• 약학회지
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• 제48권1호
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• pp.60-64
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• 2004

Near-infrared (NIR) spectroscopy was used to determine rapidly and nondestructively the content of ambroxol in intact ambroxol tablets containing 30 mg (12.5％ m/m nominal concentration) by collecting NIR spectra in range 1100-1750 nm. The laboratory-made samples had 10.3∼15.9％ m/m nominal ambroxol concentration. The measurements were made by reflection using a fiber-optic probe and calibration was carried out by partial least square regression (PLSR) with autoscaling. Model validation was performed by randomly splitting the data set into calibration and validation data set (7 samples as a calibration data set and 5 samples as a validation data set). The developed NIR method gave results comparable to the known values of tablets in a laboratorial manufacturing Process, standard error of calibration (SEC) and standard error of prediction (SEP) being 0.49％ and 0.49％ m/m respectively. The method showed good accuracy and repeatability NIR spectroscopic determination in intact tablets allowed the potential use of real time monitoring for a running production process.

• 비파괴검사학회지
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• 제30권4호
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• pp.330-337
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• 2010

본 논문은 원전 증기발생기(SG, steam generator) 세관의 정밀 진단을 위한 차세대 탐촉자인 배열형 와전류 탐촉자의 특성 해석에 대한 3차원 전자기 수치해석을 수행하였다. 다양한 결함 해석을 위해 ASME(American Society of Mechanical Engineers) 표준시험편과 X-probe combo 표준보정시험편(inline EXP/spiral groove combo standard)을 선정하여 탐상신호를 획득하고, 실제 실험 신호와 비교하여 결과의 타당성을 검증하였다. 표준 보정 시험편의 해석 결과를 바탕으로 원전 SG 세관에서 주로 발생하고 있는 pitting, SCC(stress corrosion cracking), multiple SCC, wear 결함에 대하여 탐상신호를 획득하였다. 해석 대상으로는 원자력발전소 SG 세관으로 사용하고 있는 Inconel 600 도체관을 사용하였고, 이때의 시험주파수는 300 kHz이다. 본 논문을 통하여 각각의 결함에 대한 신호 특성을 파악하여 배열형 와전류 탐촉자의 결함의 종류에 따른 신호 특성을 확인할 수 있었다. 본 논문의 결과는 배열형 와전류 탐촉자의 와전류 탐상 신호 평가시 도움이 될 것이다.

• 한국대기환경학회지
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• 제28권1호
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• pp.52-58
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• 2012

In this study, the effect of standard phase difference in calibration of carbonyl compounds (CC) was evaluated by using their standards prepared in both gaseous and liquid phase. For this analysis, standards in both phases were prepared for 6 different CCs (formaldehyde (FA), acetaldehyde (AA), propionaldehyde (PA), butyraldehyde (BA), isovaleraldehyde (IA) and valeraldehyde (VA)) at similar concentration levels. Their gaseous standard was calibrated after derivatization with three types of DNPH cartridge, and their calibration results were compared against liquid-phase standards. Although there was a strong compatibility between 2 phases for CCs with lower molecular weights (e.g., formaldehyde and acetaldehyde), it was not the case for the heavier CCs. The results of our analysis indicate that the analytical bias of the heavier CCs can be significantly large (by more than a few tens of %). As a result, underestimation of hevier CCs can be significant, if their gaseous samples are quantified by liquid phase standard.

• 대한기계학회논문집B
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• 제32권9호
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• pp.712-719
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• 2008

Light Oil Flow Standard System(LOFSS), as a national oil flow standard system, in Korea Research Institute of Standards and Science(KRISS) was developed for oil flowmeter calibration, and the expanded uncertainty of flow quantity determination was estimated within 0.04 %. In order to improve the reliability of the LOFSS measurement, a proficiency test was carried out in the flow range of 20 and $240\;m^3/h$ (Reynolds number $20,000{\sim}900,000$). A turbine flowmeter was used as a transfer package in round robin test. The water flow standard system of KRISS, the pipe prover of the national calibration and test organization and the master meter calibrator of the turbine flowmeter supplier, which used the different working fluid respectively, were compared with the turbine flowmeter measurement. The maximum difference of measurement was 0.15 % between the LOFSS and the pipe prover. The En numbers of the each system measurement were evaluated at the same Reynolds number. It was found that the En numbers were less than 1 in the comparison, which means the procedures of the uncertainty estimation of the each calibrators were reasonable and reliable.

• 한국기계가공학회지
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• 제21권3호
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• pp.100-109
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• 2022

In this study, calibration technology that increases the alignment accuracy in large flexible flat panels was studied. For precise of calibration, a systematization of the calibration algorithm was established, and a calibration correction technique was studied to revise calibration errors. A coordinate systems of camera and UVW stage was established to get the global position of the mark, and equations for translational and rotational calibration were systematically derived based on geometrical analysis. Correction process for the calibration data was carried, and alignment experiments were performed sequentially in cases of the presence or absence of calibration-correction. Alignment results of both calibration correction and non-calibration correction showed accuracy performance less than 1㎛. On the other hand, the standard deviation in calibration-correction is smaller than non-calibration correction. Therefore, calibration correction showed improvement of the alignment repeatability.

• 한국정밀공학회지
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• 제25권8호
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• pp.9-16
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• 2008

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2008년도 춘계학술발표대회 개요집
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• pp.15-15
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• 2008

• 천문학회보
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• 제46권2호
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• pp.76.1-76.1
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• 2021

Maemi Dual Field Telescope System (MDFTS) is a dual telescope system located at Kyung Hee University. The system consists of 0.4 m telescope and 0.1 m telescope for wide-field observation. The 0.4 m telescope provides photometric observation which covers a field of view of 21'×16'. It has been used for various purposes with Johnson-Cousins UBVRI broadband filter system, e.g., SomangNet and Intensive Monitoring Survey of Nearby Galaxies. In this poster, we present the standard calibration result for our broadband filter system. Also, we suggest a new usage of the KHAO 0.4m telescope which is narrowband photometry by demonstrating the standard calibration of H-alpha filter. For flux calibration, not only R filter but also V filter is used for compensating the central wavelength discrepancy between R filter and H-alpha filter.

• 한국음향학회지
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• 제23권2호
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• pp.90-102
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• 2004

교정 및/또는 시험기관은 국제상호인증협정 (Global Mutual Recognition Arrangement)에 따라 ISO 17025[1]의 경영요건 및 기술요건의 제반 조건 또는 이와 동등한 조건을 충족시켜야 한다. ISO 17025의 기술요건을 기술한 제 5장, 제 5.10.4 절은 교정성적서 (Calibration Certificate)에 대한 요구사항을 제시하고 있는데, 이들 중 하나가 측정 불확도 (Uncertainty of Measurement)를 교정성적서에 명시하여야 하는 것이다. 본 논문에서는 표준 마이크로폰의 가역교정에 따른 제반 불확도 요인을 측정 또는 계산하여 표준 마이크로폰의 교정에 대한 측정 불확도를 계산하였다. 중간 주파수 영역에서 1인치 및 1/2 인치 마이크로폰의 경우 확장불확도는 0.03 dB 였으며 20 Hz에서는 각각 0.10 dB과 0.11 dB, 고주파에서는 각각 0.07 dB와 0.08 dB까지 증가한다.

• 반도체디스플레이기술학회지
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• 제2권4호
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• pp.23-26
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• 2003

The general users find difficulties in using ellipsometers. Thus, the object of this study is to construct an ellipsometer with simple operation principle. We developed an ellipsometer which does not require alignment and calibration before measuring sample. A basis structure model after rotating a compensator spectroscopic ellipsometry, the fixed incidence angle at $70^{\circ}$. This ellipsometer does not demand calibration, because the plane of incidence is not changed due to the novel sample holder structure. The results for various standard samples were compared with those from conventional RCSE to test the performance of this instrument. Also repeated measurements were performed to test the precision of the calibration coefficient in a plane of incidence fixed.