• Title/Summary/Keyword: standard testing method

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Fundamental study on the development of the testing method of Triclosan with GC/ECD and GC/MS (GC/ECD 및 GC/MS를 이용한 트리클로산 정량분석에 관한 기초 연구)

  • Jeong, Hui-Jae;Lee, Jae-In;Kweon, Deok-Jun;Eom, Hui-Jeong;Choi, Zel-Ho;Choi, Ki-In
    • Analytical Science and Technology
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    • v.25 no.6
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    • pp.410-415
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    • 2012
  • In this study, a fundamental study was conducted to establish the method for quantitative analysis and pretreatment of triclosan, one of the chemicals to be used as bactericides, detergents, and sterilizers. The extraction efficiency of triclosan was the highest when it was extracted by soxhlet apparatus with n-hexane, and it showed a satisfactory result when the samples were analyzed with both GC/ECD and GC/MS. To evaluate the reproductivity of the results, each 30 reference samples made with paper filter and cotton wool was prepared in this study. From the results with high extraction effectiveness, low analysis deviation, and good statistical analysis data, the method for the extraction and analysis for triclosan were resonable for the paper and textile samples applied in this study.

A Study on Manufacturing Method of Standard Void Specimens for Non-destructive Testing in RFI Process and Effect of Void on Mechanical Properties (RFI 공정 부품 비파괴검사용 표준 기공률 시편 제조 방법 및 기공률에 따른 기계적 물성 영향에 대한 연구)

  • Han, Seong-Hyeon;Lee, Jung-Wan;Kim, Jung-Soo;Kim, Young-Min;Kim, Wee-Dae;Um, Moon-Kwang
    • Composites Research
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    • v.32 no.6
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    • pp.395-402
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    • 2019
  • The RFI process is an OoA process that fiber mats and resin films are laminated and cured in a vacuum bag. In case that resin film is insufficient to fill empty space in fibers, it makes void defect in composites and this void decrease mechanical properties of the composites. For this reason, non-destructive testing is usually used to evaluate void of manufactured composites. So, in this study, a manufacturing method of standard void specimens, which are able to be used as references in non-destructive testing, was proposed by controlling resin film thickness in the RFI process. Also, a fiber compaction test was proposed as a method to set the resin film thicknesses depending on target voids of manufacturing panels. The target void panels of 0%, 2%, and 4% were made by the proposed methods, and signal attenuation depending on void was measured by non-destructive testing and image analysis. In addition, voids of specimens for tensile, in-plane, short beam and compressive tests were estimated by signal attenuation, and mechanical properties were evaluated depending on the voids.

A Basic Study on Accelerated Life Test Method and Device of DSA (Dimensionally Stable Anode) Electrode (촉매성 산화물 전극 (DSA, Dimensionally Stable Anode)의 가속수명 테스트 방법과 장치에 관한 기초 연구)

  • Kim, Dong-Seog;Park, Young-Seek
    • Journal of Environmental Science International
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    • v.27 no.6
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    • pp.467-475
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    • 2018
  • The lifetime of the electrode is one of the most important factors on the stability of the electrode. Since the lifetime of the DSA (Dimensionally stable anode) electrode is long, an accelerated lifetime test is required to reduce the test time. Beacuse there is no basis or standard method for accelerated lifetime testing, many researchers use different methods. Therefore, there is a need for basis and methods for accelerated lifetime testing that other researchers can follow. We designed a reactor system for accelerated lifetime testing and planned specific methods. Reactor system was circulating batch reactor. Reactor volume and cooling water tank were 12.5 L and 100 L, respectively. Electrode size was $2cm{\times}3cm$ (real electrolysis area, $5cm^2$). In order to maintain the harsh conditions, accelerated lifetime test was carried out in a high current density ($0.6A/cm^2$) and low electrolyte concentration (NaCl, 0.068 mol/L). Maintaining a constant temperature was an important operation parameter for exact accelerated lifetime test. As the accelerated lifetime test progressed, the active component of electrode surface was consumed and desorption occurred. At the point of 5 V rise, corrosion of the surface of the base material(titanium) also started.

Dimension Measurement of Nuclear Fuel Rods Using an Image Processing Technology (영상처리기술에 의한 핵연료봉의 제원 측정)

  • Koo, D.S.;Min, D.K.;You, G.S.;Shin, H.S.;Hong, K.P.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.19 no.2
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    • pp.79-84
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    • 1999
  • An image processing technology was developed to measure the dimension of nuclear fuel rods and the diameter of nuclear fuel rods was measured by this method. It was confirmed that parameters such as camera-to-specimen distance. camera location, light intensity and light characteristic would affect dimension measurement of nuclear fuel rods. The percent relative error and percent standard deviation of measuring the diameter of nuclear fuel rods using image processing method were 4.88%, ${\pm}3.34%$ while the percent relative error and percent standard deviation using conventional method were 12.7%, ${\pm}9.72%$, respectively. The accuracy of diameter measurement of nuclear fuel rods using image processing method was about 3 times as high as that using conventional method.

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Development of the Dissolution Test for Dobesilate Calcium Tablets and Acepifylline Tablets (도베실산칼슘 정 및 아세피필린 정의 용출시험법 개발)

  • Park, Chan-Ho;Lee, Jin-Ha;Kim, Eun-Jung;Sohn, Kyung-Hee;Kim, Young-Ok;Kim, Dong-Sup;Song, Young-Me;Sah, Hong-Kee;Choi, Hoo-Kyun
    • YAKHAK HOEJI
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    • v.55 no.2
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    • pp.131-137
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    • 2011
  • The dissolution test method and an analytical procedure by HPLC were developed and validated for dobesilate calcium tablets and acepifylline tablets. These drugs were not yet characterized by the dissolution specifications in Korean Pharmaceutical Codex. So, with each reference and test drugs, we did the preliminary and standard experiments based on the Korean Pharmacopeia Guideline of dissolution testing for solid oral dosage forms. The dissolution test for dobesilate calcium tablets was carried out under sink conditions as following: dissolution medium water, paddle rotation speed 50 rpm and vessel volume 900 ml. More than 90% of its label amount was released within 30 min in this method. Also the dissolution test for acepifylline tablets was carried out under sink conditions as follows: dissolution medium water, paddle rotation speed 100 rpm and vessel volume 900 ml. More than 90% of its label amount was released within 45 min in this method. The dissolution samples were analyzed with a precise and accurate HPLC method. The developed dissolution test showed specificity, linearity, precision and accuracy within the acceptable range. The dissolution testing method described above was adequate for the purpose and may be proposed as a pharmacopeial standard to assess the performance of dobesilate calcium tablets and acepifylline tablets.

Design of Particle Swarm Optimization-based Polynomial Neural Networks (입자 군집 최적화 알고리즘 기반 다항식 신경회로망의 설계)

  • Park, Ho-Sung;Kim, Ki-Sang;Oh, Sung-Kwun
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.60 no.2
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    • pp.398-406
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    • 2011
  • In this paper, we introduce a new architecture of PSO-based Polynomial Neural Networks (PNN) and discuss its comprehensive design methodology. The conventional PNN is based on a extended Group Method of Data Handling (GMDH) method, and utilized the polynomial order (viz. linear, quadratic, and modified quadratic) as well as the number of node inputs fixed (selected in advance by designer) at Polynomial Neurons located in each layer through a growth process of the network. Moreover it does not guarantee that the conventional PNN generated through learning results in the optimal network architecture. The PSO-based PNN results in a structurally optimized structure and comes with a higher level of flexibility that the one encountered in the conventional PNN. The PSO-based design procedure being applied at each layer of PNN leads to the selection of preferred PNs with specific local characteristics (such as the number of input variables, input variables, and the order of the polynomial) available within the PNN. In the sequel, two general optimization mechanisms of the PSO-based PNN are explored: the structural optimization is realized via PSO whereas in case of the parametric optimization we proceed with a standard least square method-based learning. To evaluate the performance of the PSO-based PNN, the model is experimented with using Gas furnace process data, and pH neutralization process data. For the characteristic analysis of the given entire data with non-linearity and the construction of efficient model, the given entire system data is partitioned into two type such as Division I(Training dataset and Testing dataset) and Division II(Training dataset, Validation dataset, and Testing dataset). A comparative analysis shows that the proposed PSO-based PNN is model with higher accuracy as well as more superb predictive capability than other intelligent models presented previously.

A STUDY ON THE RELIABILITY OF THE OPTICAL CARIES ACTIVITY TEST (광학적 치아우식활성 검사법의 신뢰도에 관한 연구)

  • Park, Cheol-Hong;Lee, Nan-Young;Lee, Sang-Ho
    • Journal of the korean academy of Pediatric Dentistry
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    • v.33 no.4
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    • pp.615-623
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    • 2006
  • The purpose of this study was to evaluate the specificity, sensitivity, and diagnostic power of caries activity test using LED fluorescence. The subjects of this study were 55 children of $6{\sim}7$ years old. LED light were irradiated to labial or buccal surface of all teeth. Fluorescence from initial carious lesion of teeth illuminated by an LED light was observed through barrier filter and the number of teeth showing lesion, size and position of lesion were counted. Streptococcus mutans colony counting and dDfFtT rate test were also done and their correlation was compared. And then specificity, sensitivity, diagnostic power of optical caries activity test using LED light were evaluated. 1. There was positive $correlation({\gamma}=0.43)$ between LED fluorescence test and Streptococcus mutans count(P<0.05). 2. When visual examination was defined to standard testing method, the specificity, sensitivity, diagnostic power of LED fluorescence test were 100%, 76.1%, and 100%. 3. When dDfFtT rate was defined to standard testing method, the specificity, sensitivity, diagnostic power of LED fluorescence test were 88.9%, 47.8%, and 95.7%. 4. When S. mutans colony counting was defined to standard testing method, the specificity, sensitivity, diagnostic power of LED fluorescence test were 100%, 58.7%, and 100%. Considering the above results, optical caries activity test using LED light could be regarded as a practical method because of its close relationship with microbiological caries activity test.

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Experimental Study of Frost Heaving using Temperature Controlled Triaxial Cell (투명 온도제어형 삼축셀을 이용한 흙의 동상 실내실험)

  • Ryu, Byung-Hyun;Jin, Hyun-Woo;Lee, Jangguen
    • Journal of the Korean GEO-environmental Society
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    • v.17 no.6
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    • pp.23-31
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    • 2016
  • Nowadays abnormal coldness happens frequently in Korea and frost heaving causes unexpected ground deformation which results in severe problems for structures such as roadway, railroad and cutoff slope. 'Frost heave' as one of the primary phenomenon is considered to be an important factor together with 'adfreeze bond-strength' and 'creep deformation' for structural design process in permafrost area. Therefore, the fundamental study for frost heave has to be preceded for design of geo-structures in cold region. While various experimental apparatuses have been developed, there still exist a certain level of limitation to evaluate the frost-heave characteristics as design parameters. There are no standard testing method and criteria for analyzing frost heaving in Korea because temperature controlled testing apparatuses including a freezing chamber are expensive. In this paper, a new standard freezing and thawing testing apparatus is introduced, which simulates various freezing and thawing conditions in a soil specimen by using a temperature controlled triaxial cell. Frost heaving tests were performed to assess the new testing apparatus and experimental procedure to evaluate frost heaving for soils is proposed.

A Study on Conformance Testing Method to Verify the BioAPI Based System Module (BioAPl기반 시스템 모듈을 검증하기 위한 적합성시험 방법 연구)

  • Lee Yoo-Young;Kwon Young-Bin
    • The KIPS Transactions:PartB
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    • v.11B no.7 s.96
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    • pp.759-768
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    • 2004
  • Recently the biometric recognition technology is intensively studied and the standardization of the technology has been highly demanded for its commercialization. Currently many blometric recognition products are being developed based on the BioAPl(Biometric Application Program-ming Interface) specification. However, the reliable testing tools (or scenarios) to evaluate performance and conformance of the products are not shown yet. In this paper, a conformance testing method is presented, which verifies a biometric recognition system to meet the requirements of the BioAPl standard. Two different testing procedures are used in the proposed method. The first procedure evaluates that each functions offered in the BioAPl specification are correctly implemented and that the functions are actually used in the system. Through the Procedure, a BSP(Biometric Service Provider) system is executed on the framework of the BioAPl functions. It requires selection of parameters and prece-dent functions that should be executed first. The second procedure evaluates the abilities of module management, handling operations and ver-ification process by the analysis of the test cases. It tests the correctness of the system operation when a testing scenario is given. The proposed testing method is applied on a fingerprint verification BSP using the sample BSP provided by the BioAPl consortium. The experimental results shows the benefits of the proposed testing method.

Fatigue property analysis of U rib-to-crossbeam connections under heavy traffic vehicle load considering in-plane shear stress

  • Yang, Haibo;Qian, Hongliang;Wang, Ping
    • Steel and Composite Structures
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    • v.38 no.3
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    • pp.271-280
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    • 2021
  • In this study, the fatigue property of U rib-to-crossbeam connections in orthotropic steel bridge (OSB) crossbeams under heavy traffic vehicle load was investigated considering the effects of in-plane shear stress. The applicability of an improved structural stress (ISS) method was validated for the fatigue behavior analysis of nonwelded arc-shaped cutout regions in multiaxial stress states. Various types of fatigue testing specimens were compared for investigating the equivalent structural stress, fatigue crack initiation positions, and failure modes with the unified standards. Furthermore, the implications of OSB crossbeams and specified loading cases are discussed with respect to the improved method. The ISS method is proven to be applicable for analyzing the fatigue property of nonwelded arc-shaped cutout regions in OSB crossbeams. The used method is essential for gaining a reliable prediction of the most likely failure modes under a specific heavy traffic vehicle load. The evaluated results using the used method are proven to be accurate with a slighter standard deviation. We obtained the trend of equivalent structural stress in arc-shaped cutout regions and validated the crack initiation positions and propagation directions by comparing them with the fatigue testing results. The implications of crossbeam spans on fatigue property are less significant than the effects of crossbeams.