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http://dx.doi.org/10.5806/AST.2012.25.6.410

Fundamental study on the development of the testing method of Triclosan with GC/ECD and GC/MS  

Jeong, Hui-Jae (Test & standard center, Korea institute of ceramic engineering & technology)
Lee, Jae-In (Test & standard center, Korea institute of ceramic engineering & technology)
Kweon, Deok-Jun (Test & standard center, Korea institute of ceramic engineering & technology)
Eom, Hui-Jeong (Test & standard center, Korea institute of ceramic engineering & technology)
Choi, Zel-Ho (Test & standard center, Korea institute of ceramic engineering & technology)
Choi, Ki-In (Test & standard center, Korea institute of ceramic engineering & technology)
Publication Information
Analytical Science and Technology / v.25, no.6, 2012 , pp. 410-415 More about this Journal
Abstract
In this study, a fundamental study was conducted to establish the method for quantitative analysis and pretreatment of triclosan, one of the chemicals to be used as bactericides, detergents, and sterilizers. The extraction efficiency of triclosan was the highest when it was extracted by soxhlet apparatus with n-hexane, and it showed a satisfactory result when the samples were analyzed with both GC/ECD and GC/MS. To evaluate the reproductivity of the results, each 30 reference samples made with paper filter and cotton wool was prepared in this study. From the results with high extraction effectiveness, low analysis deviation, and good statistical analysis data, the method for the extraction and analysis for triclosan were resonable for the paper and textile samples applied in this study.
Keywords
Triclosan; GC-MS; GC-ECD; test method;
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  • Reference
1 Aviva Glaser, "The Ubiquitous Triclosan: A common antibacterial agent exposed", Pesticides and You, vol. 24, No. 3, 2004.
2 US EPA, Triclosan Facts, pesticides, 2010. 3.
3 US FDA, "Triclosan: What Consumers Should Know", 2010. 4. 8. (http://www.fda.gov/ForConsumers/ConsumerUpdates/ucm205999.htm)
4 Department of Health and Ageing, Australia, "Triclosan", Priority existing chemical assessment report, No. 30, 2009. 1.
5 국립환경과학원, 유독물 등의 분류기준 및 표시방법에 관한 규정, 국립환경과학원고시 제2012-22호, 2012. 8. 22.
6 The Alliance for the Prudent Use of Antibiotics(APUA), Triclosan(white Paper), 2011. 1.
7 무역환경정보네트워크(TEN) 정책동향 게시판, "EU 소비자단체, 화장품의 트리클로산 사용에 대한 우려표명", 2012. 10. 24.