• Current Research on Agriculture and Life Sciences
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• 제31권1호
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• pp.25-29
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• 2013

As a specialty oil, furan fatty acids have gained special attentions since they are known to play important roles in biological systems including human. Although several studies reported chemical synthesis of furan fatty acids, their synthesis consisted of complicated chemical multistep with chemical catalysts. Recently, a simple one-step heat treatment method was developed to produce a novel furan fatty acid, 7,10-epoxy-octadeca-7,9-dienoic acid (7,10-EODA) from a dihydroxyl fatty acid 7,10-dihydroxy-8(E)-octadecenoic acid (DOD). In this report we studied about optimization of environmental conditions for the maximum production of 7,10-EODA from DOD by heat treatment. Production of 7,10-EODA was maximized at over $85^{\circ}C$ for at least over 48 hour in hexane. Solvent volume for maximum production should be over 300 mL per 10 mg DOD.

• 열처리공학회지
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• 제35권1호
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• pp.20-26
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• 2022

This paper was designed to prevent intervertebral disc escape and treatment. we produced downsized lumbar traction bed at home and automated system depending on weight and muscle mass by using 3D print and Arduino to confirm the possibility of prototyping. Hence, we checked muscle mass 10 males in their 20s with different exercise conditions, and it shows that average muscle mass of group who exercised was 56.63kg, and non-exercise group was 50.8 kg. this is shows lumbar repetitive exercise can show the traction therapy effect can be seen traction therapy effect. In addition, we installed wooden doll substitute people with spring and test changing of length. Traction bed has the steps ranging from 1 to 4, in which the motor with torque and rpm, ranging from 4.7 to 5.5 kgf and from 4.5 to 5.3 rpm, respectively. The motor controlled with the voltage of Arduino was operated for the length of the spine to be stretched to 4-5 mm. As increasing the weight of the wooden doll by 10g, it was confirmed that the spring increased by 4-5 mm from the first step to the fourth step.

• 한국식품저장유통학회지
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• 제23권3호
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• pp.301-309
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• 2016

미숙과의 가공법 제안 및 기능성 규명을 위한 기초 연구의 일환으로 반시 미숙과를 7 step으로 나누어 열처리 숙성하면서 이화학적 특성 및 항산화 활성의 변화를 분석하였다. 반시 미숙과는 숙성됨에 따라 수분함량과 pH는 점차 감소하고, 산도는 증가하는 경향이었다. 숙성이 진행됨에 따라 갈변이 유도되면서 step 3까지 적색도는 급격히 증가하였으며, 황색도는 큰 폭으로 감소하였다. 반시의 탄력성, 씹힘성과 점착성의 경우에는 step 2~3에서 변화한 후에는 유의적인 차이를 보이지 않았다. 숙성 중 반시 미숙과의 fructose의 함량은 감소한데 반해 glucose 함량은 미량 증가하였다. 페놀성 화합물은 gallic acid와 homogentisic acid, 2종이 검출되었는데 이들 화합물은 step 2까지는 검출되지 않았으나, step 3부터 숙성단계가 지남에 따라 함량이 증가하였다. 이와 상반되게 탄닌 함량은 step 1에서 가장 높게 측정되었고 step 2에서 급감하였다. 숙성 단계별 반시 미숙과 물 추출물의 DPPH와 ABTS 라디칼 소거능 및 FRAP법에 따른 항산화 활성은 시료의 농도에 비례하여 유의적으로 증가하였으나, 숙성이 진행될수록 오히려 낮아졌다.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2004년도 춘계학술대회 논문집
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• pp.127-130
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• 2004

In the recent years, lightweight components fabricated with aluminum alloys have been applied into building the automobiles. Among the several competing fabrication methods, hot forging is taken as the most reliable technique to produce suspension parts such as control arms. Generally, Al forging products have been used widely for the aircraft building with the extruded stock as a starting material. For the economical base, however, the cast stocks turn to be as the forging stocks recently after a continuously casting technique was developed to produce quite a uniform microstructure enough to use for the forging process. Even more, there is a tendency to omit the homogenization step before forging, which is considered to be an indispensable process for all kinds of Al alloy, In the present study, a series of compression test was carried out to find out how the cast structure and the following heat treatments influence the deformation behavior, that is, forging characteristic.

• 대한기계학회논문집
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• 제10권1호
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• pp.78-85
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• 1986

본 연구에서는 결함재의 결함선단에 발생 전파하는 피로거동을 검토하기 위해서 미소원공과 미소슬릿을 가공하고, 이것들의 피로한도를 기준으로 해서 이들 결함의 형상이 피로크랙 전파특성에 미치는 영향을 상세히 고찰하고자 한다.

• 열처리공학회지
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• 제36권6호
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• pp.367-373
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• 2023

600 MPa-grade deformed bar samples were manufactured by conventional hot rolling and subsequent Tempcore heat treatment processes. Considering the short-time water quenching step of the Tempcore process for hot-rolled steel, it is inevitable that the temperature profile of the deformed bar depends strongly on its position throughout the sample thickness. As a result, its microstructure can be easily divided into two regions, the surface and the core regions. The former is expected to have a fresh martensite microstructure under rapid cooling conditions, but self-tempering occurs due to the intense heat flow from the hot core region after the process. The latter is generally known to exhibit a mixed microstructure of ferrite and pearlite due to its slow cooling rate. In this study, detailed microstructural evolutions were examined through the thickness direction. The large variation of the microstructure through the thickness direction in the deformed bar samples is partly due to the easy carbon diffusion from the limited additions of alloying elements.

• 한국주조공학회지
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• 제13권4호
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• pp.323-332
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• 1993

An implicit finite difference formulation with three methods of latent heat treatment, such as equivalent specific heat method, temperature recovery method and enthalpy method, was applied to solidification analysis. The Neumann problem was solved to compare the numerical results with the exact solution. The implicit solutions with the equivalent specific heat method and the temperature recovery method were comparatively consistent with the Neumann exact solution for smaller time steps, but its error increased with increasing time step, especially in predicting the solidification beginning time. Although the computing time to solve energy equation using temperature recovery method was shorter than using enthalpy method, the method of releasing latent heat is not realistic and causes error. The implicit formulation of phase change problem requires enthalpy method to treat the release of latent heat reasonably. We have modified the enthalpy formulation in such a way that the enthalpy gradient term is not needed, and as a result of this modification, the computation stability and the computing time were improved.

• 열처리공학회지
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• 제2권2호
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• pp.33-37
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• 1989

In order to improve hardness uniformity of standard-hardness blocks. experimental procedure was designed using Taguchi Method. For this purpose the following factors were studied: austenitizing temperature, tempering condition, grinding condition, subzero treatment, lapping time, $15{\mu}m$ polishing time, final polishing time. These factors were processed and then ten hardness values were measured on each specimen. SN (signal to noise) ratio for each condition was calculated with standard variations of these values. Finally, from the calculated value of ANOVA on SN ratios, the lapping time was found to be the main factor Better uniformity with longer lapping time implies that residual stress that was formed after quenching is a dominent parameter that affects on the uniformity of hardness. Therefore, step-quenching method was adapted to minimize the residual stress. By this modification of quenching procedure, the hardness uniformity was improved remarkably and the yield ratio was increased from 55% to 88%.

• 열처리공학회지
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• 제21권1호
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• pp.26-32
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• 2008

Effects of annealing treatment on microstructure and mechanical property of co-sputtered TiNi thin films were studied. As-deposited films showed amorphous state. However, above annealing temperature of $500^{\circ}C$ martensite phase (B19'), precipitate phase ($Ti_2Ni$) and a small amount of parent phase ($B_2$) were present, and phase transformation behaviors were three multi-step phase transformations $B19^{\prime}{\rightarrow}B_2$ and $B_2{\rightarrow}R-phase$ and $R-phase{\rightarrow}B19^{\prime}$. Increase of martensite transformation temperature, increase of microhardness and Young's modulus of TiNi films annealed above $500^{\circ}C$ were discussed in terms of precipitate phase.

• 열처리공학회지
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• 제4권4호
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• pp.24-33
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• 1991

The effects of thermomechanical treatments on microstructure and fatigue properties of 7050 Al alloy were investigated. The precipitation kinetics changed to a faster rate due to cold deformation employed in this special TAHA thermomechanical treatments including pre-aging, plastic deformation and two step final-aging. The G.P. zones in the under-aged condition were cut by dislocations and dissolved during the plastic deformation. During the low cycle fatigue, the T6' condition showed cyclic hardening behavior whereas the TMT5, TMT27 and T76 conditions showed cyclic softening at above 0.7% total strain amplitudes. The ${\Delta}K_{th}$ value of TMT27 was improved more than two times, compared with that of T76 condition. The T6' with small shearable precipitates resulted in the markedly high ${\Delta}K_{th}$ value. This is thought to be resulted from dislocation reversibility and roughness-induced crack closure due to planarity of slip.