• Title/Summary/Keyword: step heat treatment

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Optimal Production of a Novel Furan Fatty Acid from 7,10-dihydroxy-8(E)-octadecenoic Acid by Heat Treatment

  • Ellamar, Joel B.;Sohn, Hye-Ran;Kim, Hak-Ryul
    • Current Research on Agriculture and Life Sciences
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    • v.31 no.1
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    • pp.25-29
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    • 2013
  • As a specialty oil, furan fatty acids have gained special attentions since they are known to play important roles in biological systems including human. Although several studies reported chemical synthesis of furan fatty acids, their synthesis consisted of complicated chemical multistep with chemical catalysts. Recently, a simple one-step heat treatment method was developed to produce a novel furan fatty acid, 7,10-epoxy-octadeca-7,9-dienoic acid (7,10-EODA) from a dihydroxyl fatty acid 7,10-dihydroxy-8(E)-octadecenoic acid (DOD). In this report we studied about optimization of environmental conditions for the maximum production of 7,10-EODA from DOD by heat treatment. Production of 7,10-EODA was maximized at over $85^{\circ}C$ for at least over 48 hour in hexane. Solvent volume for maximum production should be over 300 mL per 10 mg DOD.

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The Development of Medical Device for Strengthening the Intervertebral Disc (추간판 강화용 의료기 개발)

  • Ryu, Suchak;Kim, Seunghyeon;Jo, Sungkwang;Shim, Keonoh
    • Journal of the Korean Society for Heat Treatment
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    • v.35 no.1
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    • pp.20-26
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    • 2022
  • This paper was designed to prevent intervertebral disc escape and treatment. we produced downsized lumbar traction bed at home and automated system depending on weight and muscle mass by using 3D print and Arduino to confirm the possibility of prototyping. Hence, we checked muscle mass 10 males in their 20s with different exercise conditions, and it shows that average muscle mass of group who exercised was 56.63kg, and non-exercise group was 50.8 kg. this is shows lumbar repetitive exercise can show the traction therapy effect can be seen traction therapy effect. In addition, we installed wooden doll substitute people with spring and test changing of length. Traction bed has the steps ranging from 1 to 4, in which the motor with torque and rpm, ranging from 4.7 to 5.5 kgf and from 4.5 to 5.3 rpm, respectively. The motor controlled with the voltage of Arduino was operated for the length of the spine to be stretched to 4-5 mm. As increasing the weight of the wooden doll by 10g, it was confirmed that the spring increased by 4-5 mm from the first step to the fourth step.

Changes in quality characteristic of immature flat persimmon (Diospyros kaki Thunb) during heat treatment aging (열처리 숙성 중 반시 미숙과의 이화학적 특성)

  • Sim, Hye-Jin;Kang, Jae-Ran;Kang, Min-Jung;Choi, Myoung-Hyo;Suh, Hwa-Jin;Shin, Jung-Hye
    • Food Science and Preservation
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    • v.23 no.3
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    • pp.301-309
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    • 2016
  • The objective of this study was to investigate physicochemical and antioxidant characteristics of immature flat persimmon during 7 heat treatment aging steps. The pH decreased, and hence, acidity increased with aging. Hunter L value decreased with aging. The a value rapidly increased until step 3, whereas the b value decreased. Fructose content decreased while glucose contents slightly increased during aging. Hardness, chewiness and gumminess rapidly decreased, indicating softening in texture, but it was negligible after aging step 3. Phenolic compounds including gallic acid and homogentisic acid were detected at step 3 and then gradually increased with aging. However, contents of flavonoid and tannin were much higher in step 1 sample than others. The antioxidant activities observed by DPPH, ABTS, and FRAP assay were the highest at step 1 possibly due to the higher levels of flavonoids and tannin acid in the step 1 sample.

Plastic Deformation Behavior of Al6061 depending on Heat Treatment Condition (연속주조 Al6061 합금의 열처리에 따른 소성변형거동)

  • Park J. H.;Kwon Y. N.;Lee Y. S.;Lee J. H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2004.05a
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    • pp.127-130
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    • 2004
  • In the recent years, lightweight components fabricated with aluminum alloys have been applied into building the automobiles. Among the several competing fabrication methods, hot forging is taken as the most reliable technique to produce suspension parts such as control arms. Generally, Al forging products have been used widely for the aircraft building with the extruded stock as a starting material. For the economical base, however, the cast stocks turn to be as the forging stocks recently after a continuously casting technique was developed to produce quite a uniform microstructure enough to use for the forging process. Even more, there is a tendency to omit the homogenization step before forging, which is considered to be an indispensable process for all kinds of Al alloy, In the present study, a series of compression test was carried out to find out how the cast structure and the following heat treatments influence the deformation behavior, that is, forging characteristic.

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Behavior of Fatigue Crack Propagation of Micro-Hole and Micro-Slit Specimensns - For High-Frequency Heat Treantment Specimens - (微小圓孔 및 微小슬릿材의 疲勞크랙 傳播擧動)

  • 송삼홍;윤명진
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.10 no.1
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    • pp.78-85
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    • 1986
  • This study has been made to investigate Behavior of the fatigue crack propagation for the purpose of taking into consideration the fatigue behavior Which initiate and propagate in tip of defect of the defected specimens, Which Contain the micro-hole or micro-slit. Especially, the specimens have been conducted with high-freguency heat treatment of 850.deg. C, 1050.deg. C to consider strength elevation of defected specimens. The results of this study are as follow; (1) The case of the same in the length of crack, the fatigue crack propagation rate of the micro-slit is always faster than that of micre-hole. But, the first step of the fatigue crack propagation it is not always so. (2) Fatigue crack propagation rate of specimens with micro-slit or micro-hole which have been treated with high-frequency heat treatment satisfy the following formula between the fatigue crack propagation rate and nominal stress; dl/dN .var..sigma.$^{m}$ *l$^{n}$ .

Investigation of Through-thickness Microstructural Evolution in a 600 MPa-Grade Reinforced Steel Bar Manufactured by Tempcore Process (Tempcore 공정을 통해 제조된 600 MPa급 철근의 두께방향 미세구조 변화 분석)

  • Jiwon Park;Hyunji Kim;Singon Kang
    • Journal of the Korean Society for Heat Treatment
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    • v.36 no.6
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    • pp.367-373
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    • 2023
  • 600 MPa-grade deformed bar samples were manufactured by conventional hot rolling and subsequent Tempcore heat treatment processes. Considering the short-time water quenching step of the Tempcore process for hot-rolled steel, it is inevitable that the temperature profile of the deformed bar depends strongly on its position throughout the sample thickness. As a result, its microstructure can be easily divided into two regions, the surface and the core regions. The former is expected to have a fresh martensite microstructure under rapid cooling conditions, but self-tempering occurs due to the intense heat flow from the hot core region after the process. The latter is generally known to exhibit a mixed microstructure of ferrite and pearlite due to its slow cooling rate. In this study, detailed microstructural evolutions were examined through the thickness direction. The large variation of the microstructure through the thickness direction in the deformed bar samples is partly due to the easy carbon diffusion from the limited additions of alloying elements.

Reduction of Computing Time through FDM using Implicit Method and Latent Heat Treatment in Solidification Analysis (FDM에 의한 응고해석시 계산시간 단축을 위한 음적해법의 적용과 잠열처리방법)

  • Kim, Tae-Gyu;Choi, Jung-Kil;Hong, Jun-Pyo;Lee, Zin-Hyoung
    • Journal of Korea Foundry Society
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    • v.13 no.4
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    • pp.323-332
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    • 1993
  • An implicit finite difference formulation with three methods of latent heat treatment, such as equivalent specific heat method, temperature recovery method and enthalpy method, was applied to solidification analysis. The Neumann problem was solved to compare the numerical results with the exact solution. The implicit solutions with the equivalent specific heat method and the temperature recovery method were comparatively consistent with the Neumann exact solution for smaller time steps, but its error increased with increasing time step, especially in predicting the solidification beginning time. Although the computing time to solve energy equation using temperature recovery method was shorter than using enthalpy method, the method of releasing latent heat is not realistic and causes error. The implicit formulation of phase change problem requires enthalpy method to treat the release of latent heat reasonably. We have modified the enthalpy formulation in such a way that the enthalpy gradient term is not needed, and as a result of this modification, the computation stability and the computing time were improved.

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Heat Treatment for Improvement of Hardness Uniformity of Standard Hardness Blocks (경도 기준편의 경도 균일성 향상을 위한 열처리)

  • Hahn, J.H.;Hwang, N.M.;Kim, J.J.;Moon, H.G.
    • Journal of the Korean Society for Heat Treatment
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    • v.2 no.2
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    • pp.33-37
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    • 1989
  • In order to improve hardness uniformity of standard-hardness blocks. experimental procedure was designed using Taguchi Method. For this purpose the following factors were studied: austenitizing temperature, tempering condition, grinding condition, subzero treatment, lapping time, $15{\mu}m$ polishing time, final polishing time. These factors were processed and then ten hardness values were measured on each specimen. SN (signal to noise) ratio for each condition was calculated with standard variations of these values. Finally, from the calculated value of ANOVA on SN ratios, the lapping time was found to be the main factor Better uniformity with longer lapping time implies that residual stress that was formed after quenching is a dominent parameter that affects on the uniformity of hardness. Therefore, step-quenching method was adapted to minimize the residual stress. By this modification of quenching procedure, the hardness uniformity was improved remarkably and the yield ratio was increased from 55% to 88%.

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Effects of Annealing Treatments on Microstructure and Mechanical Property of co-sputtered TiNi Thin Film (Co-sputtering에 의해 증착된 TiNi 박막의 미세조직 및 기계적성질에 미치는 어닐링 열처리 효과)

  • Park, S.D.;Baeg, C.H.;Hong, J.W.
    • Journal of the Korean Society for Heat Treatment
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    • v.21 no.1
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    • pp.26-32
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    • 2008
  • Effects of annealing treatment on microstructure and mechanical property of co-sputtered TiNi thin films were studied. As-deposited films showed amorphous state. However, above annealing temperature of $500^{\circ}C$ martensite phase (B19'), precipitate phase ($Ti_2Ni$) and a small amount of parent phase ($B_2$) were present, and phase transformation behaviors were three multi-step phase transformations $B19^{\prime}{\rightarrow}B_2$ and $B_2{\rightarrow}R-phase$ and $R-phase{\rightarrow}B19^{\prime}$. Increase of martensite transformation temperature, increase of microhardness and Young's modulus of TiNi films annealed above $500^{\circ}C$ were discussed in terms of precipitate phase.

The Effect of Thermomechanical Treatment on the Microstructural Changes and Fatigue Properties in 7050 Al Alloy (7050 AI 합금의 가공열처리가 미세조직변화와 피로성질에 미치는 영향)

  • Kim, M.H.;Kwun, S.I.
    • Journal of the Korean Society for Heat Treatment
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    • v.4 no.4
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    • pp.24-33
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    • 1991
  • The effects of thermomechanical treatments on microstructure and fatigue properties of 7050 Al alloy were investigated. The precipitation kinetics changed to a faster rate due to cold deformation employed in this special TAHA thermomechanical treatments including pre-aging, plastic deformation and two step final-aging. The G.P. zones in the under-aged condition were cut by dislocations and dissolved during the plastic deformation. During the low cycle fatigue, the T6' condition showed cyclic hardening behavior whereas the TMT5, TMT27 and T76 conditions showed cyclic softening at above 0.7% total strain amplitudes. The ${\Delta}K_{th}$ value of TMT27 was improved more than two times, compared with that of T76 condition. The T6' with small shearable precipitates resulted in the markedly high ${\Delta}K_{th}$ value. This is thought to be resulted from dislocation reversibility and roughness-induced crack closure due to planarity of slip.

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