor-solid (VS) mechanism where the degree of supersaturation of In vapor determines the growth morphology and the vapor was mainly by the reaction of $In_2O$ with ammonia and partially by sublimation of solid InN. The pellet method was proven to be useful to obtain homogeneous InN nanowires.

승화법에 의한 6H-SiC 단결정 성장 : (II) 내부 결함 해석 (6H-SiC single crystal growth by the sublimation method : (II) the analysis of internal defects)

  • 김화목;강승민;주경;심광보;오근호
    • 한국결정성장학회지
    • /
    • 제7권2호
    • /
    • pp.191-196
    • /
    • 1997
  • 다양한 미세결함분석기술(OM, TEM, AFM)을 이용하여 승화법에 의해서 성장된 6H-Sic 단결정 wafer의 내부미소결함을 분석하였다. Wafer내부에는 6각판상헝의 석출물 및 micropipes들이 독립적으로 혹은 혼합적으로 존재하고 있음이 확인되었고, TEM 분석에 의한 비정질상의 검출로 이들은 불안정한 결정성장 인자나 비화학양론적 $Si_{1-x}_xC_x$ 화합물 형성에 기인한다는 사실을 확인하였다.

  • PDF

회전하는 충돌제트/유출냉각기법에서 분사홀 변화에 따른 열/물질전달 특성 (Heat/Mass Transfer Characteristics for Variation of Injection Hole in Rotating Impingement/Effusion Cooling System)

  • 홍성국;조형희
    • 한국유체기계학회 논문집
    • /
    • 제10권3호
    • /
    • pp.25-32
    • /
    • 2007
  • The present paper deals with the heat/mass transfer characteristics for the rotating impingement/effusion cooling system. By changing the size and number of injection hole, its effects on heat/mass transfer are investigated and three different injection hole cases are considered such as LH, DH and SH, respectively. Reynolds number based on the effusion hole diameter is fixed to 3,330 and two jet orientations are considered. A naphthalene sublimation method is used to obtain the heat/mass transfer coefficients on the effusion plate. The LH case shows that the local heat/mass transfer is significantly varied by the rotation. Moreover, the low and non-uniform Sh distributions occur because the impinging jet is deflected by Coriolis force. Meanwhile, for DH and SH cases, the local heat/mass transfer coefficients are enhanced significantly compared to LH case and the rotation effect decreases with increasing the jet velocity. The averaged Sh value of DH and SH case rises up to 45%, 85% than that of LH case. However, the uniformity of heat/mass transfer deteriorates due to the steep variation of heat/mass transfer.

Passivation Layers for Organic Thin-film-transistors

  • Lee, Ho-Nyeon;Lee, Young-Gu;Ko, Ik-Hwan;Kang, Sung-Kee;Lee, Seong-Eui;Oh, Tae-Sik
    • Transactions on Electrical and Electronic Materials
    • /
    • 제8권1호
    • /
    • pp.36-40
    • /
    • 2007
  • Inorganic layers, such as SiOxNy and SiOx deposited using plasma sublimation method, were tested as passivation layer for organic thin-film-transistors (OTFTs). OTFTs with bottom-gate and bottom-contact structure were fabricated using pentacene as organic semiconductor and an organic gate insulator. SiOxNy layer gave little change in characteristics of OTFTs, but SiOx layer degraded the performance of OTFTs severely. Inferior barrier properties related to its lower film density, higher water vapor transmission rate (WVTR) and damage due to process environment of oxygen of SiOx film could explain these results. Polyurea and polyvinyl acetates (PVA) were tested as organic passivation layers also. PVA showed good properties as a buffer layer to reduce the damage come from the vacuum deposition process of upper passivation layers. From these results, a multilayer structure with upper SiOxNy film and lower PVA film is expected to be a superior passivation layer for OTFTs.

중환자실 간호사의 임종 환자 돌봄 경험 (Experiences of Critical Care Nurses Caring for Dying Patients)

  • 설은미;고진강
    • 중환자간호학회지
    • /
    • 제11권2호
    • /
    • pp.1-10
    • /
    • 2018
  • Purpose : This study aimed to develop an in-depth and comprehensive understanding of the experiences of critical care nurses caring for dying patients. Method : Eleven critical care nurses with experience in caring for dying patients were recruited from four tertiary hospitals. Semi-structured face-to-face interviews were conducted between November 2016 and March 2017. The transcribed data were analyzed using qualitative content analysis to identify major themes and sub-themes that represented the experiences of critical care nurses. Results : The following six themes, and twelve sub-themes, were identified: (1) the gap between expectation and reality, (2) a distorted meaning of death, (3) repeated emotional pain and stress, (4) finding a solution alone, (5) sublimation into mission and calling, and (6) integration into one's own life. Conclusion : This study found that critical care nurses experience various psychological difficulties while caring for dying patients, and they made efforts on their own to overcome them. These findings are expected to inform the development of specialized programs to support critical care nurses to tackle these challenges, create guidelines on caring for dying patients, and help promote death education.

회전하는 터빈 블레이드에서의 열전달 특성 (Detailed Heat Transfer Characteristics on Rotating Turbine Blade)

  • 이동호;조형희
    • 대한기계학회논문집B
    • /
    • 제30권11호
    • /
    • pp.1074-1083
    • /
    • 2006
  • In the present study, the effect of blade rotation on blade heat transfer is investigated by comparing with the heat transfer results for the stationary blade. The experiments are conducted in a low speed annular cascade with a single stage turbine and the turbine stage is composed of sixteen guide vanes and blades. The chord length and the height of the tested blade are 150 mm and about 125 mm, respectively. The blade has a flat tip and the mean tip clearance is 2.5% of the blade chord. A naphthalene sublimation method is used to measure detailed mass transfer coefficient on the blade. For the experiments, the inlet Reynolds number is $Re_c=1.5{\times}10^5$, which results in the blade rotation speed of 255.8 rpm. Blade rotation induces a relative motion between the blade and the shroud as well as a periodic variation of incoming flow. Therefore, different heat/mass transfer patterns are observed on the rotating blade, especially near the tip and on the tip. The relative motion reduces the tip leakage flow through the tip gap, which results in the reduction of the tip heat transfer. However, the effect of the tip leakage flow on the blade surface is increased because the tip leakage vortex is formed closer to the surface than the stationary case. The overall heat/mass transfer on the shroud is not affected much by the blade rotation.

충돌제트/유출냉각기법에서 횡방향유동이 열/물질전달에 미치는 영향 (Effect of Crossflow on Heat (Mass) Transfer of an Impingement/Effusion Cooling System)

  • 남용우;최종현;조형희;조형희
    • 대한기계학회:학술대회논문집
    • /
    • 대한기계학회 2003년도 춘계학술대회
    • /
    • pp.2219-2226
    • /
    • 2003
  • Two perforated plates are placed in parallel and staggered arrangements with a gap distance of 2 times of the hole diameter, and initial crossflow passes between the plates. Both the injection and effusion hole diameters are 10 mm, and the Reynolds number based on the hole diameter and hole-to-hole pitch are fixed to 10,000 and 6 times of the hole diameter, respectively. To investigate the effect of crossflow, the flow rate of crossflow is changed from 0.2 to 2 times of that of the impinging jet. A naphthalene sublimation method is used to determine the local heat/mass transfer coefficients on the upward facing surface of the effusion plate. With the initial crossflow, the heat/mass transfer rates on the effusion (target) plate decrease as the velocity of crossflow increases, since the crossflow induces the locally low transfer regions formed at the mid-way between the effusion holes. However, the impingement/effusion cooling with crossflow presents higher heat/mass transfer rates than the array jet impingement cooling with the same initial crossflow.

  • PDF