• YAKHAK HOEJI
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• v.48 no.1
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• pp.60-64
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• 2004

Near-infrared (NIR) spectroscopy was used to determine rapidly and nondestructively the content of ambroxol in intact ambroxol tablets containing 30 mg (12.5％ m/m nominal concentration) by collecting NIR spectra in range 1100-1750 nm. The laboratory-made samples had 10.3∼15.9％ m/m nominal ambroxol concentration. The measurements were made by reflection using a fiber-optic probe and calibration was carried out by partial least square regression (PLSR) with autoscaling. Model validation was performed by randomly splitting the data set into calibration and validation data set (7 samples as a calibration data set and 5 samples as a validation data set). The developed NIR method gave results comparable to the known values of tablets in a laboratorial manufacturing Process, standard error of calibration (SEC) and standard error of prediction (SEP) being 0.49％ and 0.49％ m/m respectively. The method showed good accuracy and repeatability NIR spectroscopic determination in intact tablets allowed the potential use of real time monitoring for a running production process.

• Journal of the Korean Society for Nondestructive Testing
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• v.30 no.4
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• pp.330-337
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• 2010

In this paper, 3-dimensional electromagnetic numerical analysis is performed about the eddy current(EC) array probe characteristic which is the next generation probe for accurate diagnosis of steam generator(SG) in nuclear power plants(NPPs). ASME(American Society of Mechanical Engineers) Standard and X-probe combo calibration standard tube are selected for acquisition of eddy current testing(ECT) signals and this result of compared with the real test signals for reasonability of result. Based on the analysis result of calibration standard tube, ECT signals that are about the defects of pitting, stress corrosion cracking(SCC), multiple SCC and wear is obtained. Material of specimen was Inconel 600 which is usually used for SG tubes in NPPs. The operation frequency of 300 kHz were used. The signal characteristics could be observed according to the various defects. The results in this paper can be helpful when the ECT signals from EC array probe are evaluated and analyzed.

• Journal of Korean Society for Atmospheric Environment
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• v.28 no.1
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• pp.52-58
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• 2012

In this study, the effect of standard phase difference in calibration of carbonyl compounds (CC) was evaluated by using their standards prepared in both gaseous and liquid phase. For this analysis, standards in both phases were prepared for 6 different CCs (formaldehyde (FA), acetaldehyde (AA), propionaldehyde (PA), butyraldehyde (BA), isovaleraldehyde (IA) and valeraldehyde (VA)) at similar concentration levels. Their gaseous standard was calibrated after derivatization with three types of DNPH cartridge, and their calibration results were compared against liquid-phase standards. Although there was a strong compatibility between 2 phases for CCs with lower molecular weights (e.g., formaldehyde and acetaldehyde), it was not the case for the heavier CCs. The results of our analysis indicate that the analytical bias of the heavier CCs can be significantly large (by more than a few tens of %). As a result, underestimation of hevier CCs can be significant, if their gaseous samples are quantified by liquid phase standard.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.32 no.9
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• pp.712-719
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• 2008

Light Oil Flow Standard System(LOFSS), as a national oil flow standard system, in Korea Research Institute of Standards and Science(KRISS) was developed for oil flowmeter calibration, and the expanded uncertainty of flow quantity determination was estimated within 0.04 %. In order to improve the reliability of the LOFSS measurement, a proficiency test was carried out in the flow range of 20 and $240\;m^3/h$ (Reynolds number $20,000{\sim}900,000$). A turbine flowmeter was used as a transfer package in round robin test. The water flow standard system of KRISS, the pipe prover of the national calibration and test organization and the master meter calibrator of the turbine flowmeter supplier, which used the different working fluid respectively, were compared with the turbine flowmeter measurement. The maximum difference of measurement was 0.15 % between the LOFSS and the pipe prover. The En numbers of the each system measurement were evaluated at the same Reynolds number. It was found that the En numbers were less than 1 in the comparison, which means the procedures of the uncertainty estimation of the each calibrators were reasonable and reliable.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.21 no.3
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• pp.100-109
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• 2022

In this study, calibration technology that increases the alignment accuracy in large flexible flat panels was studied. For precise of calibration, a systematization of the calibration algorithm was established, and a calibration correction technique was studied to revise calibration errors. A coordinate systems of camera and UVW stage was established to get the global position of the mark, and equations for translational and rotational calibration were systematically derived based on geometrical analysis. Correction process for the calibration data was carried, and alignment experiments were performed sequentially in cases of the presence or absence of calibration-correction. Alignment results of both calibration correction and non-calibration correction showed accuracy performance less than 1㎛. On the other hand, the standard deviation in calibration-correction is smaller than non-calibration correction. Therefore, calibration correction showed improvement of the alignment repeatability.

• Journal of the Korean Society for Precision Engineering
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• v.25 no.8
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• pp.9-16
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• 2008

• Proceedings of the KWS Conference
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• 2008.05a
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• pp.15-15
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• 2008

• The Bulletin of The Korean Astronomical Society
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• v.46 no.2
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• pp.76.1-76.1
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• 2021

Maemi Dual Field Telescope System (MDFTS) is a dual telescope system located at Kyung Hee University. The system consists of 0.4 m telescope and 0.1 m telescope for wide-field observation. The 0.4 m telescope provides photometric observation which covers a field of view of 21'×16'. It has been used for various purposes with Johnson-Cousins UBVRI broadband filter system, e.g., SomangNet and Intensive Monitoring Survey of Nearby Galaxies. In this poster, we present the standard calibration result for our broadband filter system. Also, we suggest a new usage of the KHAO 0.4m telescope which is narrowband photometry by demonstrating the standard calibration of H-alpha filter. For flux calibration, not only R filter but also V filter is used for compensating the central wavelength discrepancy between R filter and H-alpha filter.

• The Journal of the Acoustical Society of Korea
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• v.23 no.2
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• pp.90-102
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• 2004

According to the Mutual Recognition Arrangement (MRA), the calibration and/or test laboratories should satisfy the management and technical requirements ISO 17025 or equivalent. Chapter 5, Section 5.10.4 of the technical requirement of ISO 17025 suggests the required informations for calibration certificates, one of them is to state the uncertainty of measurement. The uncertainties of measurement in reciprocity calibration of standard laboratory microphone were calculated. The expanded uncertainties for 1 and 1/2 inch microphones were 0.03 dB in the middle frequency range and they increased up to 0.10 dB and 0.11 dB at 20 Hz, 0.07 dB and 0.08 dB at high frequency, respectively.

• Journal of the Semiconductor & Display Technology
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• v.2 no.4
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• pp.23-26
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• 2003

The general users find difficulties in using ellipsometers. Thus, the object of this study is to construct an ellipsometer with simple operation principle. We developed an ellipsometer which does not require alignment and calibration before measuring sample. A basis structure model after rotating a compensator spectroscopic ellipsometry, the fixed incidence angle at $70^{\circ}$. This ellipsometer does not demand calibration, because the plane of incidence is not changed due to the novel sample holder structure. The results for various standard samples were compared with those from conventional RCSE to test the performance of this instrument. Also repeated measurements were performed to test the precision of the calibration coefficient in a plane of incidence fixed.